Obtaining and main dielectric properties of Ba0.6Pb0.4TiO3/graphene oxide composite

The paper describes the technology of obtaining and the results of the investigations of microstructure, XRD, SEM, main dielectric properties, electrical conductivity measurements and P - E hysteresis loops of Ba 0.6 Pb 0.4 TiO 3 /graphene oxide composite (abbr. BPT/GO). In the final step of the tec...

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Veröffentlicht in:Journal of materials science. Materials in electronics 2021-05, Vol.32 (9), p.11719-11726
Hauptverfasser: Skulski, Ryszard, Bochenek, Dariusz, Brzezińska, Dagmara, Stobiński, Leszek, Niemiec, Przemysław, Dercz, Grzegorz, Osińska, Katarzyna
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container_end_page 11726
container_issue 9
container_start_page 11719
container_title Journal of materials science. Materials in electronics
container_volume 32
creator Skulski, Ryszard
Bochenek, Dariusz
Brzezińska, Dagmara
Stobiński, Leszek
Niemiec, Przemysław
Dercz, Grzegorz
Osińska, Katarzyna
description The paper describes the technology of obtaining and the results of the investigations of microstructure, XRD, SEM, main dielectric properties, electrical conductivity measurements and P - E hysteresis loops of Ba 0.6 Pb 0.4 TiO 3 /graphene oxide composite (abbr. BPT/GO). In the final step of the technology, the samples have been sintered using the Spark Plasma Sintering (SPS) method. Diffraction patterns of the BPT/GO composite exhibit lines which can be related to perovskite structure. They also reveal additional lines that can be derived from the initial component oxides. Investigations of electrical conductivity suggest that the positive temperature coefficient of resistivity (PTCR) effect occurs at temperatures up to approximately 120 °C. Dielectric hysteresis loops below 90 °C are wide and typical for materials with rather high electrical conductivity. The hysteresis loop obtained at 120 °C is more typical for ferroelectrics. The obtained material is interesting, nevertheless it is probably possible to find better conditions of obtaining and/or a better composition thereof.
doi_str_mv 10.1007/s10854-021-05792-y
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subjects Characterization and Evaluation of Materials
Chemistry and Materials Science
Dielectric properties
Diffraction patterns
Electrical resistivity
Ferroelectric materials
Ferroelectricity
Graphene
Hysteresis loops
Materials Science
Optical and Electronic Materials
Perovskite structure
Perovskites
Plasma sintering
Positive temperature coefficient
Spark plasma sintering
title Obtaining and main dielectric properties of Ba0.6Pb0.4TiO3/graphene oxide composite
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