Biochar Derived from Treated Lotus Stem and Adsorption of Phthalic Acid Esters
Phthalic acid ester (PAE), a plasticizer, is increasingly being detected in different environments. These compounds can gravely affect the human endocrine system. The present study aims to prepare adsorbents that can effectively adsorb PAE pollutants. To fabricate a better carbon structure than conv...
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| Veröffentlicht in: | Water, air, and soil pollution air, and soil pollution, 2021-06, Vol.232 (6), Article 224 |
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| container_title | Water, air, and soil pollution |
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| creator | Zhang, Ruiling Chen, Linlin Qiu, Binbin Sun, Xiaojing Qin, Songyan Wang, Bo Li, Feiyue Zhao, Lixin Zhu, Zhe |
| description | Phthalic acid ester (PAE), a plasticizer, is increasingly being detected in different environments. These compounds can gravely affect the human endocrine system. The present study aims to prepare adsorbents that can effectively adsorb PAE pollutants. To fabricate a better carbon structure than conventional biochar, the sodium hydroxide solution was used as a hydrolyzing agent to pretreat the biomass in order to weaken the bonds in lignin, cellulose, and hemicellulose. As a result, biochar with a special porous carbon structure is obtained. To study the characteristics of the biochar and its adsorption properties, dimethyl phthalate (DMP)—a PAE—was selected as the adsorbate. The morphology and structural composition of the biochar were examined via an environment scanning electron microscope with a field emission gun (SEM), surface area analyzer (BET), Fourier transform infrared spectrometer (FTIR), thermal gravimetry (TG/DTG), X-ray diffractometry (XRD), and Raman spectroscopy. The BET data of the biochar increased by 125.3 times than that of the original biochar. The layer spacing and the surface functional groups of the pretreated biochar also increased. After performing the micro-morphological regulation of biomass using sodium hydroxide, the adsorption performance of biochar with regard to PAE effectively improved and an adsorption capacity of 125 mg/g was observed for DMP. The adsorption kinetics and thermodynamic experiments showed that DMP adsorption by biochar follows the Langmuir and pseudo-second-order models. |
| doi_str_mv | 10.1007/s11270-021-05130-2 |
| format | Article |
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These compounds can gravely affect the human endocrine system. The present study aims to prepare adsorbents that can effectively adsorb PAE pollutants. To fabricate a better carbon structure than conventional biochar, the sodium hydroxide solution was used as a hydrolyzing agent to pretreat the biomass in order to weaken the bonds in lignin, cellulose, and hemicellulose. As a result, biochar with a special porous carbon structure is obtained. To study the characteristics of the biochar and its adsorption properties, dimethyl phthalate (DMP)—a PAE—was selected as the adsorbate. The morphology and structural composition of the biochar were examined via an environment scanning electron microscope with a field emission gun (SEM), surface area analyzer (BET), Fourier transform infrared spectrometer (FTIR), thermal gravimetry (TG/DTG), X-ray diffractometry (XRD), and Raman spectroscopy. The BET data of the biochar increased by 125.3 times than that of the original biochar. The layer spacing and the surface functional groups of the pretreated biochar also increased. After performing the micro-morphological regulation of biomass using sodium hydroxide, the adsorption performance of biochar with regard to PAE effectively improved and an adsorption capacity of 125 mg/g was observed for DMP. The adsorption kinetics and thermodynamic experiments showed that DMP adsorption by biochar follows the Langmuir and pseudo-second-order models.</description><identifier>ISSN: 0049-6979</identifier><identifier>EISSN: 1573-2932</identifier><identifier>DOI: 10.1007/s11270-021-05130-2</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Adsorbates ; Adsorption ; Analytical methods ; Atmospheric Protection/Air Quality Control/Air Pollution ; Biomass ; Bonding agents ; Bonding strength ; Carbon ; Caustic soda ; Cellulose ; Charcoal ; Climate Change/Climate Change Impacts ; Earth and Environmental Science ; Emission analysis ; Endocrine system ; Environment ; Environmental monitoring ; Esters ; Field emission microscopy ; Fourier transforms ; FTIR spectrometers ; Functional groups ; Gravimetric analysis ; Gravimetry ; Hemicellulose ; Hydrogeology ; Hydroxides ; Infrared analysis ; Infrared spectrometers ; Kinetics ; Lignin ; Morphology ; Phthalate esters ; Phthalates ; Phthalic acid ; Pollutants ; Raman spectroscopy ; Scanning electron microscopy ; Sodium ; Sodium hydroxide ; Soil Science & Conservation ; Surface chemistry ; Water Quality/Water Pollution</subject><ispartof>Water, air, and soil pollution, 2021-06, Vol.232 (6), Article 224</ispartof><rights>The Author(s), under exclusive licence to Springer Nature Switzerland AG 2021</rights><rights>COPYRIGHT 2021 Springer</rights><rights>The Author(s), under exclusive licence to Springer Nature Switzerland AG 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c358t-5aa0a9f8ca72fff86c37310e6ec60b3095a8f74313821ac3b55362cfb85cd1033</citedby><cites>FETCH-LOGICAL-c358t-5aa0a9f8ca72fff86c37310e6ec60b3095a8f74313821ac3b55362cfb85cd1033</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11270-021-05130-2$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11270-021-05130-2$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27923,27924,41487,42556,51318</link.rule.ids></links><search><creatorcontrib>Zhang, Ruiling</creatorcontrib><creatorcontrib>Chen, Linlin</creatorcontrib><creatorcontrib>Qiu, Binbin</creatorcontrib><creatorcontrib>Sun, Xiaojing</creatorcontrib><creatorcontrib>Qin, Songyan</creatorcontrib><creatorcontrib>Wang, Bo</creatorcontrib><creatorcontrib>Li, Feiyue</creatorcontrib><creatorcontrib>Zhao, Lixin</creatorcontrib><creatorcontrib>Zhu, Zhe</creatorcontrib><title>Biochar Derived from Treated Lotus Stem and Adsorption of Phthalic Acid Esters</title><title>Water, air, and soil pollution</title><addtitle>Water Air Soil Pollut</addtitle><description>Phthalic acid ester (PAE), a plasticizer, is increasingly being detected in different environments. These compounds can gravely affect the human endocrine system. The present study aims to prepare adsorbents that can effectively adsorb PAE pollutants. To fabricate a better carbon structure than conventional biochar, the sodium hydroxide solution was used as a hydrolyzing agent to pretreat the biomass in order to weaken the bonds in lignin, cellulose, and hemicellulose. As a result, biochar with a special porous carbon structure is obtained. To study the characteristics of the biochar and its adsorption properties, dimethyl phthalate (DMP)—a PAE—was selected as the adsorbate. The morphology and structural composition of the biochar were examined via an environment scanning electron microscope with a field emission gun (SEM), surface area analyzer (BET), Fourier transform infrared spectrometer (FTIR), thermal gravimetry (TG/DTG), X-ray diffractometry (XRD), and Raman spectroscopy. The BET data of the biochar increased by 125.3 times than that of the original biochar. The layer spacing and the surface functional groups of the pretreated biochar also increased. After performing the micro-morphological regulation of biomass using sodium hydroxide, the adsorption performance of biochar with regard to PAE effectively improved and an adsorption capacity of 125 mg/g was observed for DMP. The adsorption kinetics and thermodynamic experiments showed that DMP adsorption by biochar follows the Langmuir and pseudo-second-order models.</description><subject>Adsorbates</subject><subject>Adsorption</subject><subject>Analytical methods</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Biomass</subject><subject>Bonding agents</subject><subject>Bonding strength</subject><subject>Carbon</subject><subject>Caustic soda</subject><subject>Cellulose</subject><subject>Charcoal</subject><subject>Climate Change/Climate Change Impacts</subject><subject>Earth and Environmental Science</subject><subject>Emission analysis</subject><subject>Endocrine system</subject><subject>Environment</subject><subject>Environmental monitoring</subject><subject>Esters</subject><subject>Field emission microscopy</subject><subject>Fourier transforms</subject><subject>FTIR spectrometers</subject><subject>Functional groups</subject><subject>Gravimetric 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(PAE), a plasticizer, is increasingly being detected in different environments. These compounds can gravely affect the human endocrine system. The present study aims to prepare adsorbents that can effectively adsorb PAE pollutants. To fabricate a better carbon structure than conventional biochar, the sodium hydroxide solution was used as a hydrolyzing agent to pretreat the biomass in order to weaken the bonds in lignin, cellulose, and hemicellulose. As a result, biochar with a special porous carbon structure is obtained. To study the characteristics of the biochar and its adsorption properties, dimethyl phthalate (DMP)—a PAE—was selected as the adsorbate. The morphology and structural composition of the biochar were examined via an environment scanning electron microscope with a field emission gun (SEM), surface area analyzer (BET), Fourier transform infrared spectrometer (FTIR), thermal gravimetry (TG/DTG), X-ray diffractometry (XRD), and Raman spectroscopy. The BET data of the biochar increased by 125.3 times than that of the original biochar. The layer spacing and the surface functional groups of the pretreated biochar also increased. After performing the micro-morphological regulation of biomass using sodium hydroxide, the adsorption performance of biochar with regard to PAE effectively improved and an adsorption capacity of 125 mg/g was observed for DMP. The adsorption kinetics and thermodynamic experiments showed that DMP adsorption by biochar follows the Langmuir and pseudo-second-order models.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s11270-021-05130-2</doi></addata></record> |
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| subjects | Adsorbates Adsorption Analytical methods Atmospheric Protection/Air Quality Control/Air Pollution Biomass Bonding agents Bonding strength Carbon Caustic soda Cellulose Charcoal Climate Change/Climate Change Impacts Earth and Environmental Science Emission analysis Endocrine system Environment Environmental monitoring Esters Field emission microscopy Fourier transforms FTIR spectrometers Functional groups Gravimetric analysis Gravimetry Hemicellulose Hydrogeology Hydroxides Infrared analysis Infrared spectrometers Kinetics Lignin Morphology Phthalate esters Phthalates Phthalic acid Pollutants Raman spectroscopy Scanning electron microscopy Sodium Sodium hydroxide Soil Science & Conservation Surface chemistry Water Quality/Water Pollution |
| title | Biochar Derived from Treated Lotus Stem and Adsorption of Phthalic Acid Esters |
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