Correlation between microstructures and tensile deformation behavior of a PM near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si alloy

A powder metallurgy (PM) near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si (wt.%) alloy was fabricated by in-situ dehydrogenation and hot extrusion of a TiH2-based powder compact and heat treatments. Three types of microstructures were obtained in the as-consolidated state and after different heat treatments. They ar...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2021-09, Vol.825, p.141909, Article 141909
Hauptverfasser: Wu, Xiaogang, Zhang, Bowen, Zhang, Youyun, Niu, Hongzhi, Zhang, Deliang
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page
container_issue
container_start_page 141909
container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
container_volume 825
creator Wu, Xiaogang
Zhang, Bowen
Zhang, Youyun
Niu, Hongzhi
Zhang, Deliang
description A powder metallurgy (PM) near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si (wt.%) alloy was fabricated by in-situ dehydrogenation and hot extrusion of a TiH2-based powder compact and heat treatments. Three types of microstructures were obtained in the as-consolidated state and after different heat treatments. They are a basketweave microstructure consisting of a network of inter-penetrating α plates filled with domains of ultrafine β transformed structure (βt) (Type I microstructure), an α/β lamellar microstructure with most β layers being thin and discontinuous plus α layers at prior β grain boundaries (Type II microstructure) and an α/βt lamellar microstructure (Type III microstructure). Although the three types of microstructures render the alloy with a similar yield strength (1085–1109 MPa) and ultimate tensile strength (1217–1239 MPa) due to the balanced effects of various strengthening mechanisms, the Type II microstructure exhibits a significantly lower tensile ductility than the other two types of microstructures (elongation to fracture: 5.5% vs. 13–14%). Examination of dislocations in the tensile deformed specimens reveals that dislocations cutting through the thin β layers in the Type II microstructure during deformation. Such interactions between moving dislocations and thin β layers in the Type II microstructure are expected to be the primary reason for the clearly lower strain hardening rate, premature fracture of grain boundary α layers and low tolerance to strain localization observed in the tensile tests, fracture surface examination and DIC analysis. This correlation between the microstructures and tensile deformation behavior strongly suggests that preventing moving dislocations cutting through thin β layers by turning them into thicker and ultrafine structure strengthened βt lamellae or blocks is critically important in ensuring high tensile ductility of high strength PM near α titanium alloys. •Three types of microstructures are obtained in a PM near α titanium alloy.•All three types of microstructures render the alloy with a similar high strength.•Type II microstructure gives a much lower tensile ductility than other two types of microstructures.•The lower ductility is attributed to dislocation cutting of thin β layers in Type II microstructure.•Preventing the dislocation cutting through is key for both high ductility and high strength.
doi_str_mv 10.1016/j.msea.2021.141909
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2592349254</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0921509321011758</els_id><sourcerecordid>2592349254</sourcerecordid><originalsourceid>FETCH-LOGICAL-c328t-81a8ba6dc2f70f9b27b31deefa57df160c7e5cc57418e26135f50e492f12428f3</originalsourceid><addsrcrecordid>eNp9kE1OwzAQhS0EEqVwAVaWWKfYTpwfiU1V8Se1Aqllw8ZynLFwlMTFTou6QGLJGk7CRThET0KiwpbNzCzem3nzIXRKyYgSGp-Xo9qDHDHC6IhGNCPZHhrQNAmDKAvjfTQgGaMBJ1l4iI68LwkhNCJ8gF4n1jmoZGtsg3NoXwAaXBvlrG_dSrUrBx7LpsAtNN5UgAvQ1tV_-ie5NtZhq7HE9zPcgHT4-wsvzPbtMx5XXWXzpqvRo-vnmd2-f3SR5wbLqrKbY3SgZeXh5LcP0cPV5WJyE0zvrm8n42mgQpa2QUplmsu4UEwnRGc5S_KQFgBa8qTQNCYqAa4UTyKaAotpyDUnEGVMUxaxVIdDdLbbu3T2eQW-FaVduaY7KRjPWNhJedSp2E7Vf-8daLF0ppZuIygRPWZRih6z6DGLHebOdLEzQZd_bcAJrww0CgrjQLWisOY_-w92P4uI</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2592349254</pqid></control><display><type>article</type><title>Correlation between microstructures and tensile deformation behavior of a PM near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si alloy</title><source>ScienceDirect Journals (5 years ago - present)</source><creator>Wu, Xiaogang ; Zhang, Bowen ; Zhang, Youyun ; Niu, Hongzhi ; Zhang, Deliang</creator><creatorcontrib>Wu, Xiaogang ; Zhang, Bowen ; Zhang, Youyun ; Niu, Hongzhi ; Zhang, Deliang</creatorcontrib><description>A powder metallurgy (PM) near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si (wt.%) alloy was fabricated by in-situ dehydrogenation and hot extrusion of a TiH2-based powder compact and heat treatments. Three types of microstructures were obtained in the as-consolidated state and after different heat treatments. They are a basketweave microstructure consisting of a network of inter-penetrating α plates filled with domains of ultrafine β transformed structure (βt) (Type I microstructure), an α/β lamellar microstructure with most β layers being thin and discontinuous plus α layers at prior β grain boundaries (Type II microstructure) and an α/βt lamellar microstructure (Type III microstructure). Although the three types of microstructures render the alloy with a similar yield strength (1085–1109 MPa) and ultimate tensile strength (1217–1239 MPa) due to the balanced effects of various strengthening mechanisms, the Type II microstructure exhibits a significantly lower tensile ductility than the other two types of microstructures (elongation to fracture: 5.5% vs. 13–14%). Examination of dislocations in the tensile deformed specimens reveals that dislocations cutting through the thin β layers in the Type II microstructure during deformation. Such interactions between moving dislocations and thin β layers in the Type II microstructure are expected to be the primary reason for the clearly lower strain hardening rate, premature fracture of grain boundary α layers and low tolerance to strain localization observed in the tensile tests, fracture surface examination and DIC analysis. This correlation between the microstructures and tensile deformation behavior strongly suggests that preventing moving dislocations cutting through thin β layers by turning them into thicker and ultrafine structure strengthened βt lamellae or blocks is critically important in ensuring high tensile ductility of high strength PM near α titanium alloys. •Three types of microstructures are obtained in a PM near α titanium alloy.•All three types of microstructures render the alloy with a similar high strength.•Type II microstructure gives a much lower tensile ductility than other two types of microstructures.•The lower ductility is attributed to dislocation cutting of thin β layers in Type II microstructure.•Preventing the dislocation cutting through is key for both high ductility and high strength.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2021.141909</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Compacting ; Cutting ; Deformation behavior ; Dehydrogenation ; Ductility ; Elongation ; Fracture surfaces ; Grain boundaries ; Hardening rate ; Heat treatment ; Hot extrusion ; Lamellar structure ; Mechanical properties ; Microstructure ; Microstructures ; Near α titanium alloy ; Powder metallurgy ; Strain hardening ; Strain localization ; Tensile deformation ; Tensile tests ; Thermomechanical powder consolidation ; Thin films ; Titanium alloys ; Titanium base alloys ; Turning (machining) ; Ultimate tensile strength ; Ultrafines</subject><ispartof>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing, 2021-09, Vol.825, p.141909, Article 141909</ispartof><rights>2021 Elsevier B.V.</rights><rights>Copyright Elsevier BV Sep 21, 2021</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c328t-81a8ba6dc2f70f9b27b31deefa57df160c7e5cc57418e26135f50e492f12428f3</citedby><cites>FETCH-LOGICAL-c328t-81a8ba6dc2f70f9b27b31deefa57df160c7e5cc57418e26135f50e492f12428f3</cites><orcidid>0000-0003-0055-0152 ; 0000-0002-2367-5778</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.msea.2021.141909$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3548,27923,27924,45994</link.rule.ids></links><search><creatorcontrib>Wu, Xiaogang</creatorcontrib><creatorcontrib>Zhang, Bowen</creatorcontrib><creatorcontrib>Zhang, Youyun</creatorcontrib><creatorcontrib>Niu, Hongzhi</creatorcontrib><creatorcontrib>Zhang, Deliang</creatorcontrib><title>Correlation between microstructures and tensile deformation behavior of a PM near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si alloy</title><title>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing</title><description>A powder metallurgy (PM) near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si (wt.%) alloy was fabricated by in-situ dehydrogenation and hot extrusion of a TiH2-based powder compact and heat treatments. Three types of microstructures were obtained in the as-consolidated state and after different heat treatments. They are a basketweave microstructure consisting of a network of inter-penetrating α plates filled with domains of ultrafine β transformed structure (βt) (Type I microstructure), an α/β lamellar microstructure with most β layers being thin and discontinuous plus α layers at prior β grain boundaries (Type II microstructure) and an α/βt lamellar microstructure (Type III microstructure). Although the three types of microstructures render the alloy with a similar yield strength (1085–1109 MPa) and ultimate tensile strength (1217–1239 MPa) due to the balanced effects of various strengthening mechanisms, the Type II microstructure exhibits a significantly lower tensile ductility than the other two types of microstructures (elongation to fracture: 5.5% vs. 13–14%). Examination of dislocations in the tensile deformed specimens reveals that dislocations cutting through the thin β layers in the Type II microstructure during deformation. Such interactions between moving dislocations and thin β layers in the Type II microstructure are expected to be the primary reason for the clearly lower strain hardening rate, premature fracture of grain boundary α layers and low tolerance to strain localization observed in the tensile tests, fracture surface examination and DIC analysis. This correlation between the microstructures and tensile deformation behavior strongly suggests that preventing moving dislocations cutting through thin β layers by turning them into thicker and ultrafine structure strengthened βt lamellae or blocks is critically important in ensuring high tensile ductility of high strength PM near α titanium alloys. •Three types of microstructures are obtained in a PM near α titanium alloy.•All three types of microstructures render the alloy with a similar high strength.•Type II microstructure gives a much lower tensile ductility than other two types of microstructures.•The lower ductility is attributed to dislocation cutting of thin β layers in Type II microstructure.•Preventing the dislocation cutting through is key for both high ductility and high strength.</description><subject>Compacting</subject><subject>Cutting</subject><subject>Deformation behavior</subject><subject>Dehydrogenation</subject><subject>Ductility</subject><subject>Elongation</subject><subject>Fracture surfaces</subject><subject>Grain boundaries</subject><subject>Hardening rate</subject><subject>Heat treatment</subject><subject>Hot extrusion</subject><subject>Lamellar structure</subject><subject>Mechanical properties</subject><subject>Microstructure</subject><subject>Microstructures</subject><subject>Near α titanium alloy</subject><subject>Powder metallurgy</subject><subject>Strain hardening</subject><subject>Strain localization</subject><subject>Tensile deformation</subject><subject>Tensile tests</subject><subject>Thermomechanical powder consolidation</subject><subject>Thin films</subject><subject>Titanium alloys</subject><subject>Titanium base alloys</subject><subject>Turning (machining)</subject><subject>Ultimate tensile strength</subject><subject>Ultrafines</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kE1OwzAQhS0EEqVwAVaWWKfYTpwfiU1V8Se1Aqllw8ZynLFwlMTFTou6QGLJGk7CRThET0KiwpbNzCzem3nzIXRKyYgSGp-Xo9qDHDHC6IhGNCPZHhrQNAmDKAvjfTQgGaMBJ1l4iI68LwkhNCJ8gF4n1jmoZGtsg3NoXwAaXBvlrG_dSrUrBx7LpsAtNN5UgAvQ1tV_-ie5NtZhq7HE9zPcgHT4-wsvzPbtMx5XXWXzpqvRo-vnmd2-f3SR5wbLqrKbY3SgZeXh5LcP0cPV5WJyE0zvrm8n42mgQpa2QUplmsu4UEwnRGc5S_KQFgBa8qTQNCYqAa4UTyKaAotpyDUnEGVMUxaxVIdDdLbbu3T2eQW-FaVduaY7KRjPWNhJedSp2E7Vf-8daLF0ppZuIygRPWZRih6z6DGLHebOdLEzQZd_bcAJrww0CgrjQLWisOY_-w92P4uI</recordid><startdate>20210921</startdate><enddate>20210921</enddate><creator>Wu, Xiaogang</creator><creator>Zhang, Bowen</creator><creator>Zhang, Youyun</creator><creator>Niu, Hongzhi</creator><creator>Zhang, Deliang</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0003-0055-0152</orcidid><orcidid>https://orcid.org/0000-0002-2367-5778</orcidid></search><sort><creationdate>20210921</creationdate><title>Correlation between microstructures and tensile deformation behavior of a PM near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si alloy</title><author>Wu, Xiaogang ; Zhang, Bowen ; Zhang, Youyun ; Niu, Hongzhi ; Zhang, Deliang</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c328t-81a8ba6dc2f70f9b27b31deefa57df160c7e5cc57418e26135f50e492f12428f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Compacting</topic><topic>Cutting</topic><topic>Deformation behavior</topic><topic>Dehydrogenation</topic><topic>Ductility</topic><topic>Elongation</topic><topic>Fracture surfaces</topic><topic>Grain boundaries</topic><topic>Hardening rate</topic><topic>Heat treatment</topic><topic>Hot extrusion</topic><topic>Lamellar structure</topic><topic>Mechanical properties</topic><topic>Microstructure</topic><topic>Microstructures</topic><topic>Near α titanium alloy</topic><topic>Powder metallurgy</topic><topic>Strain hardening</topic><topic>Strain localization</topic><topic>Tensile deformation</topic><topic>Tensile tests</topic><topic>Thermomechanical powder consolidation</topic><topic>Thin films</topic><topic>Titanium alloys</topic><topic>Titanium base alloys</topic><topic>Turning (machining)</topic><topic>Ultimate tensile strength</topic><topic>Ultrafines</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wu, Xiaogang</creatorcontrib><creatorcontrib>Zhang, Bowen</creatorcontrib><creatorcontrib>Zhang, Youyun</creatorcontrib><creatorcontrib>Niu, Hongzhi</creatorcontrib><creatorcontrib>Zhang, Deliang</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wu, Xiaogang</au><au>Zhang, Bowen</au><au>Zhang, Youyun</au><au>Niu, Hongzhi</au><au>Zhang, Deliang</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Correlation between microstructures and tensile deformation behavior of a PM near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si alloy</atitle><jtitle>Materials science &amp; engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2021-09-21</date><risdate>2021</risdate><volume>825</volume><spage>141909</spage><pages>141909-</pages><artnum>141909</artnum><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>A powder metallurgy (PM) near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si (wt.%) alloy was fabricated by in-situ dehydrogenation and hot extrusion of a TiH2-based powder compact and heat treatments. Three types of microstructures were obtained in the as-consolidated state and after different heat treatments. They are a basketweave microstructure consisting of a network of inter-penetrating α plates filled with domains of ultrafine β transformed structure (βt) (Type I microstructure), an α/β lamellar microstructure with most β layers being thin and discontinuous plus α layers at prior β grain boundaries (Type II microstructure) and an α/βt lamellar microstructure (Type III microstructure). Although the three types of microstructures render the alloy with a similar yield strength (1085–1109 MPa) and ultimate tensile strength (1217–1239 MPa) due to the balanced effects of various strengthening mechanisms, the Type II microstructure exhibits a significantly lower tensile ductility than the other two types of microstructures (elongation to fracture: 5.5% vs. 13–14%). Examination of dislocations in the tensile deformed specimens reveals that dislocations cutting through the thin β layers in the Type II microstructure during deformation. Such interactions between moving dislocations and thin β layers in the Type II microstructure are expected to be the primary reason for the clearly lower strain hardening rate, premature fracture of grain boundary α layers and low tolerance to strain localization observed in the tensile tests, fracture surface examination and DIC analysis. This correlation between the microstructures and tensile deformation behavior strongly suggests that preventing moving dislocations cutting through thin β layers by turning them into thicker and ultrafine structure strengthened βt lamellae or blocks is critically important in ensuring high tensile ductility of high strength PM near α titanium alloys. •Three types of microstructures are obtained in a PM near α titanium alloy.•All three types of microstructures render the alloy with a similar high strength.•Type II microstructure gives a much lower tensile ductility than other two types of microstructures.•The lower ductility is attributed to dislocation cutting of thin β layers in Type II microstructure.•Preventing the dislocation cutting through is key for both high ductility and high strength.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2021.141909</doi><orcidid>https://orcid.org/0000-0003-0055-0152</orcidid><orcidid>https://orcid.org/0000-0002-2367-5778</orcidid></addata></record>
fulltext fulltext
identifier ISSN: 0921-5093
ispartof Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2021-09, Vol.825, p.141909, Article 141909
issn 0921-5093
1873-4936
language eng
recordid cdi_proquest_journals_2592349254
source ScienceDirect Journals (5 years ago - present)
subjects Compacting
Cutting
Deformation behavior
Dehydrogenation
Ductility
Elongation
Fracture surfaces
Grain boundaries
Hardening rate
Heat treatment
Hot extrusion
Lamellar structure
Mechanical properties
Microstructure
Microstructures
Near α titanium alloy
Powder metallurgy
Strain hardening
Strain localization
Tensile deformation
Tensile tests
Thermomechanical powder consolidation
Thin films
Titanium alloys
Titanium base alloys
Turning (machining)
Ultimate tensile strength
Ultrafines
title Correlation between microstructures and tensile deformation behavior of a PM near α Ti–6Al–2Sn–4Zr–2Mo−0.1Si alloy
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-11T07%3A58%3A18IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Correlation%20between%20microstructures%20and%20tensile%20deformation%20behavior%20of%20a%20PM%20near%20%CE%B1%20Ti%E2%80%936Al%E2%80%932Sn%E2%80%934Zr%E2%80%932Mo%E2%88%920.1Si%20alloy&rft.jtitle=Materials%20science%20&%20engineering.%20A,%20Structural%20materials%20:%20properties,%20microstructure%20and%20processing&rft.au=Wu,%20Xiaogang&rft.date=2021-09-21&rft.volume=825&rft.spage=141909&rft.pages=141909-&rft.artnum=141909&rft.issn=0921-5093&rft.eissn=1873-4936&rft_id=info:doi/10.1016/j.msea.2021.141909&rft_dat=%3Cproquest_cross%3E2592349254%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2592349254&rft_id=info:pmid/&rft_els_id=S0921509321011758&rfr_iscdi=true