Effect of in-situ growth and separate addition method in hydrothermal process on the structural and magnetic properties of CoNiFe2O4@functionalized CNTs nanocomposite
Multi-walled carbon nanotubes (MWCNT) were synthesized by the chemical vapor deposition method and functionalized successfully through a two-step procedure, namely sonication and acid reflux. Functionalized multi-wall carbon nanotubes (FMWCNT) were decorated with crystalline nickel-substituted cobal...
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| Veröffentlicht in: | Applied physics. A, Materials science & processing Materials science & processing, 2021-12, Vol.127 (12), Article 896 |
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| creator | Hossain, M. Al-Fahat Al-Mamun, M. Rahman, M. R. Hoque, Sheikh Manjura |
| description | Multi-walled carbon nanotubes (MWCNT) were synthesized by the chemical vapor deposition method and functionalized successfully through a two-step procedure, namely sonication and acid reflux. Functionalized multi-wall carbon nanotubes (FMWCNT) were decorated with crystalline nickel-substituted cobalt ferrite nanoparticles (CNF) by the two different routes of hydrothermal method to form CNF@FMWCNT nanocomposite. The nanocomposites with different weight ratios of CNF and FMWCNT were characterized by X-ray diffraction analysis (XRD), Transmission electron microscopy (TEM), Raman spectroscopy, Fourier-transform infrared spectra analyzer (FTIR), thermogravimetric analyzer (TGA), and physical property measurement system. The XRD patterns revealed the formation of the cubic phase spinel structure of CNF with the optimized 1:1 weight ratio composite with a crystallite size of 11.55 nm, accordingly the Williamson–Hall (W–H) analysis. TEM confirmed the functionalization of FMWCNT, crystallinity of CNF and better adhesion between ferrite and FMWCNT in FCI11 composite than FCS11. FTIR study confirmed the presence of functional groups in as-synthesized samples. The study of the Raman spectra provided useful information about the quality of MWCNT and its degree of functionalization, and the quality of nanocomposites. TGA study revealed that different nanocomposites were found to have dissimilar thermal stability depending on the different synthesis routes. The magnetic study showed CNF@FMWCNT nanocomposite of 1:1 weight percent composition, produced by in-situ growth method, obtained significant magnetization features among all the samples. Nanocomposites prepared by the in-situ growth method show improved characteristics than the separate addition technique. |
| doi_str_mv | 10.1007/s00339-021-05049-9 |
| format | Article |
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Al-Fahat ; Al-Mamun, M. ; Rahman, M. R. ; Hoque, Sheikh Manjura</creator><creatorcontrib>Hossain, M. Al-Fahat ; Al-Mamun, M. ; Rahman, M. R. ; Hoque, Sheikh Manjura</creatorcontrib><description>Multi-walled carbon nanotubes (MWCNT) were synthesized by the chemical vapor deposition method and functionalized successfully through a two-step procedure, namely sonication and acid reflux. Functionalized multi-wall carbon nanotubes (FMWCNT) were decorated with crystalline nickel-substituted cobalt ferrite nanoparticles (CNF) by the two different routes of hydrothermal method to form CNF@FMWCNT nanocomposite. The nanocomposites with different weight ratios of CNF and FMWCNT were characterized by X-ray diffraction analysis (XRD), Transmission electron microscopy (TEM), Raman spectroscopy, Fourier-transform infrared spectra analyzer (FTIR), thermogravimetric analyzer (TGA), and physical property measurement system. The XRD patterns revealed the formation of the cubic phase spinel structure of CNF with the optimized 1:1 weight ratio composite with a crystallite size of 11.55 nm, accordingly the Williamson–Hall (W–H) analysis. TEM confirmed the functionalization of FMWCNT, crystallinity of CNF and better adhesion between ferrite and FMWCNT in FCI11 composite than FCS11. FTIR study confirmed the presence of functional groups in as-synthesized samples. The study of the Raman spectra provided useful information about the quality of MWCNT and its degree of functionalization, and the quality of nanocomposites. TGA study revealed that different nanocomposites were found to have dissimilar thermal stability depending on the different synthesis routes. The magnetic study showed CNF@FMWCNT nanocomposite of 1:1 weight percent composition, produced by in-situ growth method, obtained significant magnetization features among all the samples. Nanocomposites prepared by the in-situ growth method show improved characteristics than the separate addition technique.</description><identifier>ISSN: 0947-8396</identifier><identifier>EISSN: 1432-0630</identifier><identifier>DOI: 10.1007/s00339-021-05049-9</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Applied physics ; Characterization and Evaluation of Materials ; Chemical synthesis ; Chemical vapor deposition ; Cobalt ferrites ; Condensed Matter Physics ; Crystal structure ; Crystallinity ; Crystallites ; Fourier transforms ; Functional groups ; Infrared analysis ; Infrared spectra ; Infrared spectroscopy ; Machines ; Magnetic properties ; Manufacturing ; Materials science ; Multi wall carbon nanotubes ; Nanocomposites ; Nanoparticles ; Nanotechnology ; Optical and Electronic Materials ; Physics ; Physics and Astronomy ; Processes ; Raman spectra ; Raman spectroscopy ; Spectrum analysis ; Surfaces and Interfaces ; Thermal stability ; Thin Films ; Transmission electron microscopy ; X-ray diffraction</subject><ispartof>Applied physics. A, Materials science & processing, 2021-12, Vol.127 (12), Article 896</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021</rights><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-ec5ec16f4ec610434dc866888d98a623ba1ac44ae6b537b26ec00993291744ba3</citedby><cites>FETCH-LOGICAL-c319t-ec5ec16f4ec610434dc866888d98a623ba1ac44ae6b537b26ec00993291744ba3</cites><orcidid>0000-0003-1715-0518 ; 0000-0003-2555-2322</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00339-021-05049-9$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00339-021-05049-9$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27922,27923,41486,42555,51317</link.rule.ids></links><search><creatorcontrib>Hossain, M. Al-Fahat</creatorcontrib><creatorcontrib>Al-Mamun, M.</creatorcontrib><creatorcontrib>Rahman, M. R.</creatorcontrib><creatorcontrib>Hoque, Sheikh Manjura</creatorcontrib><title>Effect of in-situ growth and separate addition method in hydrothermal process on the structural and magnetic properties of CoNiFe2O4@functionalized CNTs nanocomposite</title><title>Applied physics. A, Materials science & processing</title><addtitle>Appl. Phys. A</addtitle><description>Multi-walled carbon nanotubes (MWCNT) were synthesized by the chemical vapor deposition method and functionalized successfully through a two-step procedure, namely sonication and acid reflux. Functionalized multi-wall carbon nanotubes (FMWCNT) were decorated with crystalline nickel-substituted cobalt ferrite nanoparticles (CNF) by the two different routes of hydrothermal method to form CNF@FMWCNT nanocomposite. The nanocomposites with different weight ratios of CNF and FMWCNT were characterized by X-ray diffraction analysis (XRD), Transmission electron microscopy (TEM), Raman spectroscopy, Fourier-transform infrared spectra analyzer (FTIR), thermogravimetric analyzer (TGA), and physical property measurement system. The XRD patterns revealed the formation of the cubic phase spinel structure of CNF with the optimized 1:1 weight ratio composite with a crystallite size of 11.55 nm, accordingly the Williamson–Hall (W–H) analysis. TEM confirmed the functionalization of FMWCNT, crystallinity of CNF and better adhesion between ferrite and FMWCNT in FCI11 composite than FCS11. FTIR study confirmed the presence of functional groups in as-synthesized samples. The study of the Raman spectra provided useful information about the quality of MWCNT and its degree of functionalization, and the quality of nanocomposites. TGA study revealed that different nanocomposites were found to have dissimilar thermal stability depending on the different synthesis routes. The magnetic study showed CNF@FMWCNT nanocomposite of 1:1 weight percent composition, produced by in-situ growth method, obtained significant magnetization features among all the samples. Nanocomposites prepared by the in-situ growth method show improved characteristics than the separate addition technique.</description><subject>Applied physics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical synthesis</subject><subject>Chemical vapor deposition</subject><subject>Cobalt ferrites</subject><subject>Condensed Matter Physics</subject><subject>Crystal structure</subject><subject>Crystallinity</subject><subject>Crystallites</subject><subject>Fourier transforms</subject><subject>Functional groups</subject><subject>Infrared analysis</subject><subject>Infrared spectra</subject><subject>Infrared spectroscopy</subject><subject>Machines</subject><subject>Magnetic properties</subject><subject>Manufacturing</subject><subject>Materials science</subject><subject>Multi wall carbon nanotubes</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Optical and Electronic Materials</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Processes</subject><subject>Raman spectra</subject><subject>Raman spectroscopy</subject><subject>Spectrum analysis</subject><subject>Surfaces and Interfaces</subject><subject>Thermal stability</subject><subject>Thin Films</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><issn>0947-8396</issn><issn>1432-0630</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kc1OHDEQhK0IpCyEF-BkibNJ-2e841vQCpJICC7kbHk9PbtGO-PB9gjBA-U58WQj5Za-WGp_VV1SEXLJ4ZoDrL9mACkNA8EZNKAMM5_IiispGGgJJ2QFRq1ZK43-TM5yfoY6SogV-X3b9-gLjT0NI8uhzHSX4mvZUzd2NOPkkitIXdeFEuJIByz72FWW7t-6FMse0-AOdErRY860EnVFc0mzL3OqP4vN4HYjluAXbMJUAubl4CY-hDsUj-pbP49-sXeH8I4d3Tw8ZTq6Mfo4TLGGwi_ktHeHjBd_33Py6-72afOD3T9-_7m5uWdeclMY-gY9171CrzkoqTrfat22bWdap4XcOu68Ug71tpHrrdDoAYyRwvC1Ulsnz8nV0bcmfZkxF_sc51RzZSsao7RpoFGVEkfKp5hzwt5OKQwuvVkOdunDHvuwtQ_7pw9rqkgeRbnC4w7TP-v_qD4AQAaRKw</recordid><startdate>20211201</startdate><enddate>20211201</enddate><creator>Hossain, M. Al-Fahat</creator><creator>Al-Mamun, M.</creator><creator>Rahman, M. R.</creator><creator>Hoque, Sheikh Manjura</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-1715-0518</orcidid><orcidid>https://orcid.org/0000-0003-2555-2322</orcidid></search><sort><creationdate>20211201</creationdate><title>Effect of in-situ growth and separate addition method in hydrothermal process on the structural and magnetic properties of CoNiFe2O4@functionalized CNTs nanocomposite</title><author>Hossain, M. Al-Fahat ; Al-Mamun, M. ; Rahman, M. R. ; Hoque, Sheikh Manjura</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-ec5ec16f4ec610434dc866888d98a623ba1ac44ae6b537b26ec00993291744ba3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Applied physics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical synthesis</topic><topic>Chemical vapor deposition</topic><topic>Cobalt ferrites</topic><topic>Condensed Matter Physics</topic><topic>Crystal structure</topic><topic>Crystallinity</topic><topic>Crystallites</topic><topic>Fourier transforms</topic><topic>Functional groups</topic><topic>Infrared analysis</topic><topic>Infrared spectra</topic><topic>Infrared spectroscopy</topic><topic>Machines</topic><topic>Magnetic properties</topic><topic>Manufacturing</topic><topic>Materials science</topic><topic>Multi wall carbon nanotubes</topic><topic>Nanocomposites</topic><topic>Nanoparticles</topic><topic>Nanotechnology</topic><topic>Optical and Electronic Materials</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Processes</topic><topic>Raman spectra</topic><topic>Raman spectroscopy</topic><topic>Spectrum analysis</topic><topic>Surfaces and Interfaces</topic><topic>Thermal stability</topic><topic>Thin Films</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hossain, M. Al-Fahat</creatorcontrib><creatorcontrib>Al-Mamun, M.</creatorcontrib><creatorcontrib>Rahman, M. R.</creatorcontrib><creatorcontrib>Hoque, Sheikh Manjura</creatorcontrib><collection>CrossRef</collection><jtitle>Applied physics. A, Materials science & processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hossain, M. Al-Fahat</au><au>Al-Mamun, M.</au><au>Rahman, M. R.</au><au>Hoque, Sheikh Manjura</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of in-situ growth and separate addition method in hydrothermal process on the structural and magnetic properties of CoNiFe2O4@functionalized CNTs nanocomposite</atitle><jtitle>Applied physics. A, Materials science & processing</jtitle><stitle>Appl. Phys. A</stitle><date>2021-12-01</date><risdate>2021</risdate><volume>127</volume><issue>12</issue><artnum>896</artnum><issn>0947-8396</issn><eissn>1432-0630</eissn><abstract>Multi-walled carbon nanotubes (MWCNT) were synthesized by the chemical vapor deposition method and functionalized successfully through a two-step procedure, namely sonication and acid reflux. Functionalized multi-wall carbon nanotubes (FMWCNT) were decorated with crystalline nickel-substituted cobalt ferrite nanoparticles (CNF) by the two different routes of hydrothermal method to form CNF@FMWCNT nanocomposite. The nanocomposites with different weight ratios of CNF and FMWCNT were characterized by X-ray diffraction analysis (XRD), Transmission electron microscopy (TEM), Raman spectroscopy, Fourier-transform infrared spectra analyzer (FTIR), thermogravimetric analyzer (TGA), and physical property measurement system. The XRD patterns revealed the formation of the cubic phase spinel structure of CNF with the optimized 1:1 weight ratio composite with a crystallite size of 11.55 nm, accordingly the Williamson–Hall (W–H) analysis. TEM confirmed the functionalization of FMWCNT, crystallinity of CNF and better adhesion between ferrite and FMWCNT in FCI11 composite than FCS11. FTIR study confirmed the presence of functional groups in as-synthesized samples. The study of the Raman spectra provided useful information about the quality of MWCNT and its degree of functionalization, and the quality of nanocomposites. TGA study revealed that different nanocomposites were found to have dissimilar thermal stability depending on the different synthesis routes. The magnetic study showed CNF@FMWCNT nanocomposite of 1:1 weight percent composition, produced by in-situ growth method, obtained significant magnetization features among all the samples. Nanocomposites prepared by the in-situ growth method show improved characteristics than the separate addition technique.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s00339-021-05049-9</doi><orcidid>https://orcid.org/0000-0003-1715-0518</orcidid><orcidid>https://orcid.org/0000-0003-2555-2322</orcidid></addata></record> |
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| subjects | Applied physics Characterization and Evaluation of Materials Chemical synthesis Chemical vapor deposition Cobalt ferrites Condensed Matter Physics Crystal structure Crystallinity Crystallites Fourier transforms Functional groups Infrared analysis Infrared spectra Infrared spectroscopy Machines Magnetic properties Manufacturing Materials science Multi wall carbon nanotubes Nanocomposites Nanoparticles Nanotechnology Optical and Electronic Materials Physics Physics and Astronomy Processes Raman spectra Raman spectroscopy Spectrum analysis Surfaces and Interfaces Thermal stability Thin Films Transmission electron microscopy X-ray diffraction |
| title | Effect of in-situ growth and separate addition method in hydrothermal process on the structural and magnetic properties of CoNiFe2O4@functionalized CNTs nanocomposite |
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