Spontaneous cationic ordering in chemical-solution-grown La2CoMnO6 double perovskite thin films
Double perovskite oxides are of interest because of their electric, magnetic, and elastic properties; however, these properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. Therefore, many efforts have been made to improve the level of cationic ord...
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| creator | Wang, Hailin Gazquez, Jaume Frontera, Carlos Chisholm, Matthew F. Pomar, Alberto Martinez, Benjamin Mestres, Narcis |
| description | Double perovskite oxides are of interest because of their electric, magnetic, and elastic properties; however, these properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. Therefore, many efforts have been made to improve the level of cationic ordering to obtain optimal properties while suppressing antisite defect formation. Here, epitaxial double perovskite La
2
CoMnO
6
thin films were grown on top of (001)-STO oriented substrates by a polymer-assisted deposition chemical solution approach. Confirmation of the achievement of full Co/Mn cationic ordering was found by scanning transmission electron microscopy (STEM) measurements; EELS maps indicated the ordered occupancy of B–B′ sites by Co/Mn cations. As a result, optimal magnetic properties (
Msat
≈ 6 µ
B
/f.u. and
Tc
≈ 230 K) are obtained. We show that the slow growth rates that occur close to thermodynamic equilibrium conditions in chemical solution methods represent an advantageous alternative to physical deposition methods for the preparation of oxide thin films in which complex cationic ordering is involved.
Thin films: Perfectly flat ceramics unleash their magnetism
Using polymers to control the growth of ceramic thin films can make it easier to produce materials for spintronic applications, which use electron spin instead of charge to carry information. When the semiconductor lanthanum cobalt manganese oxide (La
2
CoMnO
6
) adopts a crystal arrangement known as a double perovskite structure, it takes on boosted magnetic properties. Narcis Mestres from the Institut de Ciència de Materials de Barcelona in Spain and colleagues have developed a fabrication strategy that lets La
2
CoMnO
6
epitaxial thin films grow in an optimal orientation for device applications. The team used a mixture of water-soluble polymers to bind to metal cations and slow down crystallization rates so that the most thermodynamically favored perovskite structure formed. The resulting surfaces were smooth down to a nanometer scale, and had significantly higher magnetism than samples grown with conventional vapor deposition techniques.
Double perovskites have a wide range of properties and a corresponding broad range of potential applications, including magneto-optic and spintronic devices. However, their electric, magnetic, and elastic properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. In this work we show that the parti |
| doi_str_mv | 10.1038/s41427-019-0144-8 |
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2
CoMnO
6
thin films were grown on top of (001)-STO oriented substrates by a polymer-assisted deposition chemical solution approach. Confirmation of the achievement of full Co/Mn cationic ordering was found by scanning transmission electron microscopy (STEM) measurements; EELS maps indicated the ordered occupancy of B–B′ sites by Co/Mn cations. As a result, optimal magnetic properties (
Msat
≈ 6 µ
B
/f.u. and
Tc
≈ 230 K) are obtained. We show that the slow growth rates that occur close to thermodynamic equilibrium conditions in chemical solution methods represent an advantageous alternative to physical deposition methods for the preparation of oxide thin films in which complex cationic ordering is involved.
Thin films: Perfectly flat ceramics unleash their magnetism
Using polymers to control the growth of ceramic thin films can make it easier to produce materials for spintronic applications, which use electron spin instead of charge to carry information. When the semiconductor lanthanum cobalt manganese oxide (La
2
CoMnO
6
) adopts a crystal arrangement known as a double perovskite structure, it takes on boosted magnetic properties. Narcis Mestres from the Institut de Ciència de Materials de Barcelona in Spain and colleagues have developed a fabrication strategy that lets La
2
CoMnO
6
epitaxial thin films grow in an optimal orientation for device applications. The team used a mixture of water-soluble polymers to bind to metal cations and slow down crystallization rates so that the most thermodynamically favored perovskite structure formed. The resulting surfaces were smooth down to a nanometer scale, and had significantly higher magnetism than samples grown with conventional vapor deposition techniques.
Double perovskites have a wide range of properties and a corresponding broad range of potential applications, including magneto-optic and spintronic devices. However, their electric, magnetic, and elastic properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. In this work we show that the particular crystallization and growth process conditions (very slow rate, close to thermodynamic equilibrium conditions) of Polymer Assisted Deposition (PAD), promote very high B-site cationic ordering. Confirmation of the achievement of full Co/Mn cationic ordering is found in PAD grown epitaxial La
2
CoMnO
6
/SrTiO
3
double perovskite thin films displaying optimal magnetic properties.</description><identifier>ISSN: 1884-4049</identifier><identifier>EISSN: 1884-4057</identifier><identifier>DOI: 10.1038/s41427-019-0144-8</identifier><language>eng</language><publisher>London: Nature Publishing Group UK</publisher><subject>639/301/119/997 ; 639/638/298/920 ; Biomaterials ; Cations ; Chemistry and Materials Science ; Cobalt compounds ; Crystal structure ; Crystallization ; Current carriers ; Deposition ; Eels ; Elastic properties ; Electron spin ; Energy Systems ; Epitaxial growth ; Equilibrium conditions ; Lanthanum ; Magnetic properties ; Magnetism ; Manganese ; Materials Science ; MSAT ; Occupancy ; Optical and Electronic Materials ; Organic chemistry ; Perovskite structure ; Perovskites ; Scanning electron microscopy ; Scanning transmission electron microscopy ; Structural Materials ; Substrates ; Surface and Interface Science ; Thermodynamic equilibrium ; Thin Films ; Vapor deposition ; Water soluble polymers</subject><ispartof>NPG Asia materials, 2019-08, Vol.11 (1), p.1-8, Article 44</ispartof><rights>The Author(s) 2019</rights><rights>2019. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>The Author(s) 2019. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c387t-826187d7581bae73759dc9c3cf71ba87c4adfbcc4880771f2514f2550193e6783</citedby><cites>FETCH-LOGICAL-c387t-826187d7581bae73759dc9c3cf71ba87c4adfbcc4880771f2514f2550193e6783</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1038/s41427-019-0144-8$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://doi.org/10.1038/s41427-019-0144-8$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>314,780,784,864,27924,27925,41120,42189,51576</link.rule.ids></links><search><creatorcontrib>Wang, Hailin</creatorcontrib><creatorcontrib>Gazquez, Jaume</creatorcontrib><creatorcontrib>Frontera, Carlos</creatorcontrib><creatorcontrib>Chisholm, Matthew F.</creatorcontrib><creatorcontrib>Pomar, Alberto</creatorcontrib><creatorcontrib>Martinez, Benjamin</creatorcontrib><creatorcontrib>Mestres, Narcis</creatorcontrib><title>Spontaneous cationic ordering in chemical-solution-grown La2CoMnO6 double perovskite thin films</title><title>NPG Asia materials</title><addtitle>NPG Asia Mater</addtitle><description>Double perovskite oxides are of interest because of their electric, magnetic, and elastic properties; however, these properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. Therefore, many efforts have been made to improve the level of cationic ordering to obtain optimal properties while suppressing antisite defect formation. Here, epitaxial double perovskite La
2
CoMnO
6
thin films were grown on top of (001)-STO oriented substrates by a polymer-assisted deposition chemical solution approach. Confirmation of the achievement of full Co/Mn cationic ordering was found by scanning transmission electron microscopy (STEM) measurements; EELS maps indicated the ordered occupancy of B–B′ sites by Co/Mn cations. As a result, optimal magnetic properties (
Msat
≈ 6 µ
B
/f.u. and
Tc
≈ 230 K) are obtained. We show that the slow growth rates that occur close to thermodynamic equilibrium conditions in chemical solution methods represent an advantageous alternative to physical deposition methods for the preparation of oxide thin films in which complex cationic ordering is involved.
Thin films: Perfectly flat ceramics unleash their magnetism
Using polymers to control the growth of ceramic thin films can make it easier to produce materials for spintronic applications, which use electron spin instead of charge to carry information. When the semiconductor lanthanum cobalt manganese oxide (La
2
CoMnO
6
) adopts a crystal arrangement known as a double perovskite structure, it takes on boosted magnetic properties. Narcis Mestres from the Institut de Ciència de Materials de Barcelona in Spain and colleagues have developed a fabrication strategy that lets La
2
CoMnO
6
epitaxial thin films grow in an optimal orientation for device applications. The team used a mixture of water-soluble polymers to bind to metal cations and slow down crystallization rates so that the most thermodynamically favored perovskite structure formed. The resulting surfaces were smooth down to a nanometer scale, and had significantly higher magnetism than samples grown with conventional vapor deposition techniques.
Double perovskites have a wide range of properties and a corresponding broad range of potential applications, including magneto-optic and spintronic devices. However, their electric, magnetic, and elastic properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. In this work we show that the particular crystallization and growth process conditions (very slow rate, close to thermodynamic equilibrium conditions) of Polymer Assisted Deposition (PAD), promote very high B-site cationic ordering. Confirmation of the achievement of full Co/Mn cationic ordering is found in PAD grown epitaxial La
2
CoMnO
6
/SrTiO
3
double perovskite thin films displaying optimal magnetic properties.</description><subject>639/301/119/997</subject><subject>639/638/298/920</subject><subject>Biomaterials</subject><subject>Cations</subject><subject>Chemistry and Materials Science</subject><subject>Cobalt compounds</subject><subject>Crystal structure</subject><subject>Crystallization</subject><subject>Current carriers</subject><subject>Deposition</subject><subject>Eels</subject><subject>Elastic properties</subject><subject>Electron spin</subject><subject>Energy Systems</subject><subject>Epitaxial growth</subject><subject>Equilibrium conditions</subject><subject>Lanthanum</subject><subject>Magnetic properties</subject><subject>Magnetism</subject><subject>Manganese</subject><subject>Materials Science</subject><subject>MSAT</subject><subject>Occupancy</subject><subject>Optical and Electronic Materials</subject><subject>Organic chemistry</subject><subject>Perovskite structure</subject><subject>Perovskites</subject><subject>Scanning electron microscopy</subject><subject>Scanning transmission electron microscopy</subject><subject>Structural Materials</subject><subject>Substrates</subject><subject>Surface and Interface Science</subject><subject>Thermodynamic equilibrium</subject><subject>Thin Films</subject><subject>Vapor deposition</subject><subject>Water soluble polymers</subject><issn>1884-4049</issn><issn>1884-4057</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9UE1PxCAQJUYTN7o_wBuJZxQoLXA0G7-SNXtQz4SldJe1CxVajf9eao2e9DAfmZn3XuYBcEbwBcGFuEyMMMoRJjIHY0gcgBkRgiGGS3740zN5DOYp7TDGpKqYKNkMqMcu-F57G4YEje5d8M7AEGsbnd9A56HZ2r0zukUptMO4R5sY3j1caroID35VwToM69bCzsbwll5cb2G_zcDGtft0Co4a3SY7_64n4Pnm-mlxh5ar2_vF1RKZQvAeCVoRwWteCrLWlhe8lLWRpjANzwPBDdN1szaGCYE5Jw0tCcupzC8XtuKiOAHnE28Xw-tgU692YYg-SyrKpGSYUCr_vaJVJsbsi4tMVyaGlKJtVBfdXscPRbAaDVeT4Sqrq9FwNWLohEndaJyNv8x_gz4B7kyCQw</recordid><startdate>20190802</startdate><enddate>20190802</enddate><creator>Wang, Hailin</creator><creator>Gazquez, Jaume</creator><creator>Frontera, Carlos</creator><creator>Chisholm, Matthew F.</creator><creator>Pomar, Alberto</creator><creator>Martinez, Benjamin</creator><creator>Mestres, Narcis</creator><general>Nature Publishing Group UK</general><general>Nature Publishing Group</general><scope>C6C</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope></search><sort><creationdate>20190802</creationdate><title>Spontaneous cationic ordering in chemical-solution-grown La2CoMnO6 double perovskite thin films</title><author>Wang, Hailin ; Gazquez, Jaume ; Frontera, Carlos ; Chisholm, Matthew F. ; Pomar, Alberto ; Martinez, Benjamin ; Mestres, Narcis</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c387t-826187d7581bae73759dc9c3cf71ba87c4adfbcc4880771f2514f2550193e6783</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>639/301/119/997</topic><topic>639/638/298/920</topic><topic>Biomaterials</topic><topic>Cations</topic><topic>Chemistry and Materials Science</topic><topic>Cobalt compounds</topic><topic>Crystal structure</topic><topic>Crystallization</topic><topic>Current carriers</topic><topic>Deposition</topic><topic>Eels</topic><topic>Elastic properties</topic><topic>Electron spin</topic><topic>Energy Systems</topic><topic>Epitaxial growth</topic><topic>Equilibrium conditions</topic><topic>Lanthanum</topic><topic>Magnetic properties</topic><topic>Magnetism</topic><topic>Manganese</topic><topic>Materials Science</topic><topic>MSAT</topic><topic>Occupancy</topic><topic>Optical and Electronic Materials</topic><topic>Organic chemistry</topic><topic>Perovskite structure</topic><topic>Perovskites</topic><topic>Scanning electron microscopy</topic><topic>Scanning transmission electron microscopy</topic><topic>Structural Materials</topic><topic>Substrates</topic><topic>Surface and Interface Science</topic><topic>Thermodynamic equilibrium</topic><topic>Thin Films</topic><topic>Vapor deposition</topic><topic>Water soluble polymers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Hailin</creatorcontrib><creatorcontrib>Gazquez, Jaume</creatorcontrib><creatorcontrib>Frontera, Carlos</creatorcontrib><creatorcontrib>Chisholm, Matthew F.</creatorcontrib><creatorcontrib>Pomar, Alberto</creatorcontrib><creatorcontrib>Martinez, Benjamin</creatorcontrib><creatorcontrib>Mestres, Narcis</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>NPG Asia materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Hailin</au><au>Gazquez, Jaume</au><au>Frontera, Carlos</au><au>Chisholm, Matthew F.</au><au>Pomar, Alberto</au><au>Martinez, Benjamin</au><au>Mestres, Narcis</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Spontaneous cationic ordering in chemical-solution-grown La2CoMnO6 double perovskite thin films</atitle><jtitle>NPG Asia materials</jtitle><stitle>NPG Asia Mater</stitle><date>2019-08-02</date><risdate>2019</risdate><volume>11</volume><issue>1</issue><spage>1</spage><epage>8</epage><pages>1-8</pages><artnum>44</artnum><issn>1884-4049</issn><eissn>1884-4057</eissn><abstract>Double perovskite oxides are of interest because of their electric, magnetic, and elastic properties; however, these properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. Therefore, many efforts have been made to improve the level of cationic ordering to obtain optimal properties while suppressing antisite defect formation. Here, epitaxial double perovskite La
2
CoMnO
6
thin films were grown on top of (001)-STO oriented substrates by a polymer-assisted deposition chemical solution approach. Confirmation of the achievement of full Co/Mn cationic ordering was found by scanning transmission electron microscopy (STEM) measurements; EELS maps indicated the ordered occupancy of B–B′ sites by Co/Mn cations. As a result, optimal magnetic properties (
Msat
≈ 6 µ
B
/f.u. and
Tc
≈ 230 K) are obtained. We show that the slow growth rates that occur close to thermodynamic equilibrium conditions in chemical solution methods represent an advantageous alternative to physical deposition methods for the preparation of oxide thin films in which complex cationic ordering is involved.
Thin films: Perfectly flat ceramics unleash their magnetism
Using polymers to control the growth of ceramic thin films can make it easier to produce materials for spintronic applications, which use electron spin instead of charge to carry information. When the semiconductor lanthanum cobalt manganese oxide (La
2
CoMnO
6
) adopts a crystal arrangement known as a double perovskite structure, it takes on boosted magnetic properties. Narcis Mestres from the Institut de Ciència de Materials de Barcelona in Spain and colleagues have developed a fabrication strategy that lets La
2
CoMnO
6
epitaxial thin films grow in an optimal orientation for device applications. The team used a mixture of water-soluble polymers to bind to metal cations and slow down crystallization rates so that the most thermodynamically favored perovskite structure formed. The resulting surfaces were smooth down to a nanometer scale, and had significantly higher magnetism than samples grown with conventional vapor deposition techniques.
Double perovskites have a wide range of properties and a corresponding broad range of potential applications, including magneto-optic and spintronic devices. However, their electric, magnetic, and elastic properties are strongly dependent on the ordered arrangement of cations in the double perovskite structure. In this work we show that the particular crystallization and growth process conditions (very slow rate, close to thermodynamic equilibrium conditions) of Polymer Assisted Deposition (PAD), promote very high B-site cationic ordering. Confirmation of the achievement of full Co/Mn cationic ordering is found in PAD grown epitaxial La
2
CoMnO
6
/SrTiO
3
double perovskite thin films displaying optimal magnetic properties.</abstract><cop>London</cop><pub>Nature Publishing Group UK</pub><doi>10.1038/s41427-019-0144-8</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record> |
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| issn | 1884-4049 1884-4057 |
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| source | DOAJ Directory of Open Access Journals; Springer Nature OA Free Journals; Nature Free; EZB-FREE-00999 freely available EZB journals; Free Full-Text Journals in Chemistry |
| subjects | 639/301/119/997 639/638/298/920 Biomaterials Cations Chemistry and Materials Science Cobalt compounds Crystal structure Crystallization Current carriers Deposition Eels Elastic properties Electron spin Energy Systems Epitaxial growth Equilibrium conditions Lanthanum Magnetic properties Magnetism Manganese Materials Science MSAT Occupancy Optical and Electronic Materials Organic chemistry Perovskite structure Perovskites Scanning electron microscopy Scanning transmission electron microscopy Structural Materials Substrates Surface and Interface Science Thermodynamic equilibrium Thin Films Vapor deposition Water soluble polymers |
| title | Spontaneous cationic ordering in chemical-solution-grown La2CoMnO6 double perovskite thin films |
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