Self-Propagating High-Temperature Synthesis of Ceramic Material Based on Aluminum-Magnesium Spinel and Titanium Diboride
― The aim of this work is to synthesize ceramic composite materials based on aluminum-magnesium spinel strengthened by titanium diboride particles by the self-propagating high-temperature synthesis (SHS) and study the combustion characteristics of synthesized materials, their microstructure, and pha...
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| Veröffentlicht in: | Russian journal of inorganic chemistry 2021-08, Vol.66 (8), p.1115-1120 |
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| container_title | Russian journal of inorganic chemistry |
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| creator | Chizhikov, A. P. Konstantinov, A. S. Bazhin, P. M. |
| description | ―
The aim of this work is to synthesize ceramic composite materials based on aluminum-magnesium spinel strengthened by titanium diboride particles by the self-propagating high-temperature synthesis (SHS) and study the combustion characteristics of synthesized materials, their microstructure, and phase composition. For the synthesis of materials, powders of boron oxide, aluminum, magnesium, and titanium have been used. It is shown that changing the ratio of magnesium and aluminum in the composition of the initial charge results in changes in the phase composition of the synthesis products. As a result of the synthesis, composite materials based on aluminum-magnesium spinel with different contents of aluminum cations have been obtained: MgAl
3
O
4
, MgAl
2
O
4
, MgAlO
4
, and Mg
1.5
Ti
1.5
O
4
. It is shown that with an increase in the combustion temperature of the studied compositions, the morphology of the particles of the powders obtained with composite structures changes. It is shown that after SHS, crystallites of aluminum-magnesium spinel with a size of about 50 nm are formed. |
| doi_str_mv | 10.1134/S0036023621080039 |
| format | Article |
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The aim of this work is to synthesize ceramic composite materials based on aluminum-magnesium spinel strengthened by titanium diboride particles by the self-propagating high-temperature synthesis (SHS) and study the combustion characteristics of synthesized materials, their microstructure, and phase composition. For the synthesis of materials, powders of boron oxide, aluminum, magnesium, and titanium have been used. It is shown that changing the ratio of magnesium and aluminum in the composition of the initial charge results in changes in the phase composition of the synthesis products. As a result of the synthesis, composite materials based on aluminum-magnesium spinel with different contents of aluminum cations have been obtained: MgAl
3
O
4
, MgAl
2
O
4
, MgAlO
4
, and Mg
1.5
Ti
1.5
O
4
. It is shown that with an increase in the combustion temperature of the studied compositions, the morphology of the particles of the powders obtained with composite structures changes. It is shown that after SHS, crystallites of aluminum-magnesium spinel with a size of about 50 nm are formed.</description><identifier>ISSN: 0036-0236</identifier><identifier>EISSN: 1531-8613</identifier><identifier>DOI: 10.1134/S0036023621080039</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Aluminum ; Boron oxides ; Chemistry ; Chemistry and Materials Science ; Combustion temperature ; Composite materials ; Composite structures ; Crystallites ; Inorganic Chemistry ; Magnesium ; Morphology ; Particulate composites ; Phase composition ; Self propagating high temperature synthesis ; Spinel ; Synthesis and Properties of Inorganic Compounds ; Titanium ; Titanium diboride</subject><ispartof>Russian journal of inorganic chemistry, 2021-08, Vol.66 (8), p.1115-1120</ispartof><rights>Pleiades Publishing, Ltd. 2021. ISSN 0036-0236, Russian Journal of Inorganic Chemistry, 2021, Vol. 66, No. 8, pp. 1115–1120. © Pleiades Publishing, Ltd., 2021. Russian Text © The Author(s), 2021, published in Zhurnal Neorganicheskoi Khimii, 2021, Vol. 66, No. 8, pp. 1002–1008.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-b00e3e264db034d2bec29aa564cd81858855d1af7ff86c6c198c6dbbb52626fc3</citedby><cites>FETCH-LOGICAL-c316t-b00e3e264db034d2bec29aa564cd81858855d1af7ff86c6c198c6dbbb52626fc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0036023621080039$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0036023621080039$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Chizhikov, A. P.</creatorcontrib><creatorcontrib>Konstantinov, A. S.</creatorcontrib><creatorcontrib>Bazhin, P. M.</creatorcontrib><title>Self-Propagating High-Temperature Synthesis of Ceramic Material Based on Aluminum-Magnesium Spinel and Titanium Diboride</title><title>Russian journal of inorganic chemistry</title><addtitle>Russ. J. Inorg. Chem</addtitle><description>―
The aim of this work is to synthesize ceramic composite materials based on aluminum-magnesium spinel strengthened by titanium diboride particles by the self-propagating high-temperature synthesis (SHS) and study the combustion characteristics of synthesized materials, their microstructure, and phase composition. For the synthesis of materials, powders of boron oxide, aluminum, magnesium, and titanium have been used. It is shown that changing the ratio of magnesium and aluminum in the composition of the initial charge results in changes in the phase composition of the synthesis products. As a result of the synthesis, composite materials based on aluminum-magnesium spinel with different contents of aluminum cations have been obtained: MgAl
3
O
4
, MgAl
2
O
4
, MgAlO
4
, and Mg
1.5
Ti
1.5
O
4
. It is shown that with an increase in the combustion temperature of the studied compositions, the morphology of the particles of the powders obtained with composite structures changes. It is shown that after SHS, crystallites of aluminum-magnesium spinel with a size of about 50 nm are formed.</description><subject>Aluminum</subject><subject>Boron oxides</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Combustion temperature</subject><subject>Composite materials</subject><subject>Composite structures</subject><subject>Crystallites</subject><subject>Inorganic Chemistry</subject><subject>Magnesium</subject><subject>Morphology</subject><subject>Particulate composites</subject><subject>Phase composition</subject><subject>Self propagating high temperature synthesis</subject><subject>Spinel</subject><subject>Synthesis and Properties of Inorganic Compounds</subject><subject>Titanium</subject><subject>Titanium diboride</subject><issn>0036-0236</issn><issn>1531-8613</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kEtLAzEUhYMoWB8_wF3AdTSPmTRd1vqo0KIwdT1k8pimzGTGZAbsvzelggtxdS_3fOdcOADcEHxHCMvuC4wZx5RxSrBI--wETEjOCBKcsFMwOcjooJ-Dixh3GGcZnooJ-CpMY9F76HpZy8H5Gi5dvUUb0_YmyGEMBhZ7P2xNdBF2Fi7StXUKruVggpMNfJDRaNh5OG_G1vmxRWtZ-4SPLSx6500Dpddw4wbpD7dHV3XBaXMFzqxsorn-mZfg4_lps1ii1dvL62K-QooRPqAKY8MM5ZmuMMs0rYyiMylzniktiMiFyHNNpJ1aK7jiisyE4rqqqpxyyq1il-D2mNuH7nM0cSh33Rh8elnSlEJyQoVIFDlSKnQxBmPLPrhWhn1JcHkouPxTcPLQoycm1tcm_Cb_b_oGiU195g</recordid><startdate>20210801</startdate><enddate>20210801</enddate><creator>Chizhikov, A. P.</creator><creator>Konstantinov, A. S.</creator><creator>Bazhin, P. M.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20210801</creationdate><title>Self-Propagating High-Temperature Synthesis of Ceramic Material Based on Aluminum-Magnesium Spinel and Titanium Diboride</title><author>Chizhikov, A. P. ; Konstantinov, A. S. ; Bazhin, P. M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-b00e3e264db034d2bec29aa564cd81858855d1af7ff86c6c198c6dbbb52626fc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Aluminum</topic><topic>Boron oxides</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Combustion temperature</topic><topic>Composite materials</topic><topic>Composite structures</topic><topic>Crystallites</topic><topic>Inorganic Chemistry</topic><topic>Magnesium</topic><topic>Morphology</topic><topic>Particulate composites</topic><topic>Phase composition</topic><topic>Self propagating high temperature synthesis</topic><topic>Spinel</topic><topic>Synthesis and Properties of Inorganic Compounds</topic><topic>Titanium</topic><topic>Titanium diboride</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chizhikov, A. P.</creatorcontrib><creatorcontrib>Konstantinov, A. S.</creatorcontrib><creatorcontrib>Bazhin, P. M.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of inorganic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chizhikov, A. P.</au><au>Konstantinov, A. S.</au><au>Bazhin, P. M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Self-Propagating High-Temperature Synthesis of Ceramic Material Based on Aluminum-Magnesium Spinel and Titanium Diboride</atitle><jtitle>Russian journal of inorganic chemistry</jtitle><stitle>Russ. J. Inorg. Chem</stitle><date>2021-08-01</date><risdate>2021</risdate><volume>66</volume><issue>8</issue><spage>1115</spage><epage>1120</epage><pages>1115-1120</pages><issn>0036-0236</issn><eissn>1531-8613</eissn><abstract>―
The aim of this work is to synthesize ceramic composite materials based on aluminum-magnesium spinel strengthened by titanium diboride particles by the self-propagating high-temperature synthesis (SHS) and study the combustion characteristics of synthesized materials, their microstructure, and phase composition. For the synthesis of materials, powders of boron oxide, aluminum, magnesium, and titanium have been used. It is shown that changing the ratio of magnesium and aluminum in the composition of the initial charge results in changes in the phase composition of the synthesis products. As a result of the synthesis, composite materials based on aluminum-magnesium spinel with different contents of aluminum cations have been obtained: MgAl
3
O
4
, MgAl
2
O
4
, MgAlO
4
, and Mg
1.5
Ti
1.5
O
4
. It is shown that with an increase in the combustion temperature of the studied compositions, the morphology of the particles of the powders obtained with composite structures changes. It is shown that after SHS, crystallites of aluminum-magnesium spinel with a size of about 50 nm are formed.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S0036023621080039</doi><tpages>6</tpages></addata></record> |
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| language | eng |
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| subjects | Aluminum Boron oxides Chemistry Chemistry and Materials Science Combustion temperature Composite materials Composite structures Crystallites Inorganic Chemistry Magnesium Morphology Particulate composites Phase composition Self propagating high temperature synthesis Spinel Synthesis and Properties of Inorganic Compounds Titanium Titanium diboride |
| title | Self-Propagating High-Temperature Synthesis of Ceramic Material Based on Aluminum-Magnesium Spinel and Titanium Diboride |
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