Facile One-pot Synthesis of Hollow-structured CuS/Cu2S Hybrid for Enhanced Electrochemical Determination of Glucose
A novel non-enzymatic glucose sensor based on hollow-structured copper sulfide/cuprous sulfide (CuS/Cu2S) hybrid was developed by using a facile and one-pot solvothermal method. The crystal structure, morphology and surface property of the prepared CuS/Cu2S hybrid were characterized by X-ray diffrac...
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| Veröffentlicht in: | Denki kagaku oyobi kōgyō butsuri kagaku 2021/07/05, Vol.89(4), pp.340-347 |
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| container_title | Denki kagaku oyobi kōgyō butsuri kagaku |
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| creator | HUANG, Wei LIU, Fengping HUANG, Yingying YANG, Wei ZHONG, Huifang PENG, Jinyun |
| description | A novel non-enzymatic glucose sensor based on hollow-structured copper sulfide/cuprous sulfide (CuS/Cu2S) hybrid was developed by using a facile and one-pot solvothermal method. The crystal structure, morphology and surface property of the prepared CuS/Cu2S hybrid were characterized by X-ray diffraction spectroscopy, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. The electrochemical performances of this hybrid modified glassy carbon electrode for glucose oxidation were monitored by cyclic voltammograms and amperometric technology. Results showed that the novel integrated electrode exhibited excellent electrocatalytic performances to the oxidation of glucose with a wide line range of 3.0–1100.0 µM, high sensitivity of 321.3 µA mM−1 cm−2, low detection limit of 1.1 µM (3δ/S), fast response, good anti-interference ability and excellent stability. The proposed sensor was successfully applied for the determination of glucose in human blood serum sample with satisfactory recoveries. |
| doi_str_mv | 10.5796/electrochemistry.21-00027 |
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The crystal structure, morphology and surface property of the prepared CuS/Cu2S hybrid were characterized by X-ray diffraction spectroscopy, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. The electrochemical performances of this hybrid modified glassy carbon electrode for glucose oxidation were monitored by cyclic voltammograms and amperometric technology. Results showed that the novel integrated electrode exhibited excellent electrocatalytic performances to the oxidation of glucose with a wide line range of 3.0–1100.0 µM, high sensitivity of 321.3 µA mM−1 cm−2, low detection limit of 1.1 µM (3δ/S), fast response, good anti-interference ability and excellent stability. The proposed sensor was successfully applied for the determination of glucose in human blood serum sample with satisfactory recoveries.</description><identifier>ISSN: 1344-3542</identifier><identifier>EISSN: 2186-2451</identifier><identifier>DOI: 10.5796/electrochemistry.21-00027</identifier><language>eng</language><publisher>Tokyo: The Electrochemical Society of Japan</publisher><subject>Copper sulfides ; Crystal structure ; Electrical measurement ; Electrocatalytic ; Electrodes ; Electron microscopy ; Electrons ; Glassy carbon ; Glucose ; Hollow-structured Copper Sulfide/Cuprous Sulfide Hybrid ; Microscopy ; Morphology ; Non-enzymatic Glucose Sensor ; Oxidation ; Photoelectron spectroscopy ; Photoelectrons ; Scanning electron microscopy ; Solvothermal Method ; Spectrum analysis ; Surface properties ; Transmission electron microscopy ; X-ray diffraction ; X-ray spectroscopy</subject><ispartof>Electrochemistry, 2021/07/05, Vol.89(4), pp.340-347</ispartof><rights>The Author(s) 2021. Published by ECSJ.</rights><rights>2021. This work is published under http://creativecommons.org/licenses/by-nc-sa/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c550t-fd0599593e0d3c7531a4d9e60a7c5eb7d3382e928b7011b2df16530da2c5da373</citedby><cites>FETCH-LOGICAL-c550t-fd0599593e0d3c7531a4d9e60a7c5eb7d3382e928b7011b2df16530da2c5da373</cites><orcidid>0000-0002-0688-4412</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,864,1883,27924,27925</link.rule.ids></links><search><creatorcontrib>HUANG, Wei</creatorcontrib><creatorcontrib>LIU, Fengping</creatorcontrib><creatorcontrib>HUANG, Yingying</creatorcontrib><creatorcontrib>YANG, Wei</creatorcontrib><creatorcontrib>ZHONG, Huifang</creatorcontrib><creatorcontrib>PENG, Jinyun</creatorcontrib><title>Facile One-pot Synthesis of Hollow-structured CuS/Cu2S Hybrid for Enhanced Electrochemical Determination of Glucose</title><title>Denki kagaku oyobi kōgyō butsuri kagaku</title><addtitle>Electrochemistry</addtitle><description>A novel non-enzymatic glucose sensor based on hollow-structured copper sulfide/cuprous sulfide (CuS/Cu2S) hybrid was developed by using a facile and one-pot solvothermal method. The crystal structure, morphology and surface property of the prepared CuS/Cu2S hybrid were characterized by X-ray diffraction spectroscopy, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. The electrochemical performances of this hybrid modified glassy carbon electrode for glucose oxidation were monitored by cyclic voltammograms and amperometric technology. Results showed that the novel integrated electrode exhibited excellent electrocatalytic performances to the oxidation of glucose with a wide line range of 3.0–1100.0 µM, high sensitivity of 321.3 µA mM−1 cm−2, low detection limit of 1.1 µM (3δ/S), fast response, good anti-interference ability and excellent stability. The proposed sensor was successfully applied for the determination of glucose in human blood serum sample with satisfactory recoveries.</description><subject>Copper sulfides</subject><subject>Crystal structure</subject><subject>Electrical measurement</subject><subject>Electrocatalytic</subject><subject>Electrodes</subject><subject>Electron microscopy</subject><subject>Electrons</subject><subject>Glassy carbon</subject><subject>Glucose</subject><subject>Hollow-structured Copper Sulfide/Cuprous Sulfide Hybrid</subject><subject>Microscopy</subject><subject>Morphology</subject><subject>Non-enzymatic Glucose Sensor</subject><subject>Oxidation</subject><subject>Photoelectron spectroscopy</subject><subject>Photoelectrons</subject><subject>Scanning electron microscopy</subject><subject>Solvothermal Method</subject><subject>Spectrum analysis</subject><subject>Surface properties</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><subject>X-ray spectroscopy</subject><issn>1344-3542</issn><issn>2186-2451</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNplkc1qGzEUhUVpoSbNO6h0PYl-R6NlcZ04EPDC7VpopKtYZjxyJQ3Fb99x3JjSanEFuud8OnAQ-kzJnVS6vYcBXM3J7eAQS82nO0YbQghT79CC0a5tmJD0PVpQLkTDpWAf0W0p-1lCiW410wtUHqyLA-DNCM0xVbw9jXUHJRacAl6nYUi_mhk9uTpl8Hg5be-XE9vi9anP0eOQMl6NOzu6ebn6K46zA_4GFfIhjrbGNJ55j8PkUoFP6EOwQ4HbP_cN-vGw-r5cN8-bx6fl1-fGSUlqEzyRWkvNgXjulOTUCq-hJVY5Cb3ynHcMNOt6RSjtmQ-0lZx4y5z0lit-g54uXJ_s3hxzPNh8MslG8_qQ8ouxuUY3gAlMdGo-nXdUkNb10moftAXR90rbMLO-XFjHnH5OUKrZpymPc3zDpFSsVa0is0pfVC6nUjKE66-UmHNl5t_KDKPmtbLZu7l496XaF7g63yL-5-y0EefxRrgq3c5mAyP_DUkMrZM</recordid><startdate>20210705</startdate><enddate>20210705</enddate><creator>HUANG, Wei</creator><creator>LIU, Fengping</creator><creator>HUANG, Yingying</creator><creator>YANG, Wei</creator><creator>ZHONG, Huifang</creator><creator>PENG, Jinyun</creator><general>The Electrochemical Society of Japan</general><general>Japan Science and Technology Agency</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QL</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>C1K</scope><scope>F28</scope><scope>FR3</scope><scope>H8D</scope><scope>H8G</scope><scope>JG9</scope><scope>JQ2</scope><scope>KR7</scope><scope>L7M</scope><scope>L~C</scope><scope>L~D</scope><scope>P64</scope><scope>DOA</scope><orcidid>https://orcid.org/0000-0002-0688-4412</orcidid></search><sort><creationdate>20210705</creationdate><title>Facile One-pot Synthesis of Hollow-structured CuS/Cu2S Hybrid for Enhanced Electrochemical Determination of Glucose</title><author>HUANG, Wei ; LIU, Fengping ; HUANG, Yingying ; YANG, Wei ; ZHONG, Huifang ; PENG, Jinyun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c550t-fd0599593e0d3c7531a4d9e60a7c5eb7d3382e928b7011b2df16530da2c5da373</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Copper sulfides</topic><topic>Crystal structure</topic><topic>Electrical measurement</topic><topic>Electrocatalytic</topic><topic>Electrodes</topic><topic>Electron microscopy</topic><topic>Electrons</topic><topic>Glassy carbon</topic><topic>Glucose</topic><topic>Hollow-structured Copper Sulfide/Cuprous Sulfide Hybrid</topic><topic>Microscopy</topic><topic>Morphology</topic><topic>Non-enzymatic Glucose Sensor</topic><topic>Oxidation</topic><topic>Photoelectron spectroscopy</topic><topic>Photoelectrons</topic><topic>Scanning electron microscopy</topic><topic>Solvothermal Method</topic><topic>Spectrum analysis</topic><topic>Surface properties</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><topic>X-ray spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>HUANG, Wei</creatorcontrib><creatorcontrib>LIU, Fengping</creatorcontrib><creatorcontrib>HUANG, Yingying</creatorcontrib><creatorcontrib>YANG, Wei</creatorcontrib><creatorcontrib>ZHONG, Huifang</creatorcontrib><creatorcontrib>PENG, Jinyun</creatorcontrib><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Bacteriology Abstracts (Microbiology B)</collection><collection>Biotechnology Research Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Computer and Information Systems Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Materials Business File</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Aerospace Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>ProQuest Computer Science Collection</collection><collection>Civil Engineering Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Computer and Information Systems Abstracts Academic</collection><collection>Computer and Information Systems Abstracts Professional</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Denki kagaku oyobi kōgyō butsuri kagaku</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>HUANG, Wei</au><au>LIU, Fengping</au><au>HUANG, Yingying</au><au>YANG, Wei</au><au>ZHONG, Huifang</au><au>PENG, Jinyun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Facile One-pot Synthesis of Hollow-structured CuS/Cu2S Hybrid for Enhanced Electrochemical Determination of Glucose</atitle><jtitle>Denki kagaku oyobi kōgyō butsuri kagaku</jtitle><addtitle>Electrochemistry</addtitle><date>2021-07-05</date><risdate>2021</risdate><volume>89</volume><issue>4</issue><spage>340</spage><epage>347</epage><pages>340-347</pages><artnum>21-00027</artnum><issn>1344-3542</issn><eissn>2186-2451</eissn><abstract>A novel non-enzymatic glucose sensor based on hollow-structured copper sulfide/cuprous sulfide (CuS/Cu2S) hybrid was developed by using a facile and one-pot solvothermal method. The crystal structure, morphology and surface property of the prepared CuS/Cu2S hybrid were characterized by X-ray diffraction spectroscopy, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. The electrochemical performances of this hybrid modified glassy carbon electrode for glucose oxidation were monitored by cyclic voltammograms and amperometric technology. Results showed that the novel integrated electrode exhibited excellent electrocatalytic performances to the oxidation of glucose with a wide line range of 3.0–1100.0 µM, high sensitivity of 321.3 µA mM−1 cm−2, low detection limit of 1.1 µM (3δ/S), fast response, good anti-interference ability and excellent stability. 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| subjects | Copper sulfides Crystal structure Electrical measurement Electrocatalytic Electrodes Electron microscopy Electrons Glassy carbon Glucose Hollow-structured Copper Sulfide/Cuprous Sulfide Hybrid Microscopy Morphology Non-enzymatic Glucose Sensor Oxidation Photoelectron spectroscopy Photoelectrons Scanning electron microscopy Solvothermal Method Spectrum analysis Surface properties Transmission electron microscopy X-ray diffraction X-ray spectroscopy |
| title | Facile One-pot Synthesis of Hollow-structured CuS/Cu2S Hybrid for Enhanced Electrochemical Determination of Glucose |
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