Ceramification of Composites of MgO-Al3O3-SiO2/Boron Phenolic Resin with Different Calcine Time
The ceramifiable polymer composite of MgO-Al 2 O 3 -SiO 2 /boron phenolic resin(MAS/BPF) with 40wt% of inorganic fillers was calcined at 1 200 °C for different time to promote ceramification of ceramifiable composite and improve heat resistance. The effects of different calcine time on the macroscop...
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| Veröffentlicht in: | Journal of Wuhan University of Technology. Materials science edition 2021-04, Vol.36 (2), p.174-182 |
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| container_issue | 2 |
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| container_title | Journal of Wuhan University of Technology. Materials science edition |
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| creator | Shi, Minxian Tang, Qingxiu Fan, Shanshan Dong, Chuang Huang, Zhixiong |
| description | The ceramifiable polymer composite of MgO-Al
2
O
3
-SiO
2
/boron phenolic resin(MAS/BPF) with 40wt% of inorganic fillers was calcined at 1 200 °C for different time to promote ceramification of ceramifiable composite and improve heat resistance. The effects of different calcine time on the macroscopical morphology, mass loss, phase evolution, microstructure and chemical bond evolution of MAS/BPF composites were characterized by XRD, XPS, and SEM analyses. The experimental results reveal that the increase of calcine time result in the fewer holes, relatively denser and smoother top layer of MAS/BPF composites and protect the interior from deeper decomposition. The final residues of composites are amorphous carbon and C-O-Si-Al-Mg ceramic. And MAS/BPF composites show excellent mass stability, low shrinkage and self-supporting features after 2 h holding compared with BPF composites without 40wt% of inorganic fillers. |
| doi_str_mv | 10.1007/s11595-021-2391-0 |
| format | Article |
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2
O
3
-SiO
2
/boron phenolic resin(MAS/BPF) with 40wt% of inorganic fillers was calcined at 1 200 °C for different time to promote ceramification of ceramifiable composite and improve heat resistance. The effects of different calcine time on the macroscopical morphology, mass loss, phase evolution, microstructure and chemical bond evolution of MAS/BPF composites were characterized by XRD, XPS, and SEM analyses. The experimental results reveal that the increase of calcine time result in the fewer holes, relatively denser and smoother top layer of MAS/BPF composites and protect the interior from deeper decomposition. The final residues of composites are amorphous carbon and C-O-Si-Al-Mg ceramic. And MAS/BPF composites show excellent mass stability, low shrinkage and self-supporting features after 2 h holding compared with BPF composites without 40wt% of inorganic fillers.</description><identifier>ISSN: 1000-2413</identifier><identifier>EISSN: 1993-0437</identifier><identifier>DOI: 10.1007/s11595-021-2391-0</identifier><language>eng</language><publisher>Wuhan: Wuhan University of Technology</publisher><subject>Advanced Materials ; Aluminum oxide ; Boron ; Chemical bonds ; Chemistry and Materials Science ; Evolution ; Fillers ; Heat resistance ; Magnesium oxide ; Materials Science ; Morphology ; Phenolic resins ; Polymer matrix composites ; Silicon dioxide ; Thermal resistance ; X ray photoelectron spectroscopy</subject><ispartof>Journal of Wuhan University of Technology. Materials science edition, 2021-04, Vol.36 (2), p.174-182</ispartof><rights>Wuhan University of Technology and Springer-Verlag GmbH Germany, Part of Springer Nature 2021</rights><rights>Wuhan University of Technology and Springer-Verlag GmbH Germany, Part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-e542c2f87e8cfadefb32015fce38a63ebb031b5235b6ec23c76fa3a6b1f4bb3</citedby><cites>FETCH-LOGICAL-c316t-e542c2f87e8cfadefb32015fce38a63ebb031b5235b6ec23c76fa3a6b1f4bb3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11595-021-2391-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11595-021-2391-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Shi, Minxian</creatorcontrib><creatorcontrib>Tang, Qingxiu</creatorcontrib><creatorcontrib>Fan, Shanshan</creatorcontrib><creatorcontrib>Dong, Chuang</creatorcontrib><creatorcontrib>Huang, Zhixiong</creatorcontrib><title>Ceramification of Composites of MgO-Al3O3-SiO2/Boron Phenolic Resin with Different Calcine Time</title><title>Journal of Wuhan University of Technology. Materials science edition</title><addtitle>J. Wuhan Univ. Technol.-Mat. Sci. Edit</addtitle><description>The ceramifiable polymer composite of MgO-Al
2
O
3
-SiO
2
/boron phenolic resin(MAS/BPF) with 40wt% of inorganic fillers was calcined at 1 200 °C for different time to promote ceramification of ceramifiable composite and improve heat resistance. The effects of different calcine time on the macroscopical morphology, mass loss, phase evolution, microstructure and chemical bond evolution of MAS/BPF composites were characterized by XRD, XPS, and SEM analyses. The experimental results reveal that the increase of calcine time result in the fewer holes, relatively denser and smoother top layer of MAS/BPF composites and protect the interior from deeper decomposition. The final residues of composites are amorphous carbon and C-O-Si-Al-Mg ceramic. And MAS/BPF composites show excellent mass stability, low shrinkage and self-supporting features after 2 h holding compared with BPF composites without 40wt% of inorganic fillers.</description><subject>Advanced Materials</subject><subject>Aluminum oxide</subject><subject>Boron</subject><subject>Chemical bonds</subject><subject>Chemistry and Materials Science</subject><subject>Evolution</subject><subject>Fillers</subject><subject>Heat resistance</subject><subject>Magnesium oxide</subject><subject>Materials Science</subject><subject>Morphology</subject><subject>Phenolic resins</subject><subject>Polymer matrix composites</subject><subject>Silicon dioxide</subject><subject>Thermal resistance</subject><subject>X ray photoelectron spectroscopy</subject><issn>1000-2413</issn><issn>1993-0437</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kF1LwzAUhoMoOKc_wLuC13H5aNL2ctZPmFTc7kMST7aMtplJh_jv7ZjglVfnHHje98CD0DUlt5SQYpYoFZXAhFHMeEUxOUETWlUck5wXp-NOCMEsp_wcXaS0JSQnXMoJUjVE3XnnrR586LPgsjp0u5D8AOlwva4bPG95w_HSN2x2F-JIvW2gD6232Tsk32dffthk9945iNAPWa1b63vIVr6DS3TmdJvg6ndO0fLxYVU_40Xz9FLPF9hyKgcMImeWubKA0jr9Ac5wRqhwFnipJQdjCKdGMC6MBMu4LaTTXEtDXW4Mn6KbY-suhs89pEFtwz7240PFhMiLMheFHCl6pGwMKUVwahd9p-O3okQdLKqjRTVaVAeLiowZdsykke3XEP-a_w_9AJL8dIw</recordid><startdate>20210401</startdate><enddate>20210401</enddate><creator>Shi, Minxian</creator><creator>Tang, Qingxiu</creator><creator>Fan, Shanshan</creator><creator>Dong, Chuang</creator><creator>Huang, Zhixiong</creator><general>Wuhan University of Technology</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20210401</creationdate><title>Ceramification of Composites of MgO-Al3O3-SiO2/Boron Phenolic Resin with Different Calcine Time</title><author>Shi, Minxian ; Tang, Qingxiu ; Fan, Shanshan ; Dong, Chuang ; Huang, Zhixiong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-e542c2f87e8cfadefb32015fce38a63ebb031b5235b6ec23c76fa3a6b1f4bb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Advanced Materials</topic><topic>Aluminum oxide</topic><topic>Boron</topic><topic>Chemical bonds</topic><topic>Chemistry and Materials Science</topic><topic>Evolution</topic><topic>Fillers</topic><topic>Heat resistance</topic><topic>Magnesium oxide</topic><topic>Materials Science</topic><topic>Morphology</topic><topic>Phenolic resins</topic><topic>Polymer matrix composites</topic><topic>Silicon dioxide</topic><topic>Thermal resistance</topic><topic>X ray photoelectron spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Shi, Minxian</creatorcontrib><creatorcontrib>Tang, Qingxiu</creatorcontrib><creatorcontrib>Fan, Shanshan</creatorcontrib><creatorcontrib>Dong, Chuang</creatorcontrib><creatorcontrib>Huang, Zhixiong</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of Wuhan University of Technology. Materials science edition</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Shi, Minxian</au><au>Tang, Qingxiu</au><au>Fan, Shanshan</au><au>Dong, Chuang</au><au>Huang, Zhixiong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ceramification of Composites of MgO-Al3O3-SiO2/Boron Phenolic Resin with Different Calcine Time</atitle><jtitle>Journal of Wuhan University of Technology. Materials science edition</jtitle><stitle>J. Wuhan Univ. Technol.-Mat. Sci. Edit</stitle><date>2021-04-01</date><risdate>2021</risdate><volume>36</volume><issue>2</issue><spage>174</spage><epage>182</epage><pages>174-182</pages><issn>1000-2413</issn><eissn>1993-0437</eissn><abstract>The ceramifiable polymer composite of MgO-Al
2
O
3
-SiO
2
/boron phenolic resin(MAS/BPF) with 40wt% of inorganic fillers was calcined at 1 200 °C for different time to promote ceramification of ceramifiable composite and improve heat resistance. The effects of different calcine time on the macroscopical morphology, mass loss, phase evolution, microstructure and chemical bond evolution of MAS/BPF composites were characterized by XRD, XPS, and SEM analyses. The experimental results reveal that the increase of calcine time result in the fewer holes, relatively denser and smoother top layer of MAS/BPF composites and protect the interior from deeper decomposition. The final residues of composites are amorphous carbon and C-O-Si-Al-Mg ceramic. And MAS/BPF composites show excellent mass stability, low shrinkage and self-supporting features after 2 h holding compared with BPF composites without 40wt% of inorganic fillers.</abstract><cop>Wuhan</cop><pub>Wuhan University of Technology</pub><doi>10.1007/s11595-021-2391-0</doi><tpages>9</tpages></addata></record> |
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| issn | 1000-2413 1993-0437 |
| language | eng |
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| source | Springer Online Journals Complete; Alma/SFX Local Collection |
| subjects | Advanced Materials Aluminum oxide Boron Chemical bonds Chemistry and Materials Science Evolution Fillers Heat resistance Magnesium oxide Materials Science Morphology Phenolic resins Polymer matrix composites Silicon dioxide Thermal resistance X ray photoelectron spectroscopy |
| title | Ceramification of Composites of MgO-Al3O3-SiO2/Boron Phenolic Resin with Different Calcine Time |
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