Effect of Synthesis Conditions of Platinum/Reduced Graphene Oxide Nanocomposites on the Electrochemical Behaviors of Cathodes in Dye-Sensitized Solar Cells
This study deals with the preparation and characterization of platinum/reduced graphene oxide (Pt/rGO) as an efficient cathode for dye-sensitized solar cells. Herein, the Pt/rGO material was synthesized by co-precipitation from hexachloroplatinic acid (H 2 PtCl 6 ) and graphene oxide (GO) precursors...
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| Veröffentlicht in: | Journal of electronic materials 2021-03, Vol.50 (3), p.1425-1433 |
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| creator | Dang, C. L. T. Van Le, C. Nguyen, T. D. Le, N. T. T. Nguyen, K. D. Nguyen, M. T. T. Le, H. K. Ho, D. H. Nguyen, H. T. Pham, C. T. L. Hoang, N. M. Mai, P. T. Nguyen, H. H. |
| description | This study deals with the preparation and characterization of platinum/reduced graphene oxide (Pt/rGO) as an efficient cathode for dye-sensitized solar cells. Herein, the Pt/rGO material was synthesized by co-precipitation from hexachloroplatinic acid (H
2
PtCl
6
) and graphene oxide (GO) precursors. The fabrication of cathodes from Pt/rGO composite paste was carried out using screen-printing paste. The electrochemical behaviors of as-prepared cathodes were analyzed by cyclic voltammetry; the performance of fabricated DSSCs was measured by current density–voltage (J-V) curves and electrochemical impedance spectroscopy. The structural characteristics of the Pt/rGO binary composites were confirmed by Fourier-transform infrared spectroscopy, Raman spectroscopy, x-ray diffraction (XRD), and transmission electron microscopy. Empirical data showed that choosing ascorbic acid as a reducing agent at a ratio of 5:1 between ascorbic acid weight and precursor mixture weight, as well as a GO weight percentage of 20% fabricated DSSCs successfully with a conversion efficiency of 6.25%, which was approximately 90% compared to that of pure commercial Pt material. Characterization results indicated that the Pt nanoparticles were homogeneously distributed on the rGO sheets with an average diameter of less than 25 nm. The Pt/rGO hybrid composite is highly expected to replace Pt in the fabrication of cathodes in DSSCs for low-cost DSSC production in the promising future. |
| doi_str_mv | 10.1007/s11664-020-08650-5 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2490402533</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2490402533</sourcerecordid><originalsourceid>FETCH-LOGICAL-c392t-1f575a8b3d1abace2c54f396a106ab9c74c080e3f37ac2a08ab81aef852632753</originalsourceid><addsrcrecordid>eNp9kc1qGzEURkVJoE7SF-hKkLUa_Yxmxstm6rqBkIS6he7EteaqozCWHGlc6rxKX7ZyHOiuK8HlnKPFR8h7wT8IzpurLERdV4xLznhba870GzITulJMtPWPEzLjqhZMS6XfkrOcHzkXWrRiRv4snEM70ejoah-mAbPPtIuh95OPIR_uDyNMPuw2V1-x31ns6TLBdsCA9P6375HeQYg2brYx-wmLEWjJ0MVYsinaATfewkivcYBfPqaXZAfTEPsC-0A_7ZGtMBTZP5f4Ko6QaIfjmC_IqYMx47vX95x8_7z41n1ht_fLm-7jLbNqLicmnG40tGvVC1iDRWl15dS8BsFrWM9tU1neclRONWAl8BbWrQB0rZa1ko1W5-Ty2N2m-LTDPJnHuEuhfGlkNecVl1qpQskjZVPMOaEz2-Q3kPZGcHMYwRxHMGUE8zKCOaTVUcoFDj8x_Uv_x_oL0qaM2Q</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2490402533</pqid></control><display><type>article</type><title>Effect of Synthesis Conditions of Platinum/Reduced Graphene Oxide Nanocomposites on the Electrochemical Behaviors of Cathodes in Dye-Sensitized Solar Cells</title><source>SpringerLink Journals - AutoHoldings</source><creator>Dang, C. L. T. ; Van Le, C. ; Nguyen, T. D. ; Le, N. T. T. ; Nguyen, K. D. ; Nguyen, M. T. T. ; Le, H. K. ; Ho, D. H. ; Nguyen, H. T. ; Pham, C. T. L. ; Hoang, N. M. ; Mai, P. T. ; Nguyen, H. H.</creator><creatorcontrib>Dang, C. L. T. ; Van Le, C. ; Nguyen, T. D. ; Le, N. T. T. ; Nguyen, K. D. ; Nguyen, M. T. T. ; Le, H. K. ; Ho, D. H. ; Nguyen, H. T. ; Pham, C. T. L. ; Hoang, N. M. ; Mai, P. T. ; Nguyen, H. H.</creatorcontrib><description>This study deals with the preparation and characterization of platinum/reduced graphene oxide (Pt/rGO) as an efficient cathode for dye-sensitized solar cells. Herein, the Pt/rGO material was synthesized by co-precipitation from hexachloroplatinic acid (H
2
PtCl
6
) and graphene oxide (GO) precursors. The fabrication of cathodes from Pt/rGO composite paste was carried out using screen-printing paste. The electrochemical behaviors of as-prepared cathodes were analyzed by cyclic voltammetry; the performance of fabricated DSSCs was measured by current density–voltage (J-V) curves and electrochemical impedance spectroscopy. The structural characteristics of the Pt/rGO binary composites were confirmed by Fourier-transform infrared spectroscopy, Raman spectroscopy, x-ray diffraction (XRD), and transmission electron microscopy. Empirical data showed that choosing ascorbic acid as a reducing agent at a ratio of 5:1 between ascorbic acid weight and precursor mixture weight, as well as a GO weight percentage of 20% fabricated DSSCs successfully with a conversion efficiency of 6.25%, which was approximately 90% compared to that of pure commercial Pt material. Characterization results indicated that the Pt nanoparticles were homogeneously distributed on the rGO sheets with an average diameter of less than 25 nm. The Pt/rGO hybrid composite is highly expected to replace Pt in the fabrication of cathodes in DSSCs for low-cost DSSC production in the promising future.</description><identifier>ISSN: 0361-5235</identifier><identifier>EISSN: 1543-186X</identifier><identifier>DOI: 10.1007/s11664-020-08650-5</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Ascorbic acid ; Cathodes ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Diameters ; Dye-sensitized solar cells ; Dyes ; Electrochemical impedance spectroscopy ; Electronics and Microelectronics ; Empirical analysis ; Fourier transforms ; Graphene ; Hybrid composites ; Instrumentation ; Materials Science ; Nanocomposites ; Nanoparticles ; Optical and Electronic Materials ; Original Research Article ; Photovoltaic cells ; Platinum ; Precursors ; Raman spectroscopy ; Reducing agents ; Screen printing ; Solid State Physics ; Spectrum analysis ; Weight</subject><ispartof>Journal of electronic materials, 2021-03, Vol.50 (3), p.1425-1433</ispartof><rights>The Minerals, Metals & Materials Society 2021</rights><rights>The Minerals, Metals & Materials Society 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c392t-1f575a8b3d1abace2c54f396a106ab9c74c080e3f37ac2a08ab81aef852632753</citedby><cites>FETCH-LOGICAL-c392t-1f575a8b3d1abace2c54f396a106ab9c74c080e3f37ac2a08ab81aef852632753</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11664-020-08650-5$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11664-020-08650-5$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Dang, C. L. T.</creatorcontrib><creatorcontrib>Van Le, C.</creatorcontrib><creatorcontrib>Nguyen, T. D.</creatorcontrib><creatorcontrib>Le, N. T. T.</creatorcontrib><creatorcontrib>Nguyen, K. D.</creatorcontrib><creatorcontrib>Nguyen, M. T. T.</creatorcontrib><creatorcontrib>Le, H. K.</creatorcontrib><creatorcontrib>Ho, D. H.</creatorcontrib><creatorcontrib>Nguyen, H. T.</creatorcontrib><creatorcontrib>Pham, C. T. L.</creatorcontrib><creatorcontrib>Hoang, N. M.</creatorcontrib><creatorcontrib>Mai, P. T.</creatorcontrib><creatorcontrib>Nguyen, H. H.</creatorcontrib><title>Effect of Synthesis Conditions of Platinum/Reduced Graphene Oxide Nanocomposites on the Electrochemical Behaviors of Cathodes in Dye-Sensitized Solar Cells</title><title>Journal of electronic materials</title><addtitle>Journal of Elec Materi</addtitle><description>This study deals with the preparation and characterization of platinum/reduced graphene oxide (Pt/rGO) as an efficient cathode for dye-sensitized solar cells. Herein, the Pt/rGO material was synthesized by co-precipitation from hexachloroplatinic acid (H
2
PtCl
6
) and graphene oxide (GO) precursors. The fabrication of cathodes from Pt/rGO composite paste was carried out using screen-printing paste. The electrochemical behaviors of as-prepared cathodes were analyzed by cyclic voltammetry; the performance of fabricated DSSCs was measured by current density–voltage (J-V) curves and electrochemical impedance spectroscopy. The structural characteristics of the Pt/rGO binary composites were confirmed by Fourier-transform infrared spectroscopy, Raman spectroscopy, x-ray diffraction (XRD), and transmission electron microscopy. Empirical data showed that choosing ascorbic acid as a reducing agent at a ratio of 5:1 between ascorbic acid weight and precursor mixture weight, as well as a GO weight percentage of 20% fabricated DSSCs successfully with a conversion efficiency of 6.25%, which was approximately 90% compared to that of pure commercial Pt material. Characterization results indicated that the Pt nanoparticles were homogeneously distributed on the rGO sheets with an average diameter of less than 25 nm. The Pt/rGO hybrid composite is highly expected to replace Pt in the fabrication of cathodes in DSSCs for low-cost DSSC production in the promising future.</description><subject>Ascorbic acid</subject><subject>Cathodes</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Diameters</subject><subject>Dye-sensitized solar cells</subject><subject>Dyes</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Electronics and Microelectronics</subject><subject>Empirical analysis</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>Hybrid composites</subject><subject>Instrumentation</subject><subject>Materials Science</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Optical and Electronic Materials</subject><subject>Original Research Article</subject><subject>Photovoltaic cells</subject><subject>Platinum</subject><subject>Precursors</subject><subject>Raman spectroscopy</subject><subject>Reducing agents</subject><subject>Screen printing</subject><subject>Solid State Physics</subject><subject>Spectrum analysis</subject><subject>Weight</subject><issn>0361-5235</issn><issn>1543-186X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>BENPR</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp9kc1qGzEURkVJoE7SF-hKkLUa_Yxmxstm6rqBkIS6he7EteaqozCWHGlc6rxKX7ZyHOiuK8HlnKPFR8h7wT8IzpurLERdV4xLznhba870GzITulJMtPWPEzLjqhZMS6XfkrOcHzkXWrRiRv4snEM70ejoah-mAbPPtIuh95OPIR_uDyNMPuw2V1-x31ns6TLBdsCA9P6375HeQYg2brYx-wmLEWjJ0MVYsinaATfewkivcYBfPqaXZAfTEPsC-0A_7ZGtMBTZP5f4Ko6QaIfjmC_IqYMx47vX95x8_7z41n1ht_fLm-7jLbNqLicmnG40tGvVC1iDRWl15dS8BsFrWM9tU1neclRONWAl8BbWrQB0rZa1ko1W5-Ty2N2m-LTDPJnHuEuhfGlkNecVl1qpQskjZVPMOaEz2-Q3kPZGcHMYwRxHMGUE8zKCOaTVUcoFDj8x_Uv_x_oL0qaM2Q</recordid><startdate>20210301</startdate><enddate>20210301</enddate><creator>Dang, C. 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L. T. ; Van Le, C. ; Nguyen, T. D. ; Le, N. T. T. ; Nguyen, K. D. ; Nguyen, M. T. T. ; Le, H. K. ; Ho, D. H. ; Nguyen, H. T. ; Pham, C. T. L. ; Hoang, N. M. ; Mai, P. T. ; Nguyen, H. 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L. T.</creatorcontrib><creatorcontrib>Van Le, C.</creatorcontrib><creatorcontrib>Nguyen, T. D.</creatorcontrib><creatorcontrib>Le, N. T. T.</creatorcontrib><creatorcontrib>Nguyen, K. D.</creatorcontrib><creatorcontrib>Nguyen, M. T. T.</creatorcontrib><creatorcontrib>Le, H. K.</creatorcontrib><creatorcontrib>Ho, D. H.</creatorcontrib><creatorcontrib>Nguyen, H. T.</creatorcontrib><creatorcontrib>Pham, C. T. L.</creatorcontrib><creatorcontrib>Hoang, N. M.</creatorcontrib><creatorcontrib>Mai, P. T.</creatorcontrib><creatorcontrib>Nguyen, H. 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L. T.</au><au>Van Le, C.</au><au>Nguyen, T. D.</au><au>Le, N. T. T.</au><au>Nguyen, K. D.</au><au>Nguyen, M. T. T.</au><au>Le, H. K.</au><au>Ho, D. H.</au><au>Nguyen, H. T.</au><au>Pham, C. T. L.</au><au>Hoang, N. M.</au><au>Mai, P. T.</au><au>Nguyen, H. H.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of Synthesis Conditions of Platinum/Reduced Graphene Oxide Nanocomposites on the Electrochemical Behaviors of Cathodes in Dye-Sensitized Solar Cells</atitle><jtitle>Journal of electronic materials</jtitle><stitle>Journal of Elec Materi</stitle><date>2021-03-01</date><risdate>2021</risdate><volume>50</volume><issue>3</issue><spage>1425</spage><epage>1433</epage><pages>1425-1433</pages><issn>0361-5235</issn><eissn>1543-186X</eissn><abstract>This study deals with the preparation and characterization of platinum/reduced graphene oxide (Pt/rGO) as an efficient cathode for dye-sensitized solar cells. Herein, the Pt/rGO material was synthesized by co-precipitation from hexachloroplatinic acid (H
2
PtCl
6
) and graphene oxide (GO) precursors. The fabrication of cathodes from Pt/rGO composite paste was carried out using screen-printing paste. The electrochemical behaviors of as-prepared cathodes were analyzed by cyclic voltammetry; the performance of fabricated DSSCs was measured by current density–voltage (J-V) curves and electrochemical impedance spectroscopy. The structural characteristics of the Pt/rGO binary composites were confirmed by Fourier-transform infrared spectroscopy, Raman spectroscopy, x-ray diffraction (XRD), and transmission electron microscopy. Empirical data showed that choosing ascorbic acid as a reducing agent at a ratio of 5:1 between ascorbic acid weight and precursor mixture weight, as well as a GO weight percentage of 20% fabricated DSSCs successfully with a conversion efficiency of 6.25%, which was approximately 90% compared to that of pure commercial Pt material. Characterization results indicated that the Pt nanoparticles were homogeneously distributed on the rGO sheets with an average diameter of less than 25 nm. The Pt/rGO hybrid composite is highly expected to replace Pt in the fabrication of cathodes in DSSCs for low-cost DSSC production in the promising future.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11664-020-08650-5</doi><tpages>9</tpages></addata></record> |
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| subjects | Ascorbic acid Cathodes Characterization and Evaluation of Materials Chemistry and Materials Science Diameters Dye-sensitized solar cells Dyes Electrochemical impedance spectroscopy Electronics and Microelectronics Empirical analysis Fourier transforms Graphene Hybrid composites Instrumentation Materials Science Nanocomposites Nanoparticles Optical and Electronic Materials Original Research Article Photovoltaic cells Platinum Precursors Raman spectroscopy Reducing agents Screen printing Solid State Physics Spectrum analysis Weight |
| title | Effect of Synthesis Conditions of Platinum/Reduced Graphene Oxide Nanocomposites on the Electrochemical Behaviors of Cathodes in Dye-Sensitized Solar Cells |
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