Effect of heat treatment on the microstructure and elevated temperature tensile properties of Rene 41 alloy produced by laser powder bed fusion

The microstructure and elevated temperature mechanical properties of a precipitation hardenable Nickel based superalloy, Rene 41, fabricated by laser powder bed fusion followed by two different heat treatment regimes were studied. The as-built (AB) microstructure consists of γ columnar grains aligne...

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Veröffentlicht in:Journal of alloys and compounds 2021-03, Vol.858, p.157645, Article 157645
Hauptverfasser: Atabay, Sıla Ece, Sanchez-Mata, Oscar, Muñiz-Lerma, Jose Alberto, Brochu, Mathieu
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Sanchez-Mata, Oscar
Muñiz-Lerma, Jose Alberto
Brochu, Mathieu
description The microstructure and elevated temperature mechanical properties of a precipitation hardenable Nickel based superalloy, Rene 41, fabricated by laser powder bed fusion followed by two different heat treatment regimes were studied. The as-built (AB) microstructure consists of γ columnar grains aligned in direction. No γ′ precipitates were observed in the AB condition. Following to a sub-solvus solutionizing and aging heat treatment, the AB grain morphology was maintained. The development of fine γ′ precipitates within the grains along with the discrete carbide particles on the grain boundaries occurred. Heat treatment above the solvus temperature of γ’ resulted in the formation of a random equiaxed grain morphology. The γ′ and carbide precipitation was also observed in this heat treatment regime, but their distribution and morphology were different. Uniaxial tensile tests were conducted at 760 °C. Average yield strength values for AB, sub-solvus and super-solvus heat treated alloys were 879, 824 and 855 MPa respectively. The three tested conditions showed similar strength values that are comparable with a wrought alloy at the testing temperature. However, the elongation and deformation behaviors were different for each condition. Sub-solvus heat treatment lead to the highest elongation at break with 22% whereas super-solvus heat treatment resulted in the highest work hardening rate during deformation. •Defect free Rene 41 parts produced by LPBF are subjected to sub-solvus/super-solvus solutionizing and aging heat treatment.•Microstructural of the parts were characterized in as built and after two different heat treatment regimes.•Elevated temperature mechanical properties were investigated and correlated with the resulting microstructures.
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The as-built (AB) microstructure consists of γ columnar grains aligned in direction. No γ′ precipitates were observed in the AB condition. Following to a sub-solvus solutionizing and aging heat treatment, the AB grain morphology was maintained. The development of fine γ′ precipitates within the grains along with the discrete carbide particles on the grain boundaries occurred. Heat treatment above the solvus temperature of γ’ resulted in the formation of a random equiaxed grain morphology. The γ′ and carbide precipitation was also observed in this heat treatment regime, but their distribution and morphology were different. Uniaxial tensile tests were conducted at 760 °C. Average yield strength values for AB, sub-solvus and super-solvus heat treated alloys were 879, 824 and 855 MPa respectively. The three tested conditions showed similar strength values that are comparable with a wrought alloy at the testing temperature. 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Sub-solvus heat treatment lead to the highest elongation at break with 22% whereas super-solvus heat treatment resulted in the highest work hardening rate during deformation. •Defect free Rene 41 parts produced by LPBF are subjected to sub-solvus/super-solvus solutionizing and aging heat treatment.•Microstructural of the parts were characterized in as built and after two different heat treatment regimes.•Elevated temperature mechanical properties were investigated and correlated with the resulting microstructures.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2020.157645</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Alloys ; Carbides ; Chemical precipitation ; Deformation ; Elongation ; Grain boundaries ; Hardenability ; Hardening rate ; Heat treating ; Heat treatment ; High temperature ; Laser powder bed fusion ; Mechanical properties ; Microstructure ; Morphology ; Nickel base alloys ; Nickel-based superalloys ; Powder beds ; Precipitates ; Rene 41 ; Superalloys ; Tensile properties ; Tensile tests ; Work hardening ; Wrought alloys</subject><ispartof>Journal of alloys and compounds, 2021-03, Vol.858, p.157645, Article 157645</ispartof><rights>2020 Elsevier B.V.</rights><rights>Copyright Elsevier BV Mar 25, 2021</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c337t-80feff3dad25bdd1048a70b522244701c1d360b31f5007f6abedf8441fd44aeb3</citedby><cites>FETCH-LOGICAL-c337t-80feff3dad25bdd1048a70b522244701c1d360b31f5007f6abedf8441fd44aeb3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jallcom.2020.157645$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Atabay, Sıla Ece</creatorcontrib><creatorcontrib>Sanchez-Mata, Oscar</creatorcontrib><creatorcontrib>Muñiz-Lerma, Jose Alberto</creatorcontrib><creatorcontrib>Brochu, Mathieu</creatorcontrib><title>Effect of heat treatment on the microstructure and elevated temperature tensile properties of Rene 41 alloy produced by laser powder bed fusion</title><title>Journal of alloys and compounds</title><description>The microstructure and elevated temperature mechanical properties of a precipitation hardenable Nickel based superalloy, Rene 41, fabricated by laser powder bed fusion followed by two different heat treatment regimes were studied. 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However, the elongation and deformation behaviors were different for each condition. Sub-solvus heat treatment lead to the highest elongation at break with 22% whereas super-solvus heat treatment resulted in the highest work hardening rate during deformation. •Defect free Rene 41 parts produced by LPBF are subjected to sub-solvus/super-solvus solutionizing and aging heat treatment.•Microstructural of the parts were characterized in as built and after two different heat treatment regimes.•Elevated temperature mechanical properties were investigated and correlated with the resulting microstructures.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2020.157645</doi></addata></record>
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subjects Alloys
Carbides
Chemical precipitation
Deformation
Elongation
Grain boundaries
Hardenability
Hardening rate
Heat treating
Heat treatment
High temperature
Laser powder bed fusion
Mechanical properties
Microstructure
Morphology
Nickel base alloys
Nickel-based superalloys
Powder beds
Precipitates
Rene 41
Superalloys
Tensile properties
Tensile tests
Work hardening
Wrought alloys
title Effect of heat treatment on the microstructure and elevated temperature tensile properties of Rene 41 alloy produced by laser powder bed fusion
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