Effect of solid loading on properties of zirconia ceramic by direct ink writing
High solid loading water-based zirconia slurries for direct ink writing had been successfully prepared in this paper. The water-soluble epoxy resin and sodium polyacrylate were used as the binder and dispersant, respectively. The effect of solid loading on the rheological properties of zirconia slur...
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| Veröffentlicht in: | Materials research express 2021-01, Vol.8 (1), p.15403 |
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| description | High solid loading water-based zirconia slurries for direct ink writing had been successfully prepared in this paper. The water-soluble epoxy resin and sodium polyacrylate were used as the binder and dispersant, respectively. The effect of solid loading on the rheological properties of zirconia slurries was systematically investigated. The 54-58 vol.% zirconia slurries exhibited suitable printability for direct ink writing. After sintering at 1550 °C for 2 h, the properties of sintered zirconia ceramic specimens including linear shrinkage, relative density, flexural strength, tensile strength and microstructure were examined by a series of test methods. Further, the intrinsic relationships between the solid loading and physical and mechanical properties of zirconia ceramic specimens were explored. The experimental results showed that the densification and strength of sintered zirconia ceramic could be significantly improved by increasing the solid loading of zirconia due to the less content of organic matter and water. The maximum relative density, flexural strength and tensile strength of the sintered specimens were 98.8% ,676 10 MPa and 92 5 MPa, respectively, when the zirconia solid loading was 58 vol.%. |
| doi_str_mv | 10.1088/2053-1591/abd866 |
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The water-soluble epoxy resin and sodium polyacrylate were used as the binder and dispersant, respectively. The effect of solid loading on the rheological properties of zirconia slurries was systematically investigated. The 54-58 vol.% zirconia slurries exhibited suitable printability for direct ink writing. After sintering at 1550 °C for 2 h, the properties of sintered zirconia ceramic specimens including linear shrinkage, relative density, flexural strength, tensile strength and microstructure were examined by a series of test methods. Further, the intrinsic relationships between the solid loading and physical and mechanical properties of zirconia ceramic specimens were explored. The experimental results showed that the densification and strength of sintered zirconia ceramic could be significantly improved by increasing the solid loading of zirconia due to the less content of organic matter and water. The maximum relative density, flexural strength and tensile strength of the sintered specimens were 98.8% ,676 10 MPa and 92 5 MPa, respectively, when the zirconia solid loading was 58 vol.%.</description><identifier>ISSN: 2053-1591</identifier><identifier>EISSN: 2053-1591</identifier><identifier>DOI: 10.1088/2053-1591/abd866</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Acrylic resins ; Ceramics ; Densification ; Density ; Direct ink writing ; Dispersants ; Epoxy resins ; Flexural strength ; Mechanical properties ; Organic matter ; Physical properties ; Rapid prototyping ; Rheological properties ; Sintering ; Slurries ; Solid loading ; Tensile strength ; Zirconia ; Zirconium dioxide</subject><ispartof>Materials research express, 2021-01, Vol.8 (1), p.15403</ispartof><rights>2021 The Author(s). Published by IOP Publishing Ltd</rights><rights>2021. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c447t-85f55d0b95a4dd72b1c3d414ef4b069223ea0189f13ec3ac6c5b125b654a00c13</citedby><cites>FETCH-LOGICAL-c447t-85f55d0b95a4dd72b1c3d414ef4b069223ea0189f13ec3ac6c5b125b654a00c13</cites><orcidid>0000-0003-4115-8317</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://iopscience.iop.org/article/10.1088/2053-1591/abd866/pdf$$EPDF$$P50$$Giop$$Hfree_for_read</linktopdf><link.rule.ids>314,776,780,860,2096,27901,27902,38845,38867,53815,53842</link.rule.ids></links><search><creatorcontrib>Xia, Xiaoguang</creatorcontrib><creatorcontrib>Duan, Guolin</creatorcontrib><title>Effect of solid loading on properties of zirconia ceramic by direct ink writing</title><title>Materials research express</title><addtitle>MRX</addtitle><addtitle>Mater. Res. Express</addtitle><description>High solid loading water-based zirconia slurries for direct ink writing had been successfully prepared in this paper. The water-soluble epoxy resin and sodium polyacrylate were used as the binder and dispersant, respectively. The effect of solid loading on the rheological properties of zirconia slurries was systematically investigated. The 54-58 vol.% zirconia slurries exhibited suitable printability for direct ink writing. After sintering at 1550 °C for 2 h, the properties of sintered zirconia ceramic specimens including linear shrinkage, relative density, flexural strength, tensile strength and microstructure were examined by a series of test methods. Further, the intrinsic relationships between the solid loading and physical and mechanical properties of zirconia ceramic specimens were explored. The experimental results showed that the densification and strength of sintered zirconia ceramic could be significantly improved by increasing the solid loading of zirconia due to the less content of organic matter and water. 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Duan, Guolin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c447t-85f55d0b95a4dd72b1c3d414ef4b069223ea0189f13ec3ac6c5b125b654a00c13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Acrylic resins</topic><topic>Ceramics</topic><topic>Densification</topic><topic>Density</topic><topic>Direct ink writing</topic><topic>Dispersants</topic><topic>Epoxy resins</topic><topic>Flexural strength</topic><topic>Mechanical properties</topic><topic>Organic matter</topic><topic>Physical properties</topic><topic>Rapid prototyping</topic><topic>Rheological properties</topic><topic>Sintering</topic><topic>Slurries</topic><topic>Solid loading</topic><topic>Tensile strength</topic><topic>Zirconia</topic><topic>Zirconium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xia, Xiaoguang</creatorcontrib><creatorcontrib>Duan, Guolin</creatorcontrib><collection>IOP Publishing Free Content</collection><collection>IOPscience (Open Access)</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Materials research express</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xia, Xiaoguang</au><au>Duan, Guolin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of solid loading on properties of zirconia ceramic by direct ink writing</atitle><jtitle>Materials research express</jtitle><stitle>MRX</stitle><addtitle>Mater. Res. Express</addtitle><date>2021-01-01</date><risdate>2021</risdate><volume>8</volume><issue>1</issue><spage>15403</spage><pages>15403-</pages><issn>2053-1591</issn><eissn>2053-1591</eissn><abstract>High solid loading water-based zirconia slurries for direct ink writing had been successfully prepared in this paper. The water-soluble epoxy resin and sodium polyacrylate were used as the binder and dispersant, respectively. The effect of solid loading on the rheological properties of zirconia slurries was systematically investigated. The 54-58 vol.% zirconia slurries exhibited suitable printability for direct ink writing. After sintering at 1550 °C for 2 h, the properties of sintered zirconia ceramic specimens including linear shrinkage, relative density, flexural strength, tensile strength and microstructure were examined by a series of test methods. Further, the intrinsic relationships between the solid loading and physical and mechanical properties of zirconia ceramic specimens were explored. The experimental results showed that the densification and strength of sintered zirconia ceramic could be significantly improved by increasing the solid loading of zirconia due to the less content of organic matter and water. The maximum relative density, flexural strength and tensile strength of the sintered specimens were 98.8% ,676 10 MPa and 92 5 MPa, respectively, when the zirconia solid loading was 58 vol.%.</abstract><cop>Bristol</cop><pub>IOP Publishing</pub><doi>10.1088/2053-1591/abd866</doi><tpages>7</tpages><orcidid>https://orcid.org/0000-0003-4115-8317</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Acrylic resins Ceramics Densification Density Direct ink writing Dispersants Epoxy resins Flexural strength Mechanical properties Organic matter Physical properties Rapid prototyping Rheological properties Sintering Slurries Solid loading Tensile strength Zirconia Zirconium dioxide |
| title | Effect of solid loading on properties of zirconia ceramic by direct ink writing |
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