Research on Nickel(II) Complexes with Aroyl Hydrazones of 5,5-Dimethyl-2,4-Dioxohexanoic Acid Ethyl Ester
Complex compounds of nickel(II) with aroyl hydrazones of 5,5-dimethyl-2,4-dioxohexanoic acid ethyl ester (H 2 L 1 –H 2 L 6 ) are synthesized and studied. The composition and structure of the obtained complex compounds based on these ligands are established by elemental analysis, infrared spectroscop...
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| Veröffentlicht in: | Moscow University chemistry bulletin 2020-11, Vol.75 (6), p.395-401 |
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| container_title | Moscow University chemistry bulletin |
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| creator | Abduraxmonov, S. F. Tursunov, M. A. Umarov, B. B. Ergashov, M. Ya Avezov, K. G. |
| description | Complex compounds of nickel(II) with aroyl hydrazones of 5,5-dimethyl-2,4-dioxohexanoic acid ethyl ester (H
2
L
1
–H
2
L
6
) are synthesized and studied. The composition and structure of the obtained complex compounds based on these ligands are established by elemental analysis, infrared spectroscopy, proton nuclear magnetic resonance spectroscopy, and X-ray diffraction analysis. The full set of the X-ray diffraction data of the NiL
6
⋅ 3Py complex is deposited in the Cambridge Structural Database (CCDC deposit no. 1911468), and it is available on request from the following site:
www.ccdc.cam.ac.uk/data_request/cif |
| doi_str_mv | 10.3103/S0027131420060085 |
| format | Article |
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2
L
1
–H
2
L
6
) are synthesized and studied. The composition and structure of the obtained complex compounds based on these ligands are established by elemental analysis, infrared spectroscopy, proton nuclear magnetic resonance spectroscopy, and X-ray diffraction analysis. The full set of the X-ray diffraction data of the NiL
6
⋅ 3Py complex is deposited in the Cambridge Structural Database (CCDC deposit no. 1911468), and it is available on request from the following site:
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2
L
1
–H
2
L
6
) are synthesized and studied. The composition and structure of the obtained complex compounds based on these ligands are established by elemental analysis, infrared spectroscopy, proton nuclear magnetic resonance spectroscopy, and X-ray diffraction analysis. The full set of the X-ray diffraction data of the NiL
6
⋅ 3Py complex is deposited in the Cambridge Structural Database (CCDC deposit no. 1911468), and it is available on request from the following site:
www.ccdc.cam.ac.uk/data_request/cif</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Complex compounds</subject><subject>Ethyl esters</subject><subject>Hydrazones</subject><subject>Infrared analysis</subject><subject>Nickel</subject><subject>NMR spectroscopy</subject><subject>Spectroscopic analysis</subject><subject>Spectrum analysis</subject><subject>X-ray diffraction</subject><issn>0027-1314</issn><issn>1935-0260</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1UEtLw0AQXkTBWv0B3ha8KDQ6u5tkk2Op1RaKgo9z2O5OTGqarbspNv56Eyp4EE_DzPdiPkLOGVwLBuLmGYBLJljIAWKAJDogA5aKKAAewyEZ9HDQ48fkxPsVQBRzIQekfEKPyumC2po-lPodq8v5_IpO7HpT4Q49_Sybgo6dbSs6a41TX7burjan0SgKbss1NkVbBXwUdovd2QJ3qralpmNdGjrtQTr1DbpTcpSryuPZzxyS17vpy2QWLB7v55PxItCCxU0QgozQLA2TymhkcZ6iEQiCqVDIaBkbbkTIlyI1SirkaaRywDjnQmOSgEzFkFzsfTfOfmzRN9nKbl3dRWY87BiJ7F8fErZnaWe9d5hnG1eulWszBlnfaPan0U7D9xrfces3dL_O_4u-AZwgdj8</recordid><startdate>20201101</startdate><enddate>20201101</enddate><creator>Abduraxmonov, S. F.</creator><creator>Tursunov, M. A.</creator><creator>Umarov, B. B.</creator><creator>Ergashov, M. Ya</creator><creator>Avezov, K. G.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20201101</creationdate><title>Research on Nickel(II) Complexes with Aroyl Hydrazones of 5,5-Dimethyl-2,4-Dioxohexanoic Acid Ethyl Ester</title><author>Abduraxmonov, S. F. ; Tursunov, M. A. ; Umarov, B. B. ; Ergashov, M. Ya ; Avezov, K. G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-4075edbd17adce16f9ed3e031a4375b6d2d342b39da7ae295af0e6f23ce880793</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Complex compounds</topic><topic>Ethyl esters</topic><topic>Hydrazones</topic><topic>Infrared analysis</topic><topic>Nickel</topic><topic>NMR spectroscopy</topic><topic>Spectroscopic analysis</topic><topic>Spectrum analysis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Abduraxmonov, S. F.</creatorcontrib><creatorcontrib>Tursunov, M. A.</creatorcontrib><creatorcontrib>Umarov, B. B.</creatorcontrib><creatorcontrib>Ergashov, M. Ya</creatorcontrib><creatorcontrib>Avezov, K. G.</creatorcontrib><collection>CrossRef</collection><jtitle>Moscow University chemistry bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Abduraxmonov, S. F.</au><au>Tursunov, M. A.</au><au>Umarov, B. B.</au><au>Ergashov, M. Ya</au><au>Avezov, K. G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Research on Nickel(II) Complexes with Aroyl Hydrazones of 5,5-Dimethyl-2,4-Dioxohexanoic Acid Ethyl Ester</atitle><jtitle>Moscow University chemistry bulletin</jtitle><stitle>Moscow Univ. Chem. Bull</stitle><date>2020-11-01</date><risdate>2020</risdate><volume>75</volume><issue>6</issue><spage>395</spage><epage>401</epage><pages>395-401</pages><issn>0027-1314</issn><eissn>1935-0260</eissn><abstract>Complex compounds of nickel(II) with aroyl hydrazones of 5,5-dimethyl-2,4-dioxohexanoic acid ethyl ester (H
2
L
1
–H
2
L
6
) are synthesized and studied. The composition and structure of the obtained complex compounds based on these ligands are established by elemental analysis, infrared spectroscopy, proton nuclear magnetic resonance spectroscopy, and X-ray diffraction analysis. The full set of the X-ray diffraction data of the NiL
6
⋅ 3Py complex is deposited in the Cambridge Structural Database (CCDC deposit no. 1911468), and it is available on request from the following site:
www.ccdc.cam.ac.uk/data_request/cif</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.3103/S0027131420060085</doi><tpages>7</tpages></addata></record> |
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| ispartof | Moscow University chemistry bulletin, 2020-11, Vol.75 (6), p.395-401 |
| issn | 0027-1314 1935-0260 |
| language | eng |
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| source | SpringerNature Journals |
| subjects | Chemistry Chemistry and Materials Science Chemistry/Food Science Complex compounds Ethyl esters Hydrazones Infrared analysis Nickel NMR spectroscopy Spectroscopic analysis Spectrum analysis X-ray diffraction |
| title | Research on Nickel(II) Complexes with Aroyl Hydrazones of 5,5-Dimethyl-2,4-Dioxohexanoic Acid Ethyl Ester |
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