Spark Plasma Sintering, Phase Composition, and Properties of AlMgB14 Ceramic Materials
AlMgB 14 -based materials have been synthesized by spark plasma sintering of an Al 12 Mg 17 –B powder mixture at 1300 and 1400°C. The phase composition, structure, and properties of these materials have been studied. According to X-ray powder diffraction evidence, spark plasma sintering leads to the...
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creator | Nikitin, P. Yu Zhukov, I. A. Boldin, M. S. Perevislov, S. N. Chuvil’deev, V. N. |
description | AlMgB
14
-based materials have been synthesized by spark plasma sintering of an Al
12
Mg
17
–B powder mixture at 1300 and 1400°C. The phase composition, structure, and properties of these materials have been studied. According to X-ray powder diffraction evidence, spark plasma sintering leads to the formation of the AlMgB
14
phase and the MgAl
2
O
4
spinel. The content of the AlMgB
14
phase in the materials is ~95 wt %. At a sintering temperature of 1400°C, the resulting material has a hardness and relative density of 30.1 GPa and 99.3%, respectively. It has been demonstrated that a major source of oxygen in the powder mixture is a B
2
O
3
oxide film on the boron powder surface. Thus, when the Al
12
Mg
17
intermetallic powder is used as a precursor, the reaction of Al
x
Mg
y
intermetallic compounds with B
2
O
3
leads to the formation of the MgAl
2
O
4
spinel. |
doi_str_mv | 10.1134/S0036023621080167 |
format | Article |
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14
-based materials have been synthesized by spark plasma sintering of an Al
12
Mg
17
–B powder mixture at 1300 and 1400°C. The phase composition, structure, and properties of these materials have been studied. According to X-ray powder diffraction evidence, spark plasma sintering leads to the formation of the AlMgB
14
phase and the MgAl
2
O
4
spinel. The content of the AlMgB
14
phase in the materials is ~95 wt %. At a sintering temperature of 1400°C, the resulting material has a hardness and relative density of 30.1 GPa and 99.3%, respectively. It has been demonstrated that a major source of oxygen in the powder mixture is a B
2
O
3
oxide film on the boron powder surface. Thus, when the Al
12
Mg
17
intermetallic powder is used as a precursor, the reaction of Al
x
Mg
y
intermetallic compounds with B
2
O
3
leads to the formation of the MgAl
2
O
4
spinel.</description><identifier>ISSN: 0036-0236</identifier><identifier>EISSN: 1531-8613</identifier><identifier>DOI: 10.1134/S0036023621080167</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Boron oxides ; Chemistry ; Chemistry and Materials Science ; Inorganic Chemistry ; Inorganic Materials and Nanomaterials ; Intermetallic compounds ; Oxide coatings ; Phase composition ; Plasma sintering ; Sintering (powder metallurgy) ; Spark plasma sintering ; Spinel ; X ray powder diffraction</subject><ispartof>Russian journal of inorganic chemistry, 2021-08, Vol.66 (8), p.1252-1256</ispartof><rights>Pleiades Publishing, Ltd. 2021. ISSN 0036-0236, Russian Journal of Inorganic Chemistry, 2021, Vol. 66, No. 8, pp. 1252–1256. © Pleiades Publishing, Ltd., 2021. Russian Text © The Author(s), 2021, published in Zhurnal Neorganicheskoi Khimii, 2021, Vol. 66, No. 8, pp. 1150–1155.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-90241c7dffdc3a0e4118899b0889251eb2c00e8e9012b28f2c5afca2ff146ca73</citedby><cites>FETCH-LOGICAL-c316t-90241c7dffdc3a0e4118899b0889251eb2c00e8e9012b28f2c5afca2ff146ca73</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0036023621080167$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0036023621080167$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,777,781,27905,27906,41469,42538,51300</link.rule.ids></links><search><creatorcontrib>Nikitin, P. Yu</creatorcontrib><creatorcontrib>Zhukov, I. A.</creatorcontrib><creatorcontrib>Boldin, M. S.</creatorcontrib><creatorcontrib>Perevislov, S. N.</creatorcontrib><creatorcontrib>Chuvil’deev, V. N.</creatorcontrib><title>Spark Plasma Sintering, Phase Composition, and Properties of AlMgB14 Ceramic Materials</title><title>Russian journal of inorganic chemistry</title><addtitle>Russ. J. Inorg. Chem</addtitle><description>AlMgB
14
-based materials have been synthesized by spark plasma sintering of an Al
12
Mg
17
–B powder mixture at 1300 and 1400°C. The phase composition, structure, and properties of these materials have been studied. According to X-ray powder diffraction evidence, spark plasma sintering leads to the formation of the AlMgB
14
phase and the MgAl
2
O
4
spinel. The content of the AlMgB
14
phase in the materials is ~95 wt %. At a sintering temperature of 1400°C, the resulting material has a hardness and relative density of 30.1 GPa and 99.3%, respectively. It has been demonstrated that a major source of oxygen in the powder mixture is a B
2
O
3
oxide film on the boron powder surface. Thus, when the Al
12
Mg
17
intermetallic powder is used as a precursor, the reaction of Al
x
Mg
y
intermetallic compounds with B
2
O
3
leads to the formation of the MgAl
2
O
4
spinel.</description><subject>Boron oxides</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Inorganic Chemistry</subject><subject>Inorganic Materials and Nanomaterials</subject><subject>Intermetallic compounds</subject><subject>Oxide coatings</subject><subject>Phase composition</subject><subject>Plasma sintering</subject><subject>Sintering (powder metallurgy)</subject><subject>Spark plasma sintering</subject><subject>Spinel</subject><subject>X ray powder diffraction</subject><issn>0036-0236</issn><issn>1531-8613</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kM1OwzAQhC0EEqXwANwscW1g13YS51gi_qRWVCpwjVzXLi5NHOz0wNuTqEgcEJedw8w3Kw0hlwjXiFzcLAF4BoxnDEECZvkRGWHKMZEZ8mMyGuxk8E_JWYxbACEglyPytmxV-KCLnYq1okvXdCa4ZjOhi3cVDS193froOuebCVXNmi6Cb03onInUWzrdzTe3KGhpgqqdpnM14GoXz8mJ7cVc_OiYvN7fvZSPyez54amczhLNMeuSAphAna-tXWuuwAhEKYtiBf1lKZoV0wBGmgKQrZi0TKfKasWsRZFplfMxuTr0tsF_7k3sqq3fh6Z_WbE0E5hCzoo-hYeUDj7GYGzVBler8FUhVMN81Z_5eoYdmNgOg5jw2_w_9A0jdm_M</recordid><startdate>20210801</startdate><enddate>20210801</enddate><creator>Nikitin, P. Yu</creator><creator>Zhukov, I. A.</creator><creator>Boldin, M. S.</creator><creator>Perevislov, S. N.</creator><creator>Chuvil’deev, V. N.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20210801</creationdate><title>Spark Plasma Sintering, Phase Composition, and Properties of AlMgB14 Ceramic Materials</title><author>Nikitin, P. Yu ; Zhukov, I. A. ; Boldin, M. S. ; Perevislov, S. N. ; Chuvil’deev, V. N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-90241c7dffdc3a0e4118899b0889251eb2c00e8e9012b28f2c5afca2ff146ca73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Boron oxides</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Inorganic Chemistry</topic><topic>Inorganic Materials and Nanomaterials</topic><topic>Intermetallic compounds</topic><topic>Oxide coatings</topic><topic>Phase composition</topic><topic>Plasma sintering</topic><topic>Sintering (powder metallurgy)</topic><topic>Spark plasma sintering</topic><topic>Spinel</topic><topic>X ray powder diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nikitin, P. Yu</creatorcontrib><creatorcontrib>Zhukov, I. A.</creatorcontrib><creatorcontrib>Boldin, M. S.</creatorcontrib><creatorcontrib>Perevislov, S. N.</creatorcontrib><creatorcontrib>Chuvil’deev, V. N.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of inorganic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nikitin, P. Yu</au><au>Zhukov, I. A.</au><au>Boldin, M. S.</au><au>Perevislov, S. N.</au><au>Chuvil’deev, V. N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Spark Plasma Sintering, Phase Composition, and Properties of AlMgB14 Ceramic Materials</atitle><jtitle>Russian journal of inorganic chemistry</jtitle><stitle>Russ. J. Inorg. Chem</stitle><date>2021-08-01</date><risdate>2021</risdate><volume>66</volume><issue>8</issue><spage>1252</spage><epage>1256</epage><pages>1252-1256</pages><issn>0036-0236</issn><eissn>1531-8613</eissn><abstract>AlMgB
14
-based materials have been synthesized by spark plasma sintering of an Al
12
Mg
17
–B powder mixture at 1300 and 1400°C. The phase composition, structure, and properties of these materials have been studied. According to X-ray powder diffraction evidence, spark plasma sintering leads to the formation of the AlMgB
14
phase and the MgAl
2
O
4
spinel. The content of the AlMgB
14
phase in the materials is ~95 wt %. At a sintering temperature of 1400°C, the resulting material has a hardness and relative density of 30.1 GPa and 99.3%, respectively. It has been demonstrated that a major source of oxygen in the powder mixture is a B
2
O
3
oxide film on the boron powder surface. Thus, when the Al
12
Mg
17
intermetallic powder is used as a precursor, the reaction of Al
x
Mg
y
intermetallic compounds with B
2
O
3
leads to the formation of the MgAl
2
O
4
spinel.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S0036023621080167</doi><tpages>5</tpages></addata></record> |
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subjects | Boron oxides Chemistry Chemistry and Materials Science Inorganic Chemistry Inorganic Materials and Nanomaterials Intermetallic compounds Oxide coatings Phase composition Plasma sintering Sintering (powder metallurgy) Spark plasma sintering Spinel X ray powder diffraction |
title | Spark Plasma Sintering, Phase Composition, and Properties of AlMgB14 Ceramic Materials |
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