Study on Separation and Purification of Chemical Components of Dichloromethane from Pine Needle Extract
To study the chemical composition of the extract of cedar pine needle methylene chloride. Methods: The paper used silica gel and Sephadex LH-20 column chromatography to separate and purify, and carried out structural identification based on physical and chemical properties and spectral data. At the...
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| Veröffentlicht in: | IOP conference series. Earth and environmental science 2021-03, Vol.714 (3), p.32039 |
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| container_title | IOP conference series. Earth and environmental science |
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| creator | Liu, Yinan Liao, Bing Guo, Wenjie Fu, Yujie Sun, Wan Fu, Yao Wang, Dandan Kang, Hongling |
| description | To study the chemical composition of the extract of cedar pine needle methylene chloride. Methods: The paper used silica gel and Sephadex LH-20 column chromatography to separate and purify, and carried out structural identification based on physical and chemical properties and spectral data. At the same time, gallic acid was preliminarily separated by high-performance liquid chromatography (HPLC), the separation conditions of gallic acid were determined, and the content change of gallic acid after tannin was acid-decomposed was determined, proving that the extract may contain decomposable hydrolysis Tannin or compound tannin. Results: Five compounds were isolated from the dichloromethane extract of cedar pine needles, which were identified as: ferulic acid (1), osthol (2), β-phenylacrylic acid (3), paeonol (4), Magnolol (5). Conclusion: All compounds except Compound 5 were isolated from this plant for the first time. |
| doi_str_mv | 10.1088/1755-1315/714/3/032039 |
| format | Article |
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Methods: The paper used silica gel and Sephadex LH-20 column chromatography to separate and purify, and carried out structural identification based on physical and chemical properties and spectral data. At the same time, gallic acid was preliminarily separated by high-performance liquid chromatography (HPLC), the separation conditions of gallic acid were determined, and the content change of gallic acid after tannin was acid-decomposed was determined, proving that the extract may contain decomposable hydrolysis Tannin or compound tannin. Results: Five compounds were isolated from the dichloromethane extract of cedar pine needles, which were identified as: ferulic acid (1), osthol (2), β-phenylacrylic acid (3), paeonol (4), Magnolol (5). Conclusion: All compounds except Compound 5 were isolated from this plant for the first time.</description><identifier>ISSN: 1755-1307</identifier><identifier>EISSN: 1755-1315</identifier><identifier>DOI: 10.1088/1755-1315/714/3/032039</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Acids ; Cedar ; Chemical composition ; Chemical properties ; Chromatography ; Column chromatography ; Decomposition ; Dichloromethane ; Ferulic acid ; Gallic acid ; High performance liquid chromatography ; Liquid chromatography ; Pine needles ; Pinus glabra ; Separation ; Silica ; Silica gel ; Silicon dioxide ; Tannins</subject><ispartof>IOP conference series. Earth and environmental science, 2021-03, Vol.714 (3), p.32039</ispartof><rights>2021. This work is published under http://creativecommons.org/licenses/by/3.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c2309-6eefd48bba0fa36852c18f99fd9bdd28cce4030ff14c324fcbee887aca191e593</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Liu, Yinan</creatorcontrib><creatorcontrib>Liao, Bing</creatorcontrib><creatorcontrib>Guo, Wenjie</creatorcontrib><creatorcontrib>Fu, Yujie</creatorcontrib><creatorcontrib>Sun, Wan</creatorcontrib><creatorcontrib>Fu, Yao</creatorcontrib><creatorcontrib>Wang, Dandan</creatorcontrib><creatorcontrib>Kang, Hongling</creatorcontrib><title>Study on Separation and Purification of Chemical Components of Dichloromethane from Pine Needle Extract</title><title>IOP conference series. Earth and environmental science</title><description>To study the chemical composition of the extract of cedar pine needle methylene chloride. Methods: The paper used silica gel and Sephadex LH-20 column chromatography to separate and purify, and carried out structural identification based on physical and chemical properties and spectral data. At the same time, gallic acid was preliminarily separated by high-performance liquid chromatography (HPLC), the separation conditions of gallic acid were determined, and the content change of gallic acid after tannin was acid-decomposed was determined, proving that the extract may contain decomposable hydrolysis Tannin or compound tannin. Results: Five compounds were isolated from the dichloromethane extract of cedar pine needles, which were identified as: ferulic acid (1), osthol (2), β-phenylacrylic acid (3), paeonol (4), Magnolol (5). Conclusion: All compounds except Compound 5 were isolated from this plant for the first time.</description><subject>Acids</subject><subject>Cedar</subject><subject>Chemical composition</subject><subject>Chemical properties</subject><subject>Chromatography</subject><subject>Column chromatography</subject><subject>Decomposition</subject><subject>Dichloromethane</subject><subject>Ferulic acid</subject><subject>Gallic acid</subject><subject>High performance liquid chromatography</subject><subject>Liquid chromatography</subject><subject>Pine needles</subject><subject>Pinus glabra</subject><subject>Separation</subject><subject>Silica</subject><subject>Silica gel</subject><subject>Silicon dioxide</subject><subject>Tannins</subject><issn>1755-1307</issn><issn>1755-1315</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNo9kN1KxDAQRoMouK6-ggS8rk2atE0upa4_sOjC6nVI04nbpW1q0oL79rZUvJoz3wwzcBC6peSeEiFimqdpRBlN45zymMWEJYTJM7T6H5z_M8kv0VUIR0KynDO5Ql_7YaxO2HV4D732eqgn1F2Fd6OvbW2WwFlcHKCd2gYXru1dB90Q5vixNofGedfCcNAdYDsh3tUTvQFUDeDNz-C1Ga7RhdVNgJu_ukafT5uP4iXavj-_Fg_byCSMyCgDsBUXZamJ1SwTaWKosFLaSpZVlQhjgBNGrKXcsIRbUwIIkWujqaSQSrZGd8vd3rvvEcKgjm703fRSJSmlknPJxbSVLVvGuxA8WNX7utX-pChRs1Q1-1KzOzVJVUwtUtkvZKBr3A</recordid><startdate>20210301</startdate><enddate>20210301</enddate><creator>Liu, Yinan</creator><creator>Liao, Bing</creator><creator>Guo, Wenjie</creator><creator>Fu, Yujie</creator><creator>Sun, Wan</creator><creator>Fu, Yao</creator><creator>Wang, Dandan</creator><creator>Kang, Hongling</creator><general>IOP Publishing</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>PATMY</scope><scope>PHGZM</scope><scope>PHGZT</scope><scope>PIMPY</scope><scope>PKEHL</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PYCSY</scope></search><sort><creationdate>20210301</creationdate><title>Study on Separation and Purification of Chemical Components of Dichloromethane from Pine Needle Extract</title><author>Liu, Yinan ; Liao, Bing ; Guo, Wenjie ; Fu, Yujie ; Sun, Wan ; Fu, Yao ; Wang, Dandan ; Kang, Hongling</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2309-6eefd48bba0fa36852c18f99fd9bdd28cce4030ff14c324fcbee887aca191e593</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Acids</topic><topic>Cedar</topic><topic>Chemical composition</topic><topic>Chemical properties</topic><topic>Chromatography</topic><topic>Column chromatography</topic><topic>Decomposition</topic><topic>Dichloromethane</topic><topic>Ferulic acid</topic><topic>Gallic acid</topic><topic>High performance liquid chromatography</topic><topic>Liquid chromatography</topic><topic>Pine needles</topic><topic>Pinus glabra</topic><topic>Separation</topic><topic>Silica</topic><topic>Silica gel</topic><topic>Silicon dioxide</topic><topic>Tannins</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Yinan</creatorcontrib><creatorcontrib>Liao, Bing</creatorcontrib><creatorcontrib>Guo, Wenjie</creatorcontrib><creatorcontrib>Fu, Yujie</creatorcontrib><creatorcontrib>Sun, Wan</creatorcontrib><creatorcontrib>Fu, Yao</creatorcontrib><creatorcontrib>Wang, Dandan</creatorcontrib><creatorcontrib>Kang, Hongling</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Environmental Science Database</collection><collection>ProQuest Central (New)</collection><collection>ProQuest One Academic (New)</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Middle East (New)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Environmental Science Collection</collection><jtitle>IOP conference series. Earth and environmental science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Yinan</au><au>Liao, Bing</au><au>Guo, Wenjie</au><au>Fu, Yujie</au><au>Sun, Wan</au><au>Fu, Yao</au><au>Wang, Dandan</au><au>Kang, Hongling</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Study on Separation and Purification of Chemical Components of Dichloromethane from Pine Needle Extract</atitle><jtitle>IOP conference series. Earth and environmental science</jtitle><date>2021-03-01</date><risdate>2021</risdate><volume>714</volume><issue>3</issue><spage>32039</spage><pages>32039-</pages><issn>1755-1307</issn><eissn>1755-1315</eissn><abstract>To study the chemical composition of the extract of cedar pine needle methylene chloride. Methods: The paper used silica gel and Sephadex LH-20 column chromatography to separate and purify, and carried out structural identification based on physical and chemical properties and spectral data. At the same time, gallic acid was preliminarily separated by high-performance liquid chromatography (HPLC), the separation conditions of gallic acid were determined, and the content change of gallic acid after tannin was acid-decomposed was determined, proving that the extract may contain decomposable hydrolysis Tannin or compound tannin. Results: Five compounds were isolated from the dichloromethane extract of cedar pine needles, which were identified as: ferulic acid (1), osthol (2), β-phenylacrylic acid (3), paeonol (4), Magnolol (5). Conclusion: All compounds except Compound 5 were isolated from this plant for the first time.</abstract><cop>Bristol</cop><pub>IOP Publishing</pub><doi>10.1088/1755-1315/714/3/032039</doi><oa>free_for_read</oa></addata></record> |
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| subjects | Acids Cedar Chemical composition Chemical properties Chromatography Column chromatography Decomposition Dichloromethane Ferulic acid Gallic acid High performance liquid chromatography Liquid chromatography Pine needles Pinus glabra Separation Silica Silica gel Silicon dioxide Tannins |
| title | Study on Separation and Purification of Chemical Components of Dichloromethane from Pine Needle Extract |
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