Effects of microwave-assisted reflux in wet-chemical synthesis of high sodium-ion conductive Na5DySi4O12

Sodium rare-earth silicate with Na5DySi4O12 components is known as a highly conductive and stable sodium ion solid electrolyte though are difficulties in obtaining a single-phase, highly conductive Na5DySi4O12 pellet because it has low conductivity impurity phases. In this study, microwave heating f...

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Veröffentlicht in:	Solid state ionics 2021-06, Vol.364, p.115607, Article 115607
Hauptverfasser:	Takase, Satoko, Nakashima, Kazuaki, Arima, Masato, Terada, Kouki, Shimizu, Youichi
Format:	Artikel
Sprache:	eng
Schlagworte:	Aqueous solutions Chemical synthesis Conductivity Crystal structure Crystallinity Electrolytes Heating Low conductivity Microwave-heating Microwaves Na5DySi4O12 Particle size distribution Pellets Precursors Rare earth elements Roasting Silica Sintering Sodium Sodium ion conductor Solid electrolytes Thermal analysis Wet chemical synthesis
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