Temperature measurement in double-sided laser-heated diamond anvil cell and reaction of carbon
In this work, a double-sided laser-heated diamond anvil cell facility for studies at extreme conditions of pressure and temperature that has been developed is described in detail. Phase transitions occurring at extreme conditions can be mapped by accurate measurements of pressure and temperature. Mi...
Gespeichert in:
| Veröffentlicht in: | Indian journal of physics 2021-04, Vol.95 (4), p.621-628 |
|---|---|
| Hauptverfasser: | , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 628 |
|---|---|
| container_issue | 4 |
| container_start_page | 621 |
| container_title | Indian journal of physics |
| container_volume | 95 |
| creator | Saha, P Mukherjee, G D |
| description | In this work, a double-sided laser-heated diamond anvil cell facility for studies at extreme conditions of pressure and temperature that has been developed is described in detail. Phase transitions occurring at extreme conditions can be mapped by accurate measurements of pressure and temperature. Micrometer-sized diamond crystals having regular facets have been synthesized at a pressure of 18 GPa and temperature 1785 K, which is confirmed by visual inspection, micro-Raman and field emission scanning electron micrograph measurements. A low-temperature gradient is observed across the sample surface during the formation of micrometer-sized diamond crystals. Our observation restricts the use of steel gasket as it can react with carbon (C) transported from the diamond anvil. The reaction of C with one of the potential thermal insulating medium Al
2
O
3
is observed in the X-ray diffraction measurements. |
| doi_str_mv | 10.1007/s12648-020-01699-2 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2504492370</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2504492370</sourcerecordid><originalsourceid>FETCH-LOGICAL-c319t-7d83f4cf2890912c5efd2bc06442dccd14bdb332232be5b64cef8735f2b038803</originalsourceid><addsrcrecordid>eNp9kElLBDEUhIMoOI7-AU8Bz9FsveQogxsIXsarIcuL9tCdjEmP4L-3Z1rw5qnqQVU9-BC6ZPSaUdrcFMZr2RLKKaGsVorwI7SgqpFEtbI6PnhBmKzaU3RWyobSWrGmWqC3NQxbyGbcZcADmDLpAHHEXcQ-7WwPpHQePO5NgUw-wIzT4TszpOixiV9djx30_WQ9zmDc2KWIU8DOZJviOToJpi9w8atL9Hp_t149kueXh6fV7TNxgqmRNL4VQbrAW0UV466C4Ll1tJaSe-c8k9ZbITgX3EJla-kgtI2oArdUtC0VS3Q1725z-txBGfUm7XKcXmpeUSkVF80-xeeUy6mUDEFvczeY_K0Z1XuOeuaoJ476wFHzqSTmUpnC8R3y3_Q_rR8UvnZ7</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2504492370</pqid></control><display><type>article</type><title>Temperature measurement in double-sided laser-heated diamond anvil cell and reaction of carbon</title><source>Springer Nature - Complete Springer Journals</source><creator>Saha, P ; Mukherjee, G D</creator><creatorcontrib>Saha, P ; Mukherjee, G D</creatorcontrib><description>In this work, a double-sided laser-heated diamond anvil cell facility for studies at extreme conditions of pressure and temperature that has been developed is described in detail. Phase transitions occurring at extreme conditions can be mapped by accurate measurements of pressure and temperature. Micrometer-sized diamond crystals having regular facets have been synthesized at a pressure of 18 GPa and temperature 1785 K, which is confirmed by visual inspection, micro-Raman and field emission scanning electron micrograph measurements. A low-temperature gradient is observed across the sample surface during the formation of micrometer-sized diamond crystals. Our observation restricts the use of steel gasket as it can react with carbon (C) transported from the diamond anvil. The reaction of C with one of the potential thermal insulating medium Al
2
O
3
is observed in the X-ray diffraction measurements.</description><identifier>ISSN: 0973-1458</identifier><identifier>EISSN: 0974-9845</identifier><identifier>DOI: 10.1007/s12648-020-01699-2</identifier><language>eng</language><publisher>New Delhi: Springer India</publisher><subject>Anvils ; Astrophysics and Astroparticles ; Carbon ; Diamond anvil cells ; Electron micrographs ; Field emission ; Inspection ; Laser beam heating ; Low temperature ; Original Paper ; Phase transitions ; Physics ; Physics and Astronomy ; Temperature measurement ; Visual fields</subject><ispartof>Indian journal of physics, 2021-04, Vol.95 (4), p.621-628</ispartof><rights>Indian Association for the Cultivation of Science 2020</rights><rights>Indian Association for the Cultivation of Science 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-7d83f4cf2890912c5efd2bc06442dccd14bdb332232be5b64cef8735f2b038803</citedby><cites>FETCH-LOGICAL-c319t-7d83f4cf2890912c5efd2bc06442dccd14bdb332232be5b64cef8735f2b038803</cites><orcidid>0000-0001-9832-3024</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s12648-020-01699-2$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s12648-020-01699-2$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Saha, P</creatorcontrib><creatorcontrib>Mukherjee, G D</creatorcontrib><title>Temperature measurement in double-sided laser-heated diamond anvil cell and reaction of carbon</title><title>Indian journal of physics</title><addtitle>Indian J Phys</addtitle><description>In this work, a double-sided laser-heated diamond anvil cell facility for studies at extreme conditions of pressure and temperature that has been developed is described in detail. Phase transitions occurring at extreme conditions can be mapped by accurate measurements of pressure and temperature. Micrometer-sized diamond crystals having regular facets have been synthesized at a pressure of 18 GPa and temperature 1785 K, which is confirmed by visual inspection, micro-Raman and field emission scanning electron micrograph measurements. A low-temperature gradient is observed across the sample surface during the formation of micrometer-sized diamond crystals. Our observation restricts the use of steel gasket as it can react with carbon (C) transported from the diamond anvil. The reaction of C with one of the potential thermal insulating medium Al
2
O
3
is observed in the X-ray diffraction measurements.</description><subject>Anvils</subject><subject>Astrophysics and Astroparticles</subject><subject>Carbon</subject><subject>Diamond anvil cells</subject><subject>Electron micrographs</subject><subject>Field emission</subject><subject>Inspection</subject><subject>Laser beam heating</subject><subject>Low temperature</subject><subject>Original Paper</subject><subject>Phase transitions</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Temperature measurement</subject><subject>Visual fields</subject><issn>0973-1458</issn><issn>0974-9845</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kElLBDEUhIMoOI7-AU8Bz9FsveQogxsIXsarIcuL9tCdjEmP4L-3Z1rw5qnqQVU9-BC6ZPSaUdrcFMZr2RLKKaGsVorwI7SgqpFEtbI6PnhBmKzaU3RWyobSWrGmWqC3NQxbyGbcZcADmDLpAHHEXcQ-7WwPpHQePO5NgUw-wIzT4TszpOixiV9djx30_WQ9zmDc2KWIU8DOZJviOToJpi9w8atL9Hp_t149kueXh6fV7TNxgqmRNL4VQbrAW0UV466C4Ll1tJaSe-c8k9ZbITgX3EJla-kgtI2oArdUtC0VS3Q1725z-txBGfUm7XKcXmpeUSkVF80-xeeUy6mUDEFvczeY_K0Z1XuOeuaoJ476wFHzqSTmUpnC8R3y3_Q_rR8UvnZ7</recordid><startdate>20210401</startdate><enddate>20210401</enddate><creator>Saha, P</creator><creator>Mukherjee, G D</creator><general>Springer India</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0001-9832-3024</orcidid></search><sort><creationdate>20210401</creationdate><title>Temperature measurement in double-sided laser-heated diamond anvil cell and reaction of carbon</title><author>Saha, P ; Mukherjee, G D</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-7d83f4cf2890912c5efd2bc06442dccd14bdb332232be5b64cef8735f2b038803</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Anvils</topic><topic>Astrophysics and Astroparticles</topic><topic>Carbon</topic><topic>Diamond anvil cells</topic><topic>Electron micrographs</topic><topic>Field emission</topic><topic>Inspection</topic><topic>Laser beam heating</topic><topic>Low temperature</topic><topic>Original Paper</topic><topic>Phase transitions</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Temperature measurement</topic><topic>Visual fields</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Saha, P</creatorcontrib><creatorcontrib>Mukherjee, G D</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Indian journal of physics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Saha, P</au><au>Mukherjee, G D</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Temperature measurement in double-sided laser-heated diamond anvil cell and reaction of carbon</atitle><jtitle>Indian journal of physics</jtitle><stitle>Indian J Phys</stitle><date>2021-04-01</date><risdate>2021</risdate><volume>95</volume><issue>4</issue><spage>621</spage><epage>628</epage><pages>621-628</pages><issn>0973-1458</issn><eissn>0974-9845</eissn><abstract>In this work, a double-sided laser-heated diamond anvil cell facility for studies at extreme conditions of pressure and temperature that has been developed is described in detail. Phase transitions occurring at extreme conditions can be mapped by accurate measurements of pressure and temperature. Micrometer-sized diamond crystals having regular facets have been synthesized at a pressure of 18 GPa and temperature 1785 K, which is confirmed by visual inspection, micro-Raman and field emission scanning electron micrograph measurements. A low-temperature gradient is observed across the sample surface during the formation of micrometer-sized diamond crystals. Our observation restricts the use of steel gasket as it can react with carbon (C) transported from the diamond anvil. The reaction of C with one of the potential thermal insulating medium Al
2
O
3
is observed in the X-ray diffraction measurements.</abstract><cop>New Delhi</cop><pub>Springer India</pub><doi>10.1007/s12648-020-01699-2</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0001-9832-3024</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0973-1458 |
| ispartof | Indian journal of physics, 2021-04, Vol.95 (4), p.621-628 |
| issn | 0973-1458 0974-9845 |
| language | eng |
| recordid | cdi_proquest_journals_2504492370 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Anvils Astrophysics and Astroparticles Carbon Diamond anvil cells Electron micrographs Field emission Inspection Laser beam heating Low temperature Original Paper Phase transitions Physics Physics and Astronomy Temperature measurement Visual fields |
| title | Temperature measurement in double-sided laser-heated diamond anvil cell and reaction of carbon |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-31T15%3A46%3A14IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Temperature%20measurement%20in%20double-sided%20laser-heated%20diamond%20anvil%20cell%20and%20reaction%20of%20carbon&rft.jtitle=Indian%20journal%20of%20physics&rft.au=Saha,%20P&rft.date=2021-04-01&rft.volume=95&rft.issue=4&rft.spage=621&rft.epage=628&rft.pages=621-628&rft.issn=0973-1458&rft.eissn=0974-9845&rft_id=info:doi/10.1007/s12648-020-01699-2&rft_dat=%3Cproquest_cross%3E2504492370%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2504492370&rft_id=info:pmid/&rfr_iscdi=true |