Synthesis, Characterization of New Polytriazole Derivatives from Polyacryloyl chloride and Theoretical with Corrosion Inhibitor Study for Stainless steel in acidic medium
The purpose of the study is to synthesize and characterize a new polytriazole derivative from polyacryloyl chloried, first reaction of polyacryloyl chloride with hydrazine hydrate in the presence of DMF as a solvent to obtained acid hydrazide (1) than reacted with different amide to give poly 1,2,4-...
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| Veröffentlicht in: | Research journal of pharmacy and technology 2021-07, Vol.14 (7), p.3721-3726 |
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| container_title | Research journal of pharmacy and technology |
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| creator | Sadiq, Amaal S. Al-Tamimi, Entesar O. |
| description | The purpose of the study is to synthesize and characterize a new polytriazole derivative from polyacryloyl chloried, first reaction of polyacryloyl chloride with hydrazine hydrate in the presence of DMF as a solvent to obtained acid hydrazide (1) than reacted with different amide to give poly 1,2,4-triazole derivatives(1a-1c). Newly synthesized compounds were characterized by spectral methods [13C-NMR, 1H-NMR, and FTIR] and calculated some of its physical properties. Also, we worked theoretical study involving calculated the geometric configurations, total energy, dipole moment etc..,. In addition, the inhibition effect of the synthesized compounds (1a-1c) on corrosion of stainless steel in 1M HCl were studied by method of weight loss. The results of weight loss measurements showed that corrosion inhibition efficiency by increasing the concentration of organic inhibitors for stainless steel in 1M HCl solution at 30oC. |
| doi_str_mv | 10.52711/0974-360X.2021.00644 |
| format | Article |
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Newly synthesized compounds were characterized by spectral methods [13C-NMR, 1H-NMR, and FTIR] and calculated some of its physical properties. Also, we worked theoretical study involving calculated the geometric configurations, total energy, dipole moment etc..,. In addition, the inhibition effect of the synthesized compounds (1a-1c) on corrosion of stainless steel in 1M HCl were studied by method of weight loss. The results of weight loss measurements showed that corrosion inhibition efficiency by increasing the concentration of organic inhibitors for stainless steel in 1M HCl solution at 30oC.</description><identifier>ISSN: 0974-3618</identifier><identifier>EISSN: 0974-360X</identifier><identifier>EISSN: 0974-306X</identifier><identifier>DOI: 10.52711/0974-360X.2021.00644</identifier><language>eng</language><publisher>Raipur: A&V Publications</publisher><subject>Adsorption ; Corrosion ; Corrosion inhibitors ; Efficiency ; Physical properties ; Polymers ; Stainless steel</subject><ispartof>Research journal of pharmacy and technology, 2021-07, Vol.14 (7), p.3721-3726</ispartof><rights>Copyright A&V Publications Jul 2021</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c144t-8120b55867b9f90a13f56b5eb75af5a6db084f96beee2641f2353e7e04a97dac3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Sadiq, Amaal S.</creatorcontrib><creatorcontrib>Al-Tamimi, Entesar O.</creatorcontrib><title>Synthesis, Characterization of New Polytriazole Derivatives from Polyacryloyl chloride and Theoretical with Corrosion Inhibitor Study for Stainless steel in acidic medium</title><title>Research journal of pharmacy and technology</title><description>The purpose of the study is to synthesize and characterize a new polytriazole derivative from polyacryloyl chloried, first reaction of polyacryloyl chloride with hydrazine hydrate in the presence of DMF as a solvent to obtained acid hydrazide (1) than reacted with different amide to give poly 1,2,4-triazole derivatives(1a-1c). Newly synthesized compounds were characterized by spectral methods [13C-NMR, 1H-NMR, and FTIR] and calculated some of its physical properties. Also, we worked theoretical study involving calculated the geometric configurations, total energy, dipole moment etc..,. In addition, the inhibition effect of the synthesized compounds (1a-1c) on corrosion of stainless steel in 1M HCl were studied by method of weight loss. The results of weight loss measurements showed that corrosion inhibition efficiency by increasing the concentration of organic inhibitors for stainless steel in 1M HCl solution at 30oC.</description><subject>Adsorption</subject><subject>Corrosion</subject><subject>Corrosion inhibitors</subject><subject>Efficiency</subject><subject>Physical properties</subject><subject>Polymers</subject><subject>Stainless steel</subject><issn>0974-3618</issn><issn>0974-360X</issn><issn>0974-306X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><recordid>eNo9UV1LxDAQLKKgqD9BWPDVO5M0SdtHOT9BVFDBt5CmGxrJNZrklPqT_JX2TnFfdtgZZtmdojiiZC5YRekpaSo-KyV5mTPC6JwQyflWsfc_3v7HtN4tDlN6JVPJWjBe7xXfj-OQe0wuncCi11GbjNF96ezCAMHCHX7CQ_Bjjk5_BY9wPtEfE_2BCWwMyw2rTRx9GD2Y3ofoOgQ9dPDUY4iYndEePl3uYRFiDGntfDP0rnU5RHjMq24Eu0HaDR5TgpQRPbgBtHGdM7DEzq2WB8WO1T7h4V_fL54vL54W17Pb-6ubxdntzFDO86ymjLRC1LJqG9sQTUsrZCuwrYS2QsuuJTW3jWwRkUlOLStFiRUSrpuq06bcL45_fd9ieF9hyuo1rOIwrVRMCEnKppRsUolflZlOShGteotuqeOoKFGbZNT67WodgVonozbJlD9ucYXH</recordid><startdate>20210701</startdate><enddate>20210701</enddate><creator>Sadiq, Amaal S.</creator><creator>Al-Tamimi, Entesar O.</creator><general>A&V Publications</general><scope>AAYXX</scope><scope>CITATION</scope><scope>04Q</scope><scope>04S</scope><scope>04W</scope><scope>3V.</scope><scope>7X7</scope><scope>7XB</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>CCPQU</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>K9.</scope><scope>M0S</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope></search><sort><creationdate>20210701</creationdate><title>Synthesis, Characterization of New Polytriazole Derivatives from Polyacryloyl chloride and Theoretical with Corrosion Inhibitor Study for Stainless steel in acidic medium</title><author>Sadiq, Amaal S. ; 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| ispartof | Research journal of pharmacy and technology, 2021-07, Vol.14 (7), p.3721-3726 |
| issn | 0974-3618 0974-360X 0974-306X |
| language | eng |
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| source | EZB-FREE-00999 freely available EZB journals |
| subjects | Adsorption Corrosion Corrosion inhibitors Efficiency Physical properties Polymers Stainless steel |
| title | Synthesis, Characterization of New Polytriazole Derivatives from Polyacryloyl chloride and Theoretical with Corrosion Inhibitor Study for Stainless steel in acidic medium |
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