Usefulness of Dilution for Rapid Simultaneous Determination of Residual Pesticides in Edamame (Immature Soybeans) by LC-MS/MS
A rapid, easy and versatile, simultaneous analytical method by LC-MS/MS based on extraction of QuEChERS method (EN 15662:2008) was developed for the determination of residual pesticides in Edamame (immature soybeans). In this method, it allowed to prepare a test solution only dilution without purifi...
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| Veröffentlicht in: | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 2021/08/25, Vol.62(4), pp.133-137 |
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| container_title | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) |
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| creator | Daimon, Takumi Takahashi, Kunihiko |
| description | A rapid, easy and versatile, simultaneous analytical method by LC-MS/MS based on extraction of QuEChERS method (EN 15662:2008) was developed for the determination of residual pesticides in Edamame (immature soybeans). In this method, it allowed to prepare a test solution only dilution without purification using solid column. As a result, 202 analytes met the management criteria of the guideline for validity assessment (Ministry of Health, Labour and Welfare of Japan). Thus, the present method could be useful for a rapid simultaneous determination of residual pesticides in green soybean. |
| doi_str_mv | 10.3358/shokueishi.62.133 |
| format | Article |
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In this method, it allowed to prepare a test solution only dilution without purification using solid column. As a result, 202 analytes met the management criteria of the guideline for validity assessment (Ministry of Health, Labour and Welfare of Japan). Thus, the present method could be useful for a rapid simultaneous determination of residual pesticides in green soybean.</description><identifier>ISSN: 0015-6426</identifier><identifier>EISSN: 1882-1006</identifier><identifier>DOI: 10.3358/shokueishi.62.133</identifier><identifier>PMID: 34470943</identifier><language>jpn</language><publisher>Japan: Japanese Society for Food Hygiene and Safety</publisher><subject>Chromatography, Liquid ; Dilution ; Edamame (immature soybeans) ; Glycine max ; Labour ; LC-MS/MS ; Pesticide residues ; Pesticide Residues - analysis ; Pesticides ; QuEChERS method ; residual pesticide ; Soybeans ; Tandem Mass Spectrometry ; validation study ; Water purification</subject><ispartof>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi), 2021/08/25, Vol.62(4), pp.133-137</ispartof><rights>2021 Japanese Society for Food Hygiene and Safety</rights><rights>Copyright Japan Science and Technology Agency 2021</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,4009,27902,27903,27904</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/34470943$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Daimon, Takumi</creatorcontrib><creatorcontrib>Takahashi, Kunihiko</creatorcontrib><title>Usefulness of Dilution for Rapid Simultaneous Determination of Residual Pesticides in Edamame (Immature Soybeans) by LC-MS/MS</title><title>Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)</title><addtitle>Food Hyg. 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Thus, the present method could be useful for a rapid simultaneous determination of residual pesticides in green soybean.</description><subject>Chromatography, Liquid</subject><subject>Dilution</subject><subject>Edamame (immature soybeans)</subject><subject>Glycine max</subject><subject>Labour</subject><subject>LC-MS/MS</subject><subject>Pesticide residues</subject><subject>Pesticide Residues - analysis</subject><subject>Pesticides</subject><subject>QuEChERS method</subject><subject>residual pesticide</subject><subject>Soybeans</subject><subject>Tandem Mass Spectrometry</subject><subject>validation study</subject><subject>Water purification</subject><issn>0015-6426</issn><issn>1882-1006</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpFkU1PAjEQhhujEYL8AC-miRc9LHTbbukeDaCSQDQg5013OyvF_cB2e-Dgf3cVxMvMYZ75eOdF6DokA8YiOXSb-sODcRszEHQQMnaGuqGUNAgJEeeoS0gYBYJT0UF950xKCIlHlFF6iTqM8xGJOeuir7WD3BcVOIfrHE9M4RtTVzivLV6qndF4ZUpfNKqC2js8gQZsaSr1C7UNS3BGe1XgV3CNyYwGh02Fp1qVqgR8NytL1XgLeFXvU1CVu8fpHs_HwWI1XKyu0EWuCgf9Y-6h9eP0bfwczF-eZuOHebCljDRBLLM0BsgFybQm0SiWOWc85aJVk7NQSAqCZooICVxynVPKUipBMZoBVyRiPXR7mLuz9advL022tbdVuzKhkZCMcMJ5S90cKZ-WoJOdNaWy--TvWy0wOQBb16h3OAHKttILSP4tSQRN-E9ofTmVs42yCVTsG1BYiEg</recordid><startdate>2021</startdate><enddate>2021</enddate><creator>Daimon, Takumi</creator><creator>Takahashi, Kunihiko</creator><general>Japanese Society for Food Hygiene and Safety</general><general>Japan Science and Technology Agency</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>7T2</scope><scope>7T7</scope><scope>7U7</scope><scope>8FD</scope><scope>C1K</scope><scope>F1W</scope><scope>FR3</scope><scope>H95</scope><scope>H96</scope><scope>H97</scope><scope>H98</scope><scope>H99</scope><scope>L.F</scope><scope>L.G</scope><scope>P64</scope></search><sort><creationdate>2021</creationdate><title>Usefulness of Dilution for Rapid Simultaneous Determination of Residual Pesticides in Edamame (Immature Soybeans) by LC-MS/MS</title><author>Daimon, Takumi ; 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| ispartof | Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi), 2021/08/25, Vol.62(4), pp.133-137 |
| issn | 0015-6426 1882-1006 |
| language | jpn |
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| source | MEDLINE; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; AgriKnowledge（アグリナレッジ）AGROLib |
| subjects | Chromatography, Liquid Dilution Edamame (immature soybeans) Glycine max Labour LC-MS/MS Pesticide residues Pesticide Residues - analysis Pesticides QuEChERS method residual pesticide Soybeans Tandem Mass Spectrometry validation study Water purification |
| title | Usefulness of Dilution for Rapid Simultaneous Determination of Residual Pesticides in Edamame (Immature Soybeans) by LC-MS/MS |
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