XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches
Cobalt doped Zinc Oxide (Zn1-xCoxO) (x = 0.03) nanoparticles have been synthesized by chemical co-precipitation method at room temperature and characterized by X-ray diffraction (XRD) study. The XRD pattern indicates that Co doped ZnO NPs are with hexagonal wurtzite geometry and diffraction peaks ge...
Gespeichert in:
| Veröffentlicht in: | Physica. B, Condensed matter Condensed matter, 2020-10, Vol.595, p.412342, Article 412342 |
|---|---|
| Hauptverfasser: | , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | |
| container_start_page | 412342 |
| container_title | Physica. B, Condensed matter |
| container_volume | 595 |
| creator | Shunmuga Sundaram, P. Sangeetha, T. Rajakarthihan, S. Vijayalaksmi, R. Elangovan, A. Arivazhagan, G. |
| description | Cobalt doped Zinc Oxide (Zn1-xCoxO) (x = 0.03) nanoparticles have been synthesized by chemical co-precipitation method at room temperature and characterized by X-ray diffraction (XRD) study. The XRD pattern indicates that Co doped ZnO NPs are with hexagonal wurtzite geometry and diffraction peaks get shifted to higher angles which is the characteristic influence of dopant Co that has an ionic radius smaller than the host cation. The true values of lattice constants have been calculated using Nelson–Riley Function. Crystallite size calculated using Scherrer formula has been compared with that estimated by uniform deformation (UDM), uniform stress deformation (USDM) and uniform deformation energy density (UDEDM) models of Williamson – Hall method, and also by size-strain plot (SSP) method. The lattice strain has also been calculated. The surface morphology and elemental analysis of the product have been characterized by field emission scanning electron microscopy (FESEM) and energy dispersive (EDAX) spectra. |
| doi_str_mv | 10.1016/j.physb.2020.412342 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2478622039</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0921452620303537</els_id><sourcerecordid>2478622039</sourcerecordid><originalsourceid>FETCH-LOGICAL-c331t-fcc8315db067ac6b78206acb90e3f72eb990bcbcedb02624489c16f4f11824a73</originalsourceid><addsrcrecordid>eNp9kctOAyEYhYnRxFp9Ajckrqdymc7FxIWpl5o0MTEa3RFgmJSGAgJjbB_E55Va17L5WZzvHPgPAOcYTTDC1eVq4pebKCYEETQpMaElOQAj3NS0IJhOD8EItQQX5ZRUx-AkxhXKB9d4BL7fn29hTGGQaQjc5OvQaRWhs1A6wU2CnfOqg1ttJXRfulPQcus8D0lLk4VxY9NSRb3NIrHJkA9Kaq8TTzqbrFVauu4KvmljNF9HZ4s5NwZy28EdVORsri30xiXIvQ-Oy2x3Co56bqI6-5tj8Hp_9zKbF4unh8fZzaKQlOJU9FI2FE87gaqay0rUDUEVl6JFivY1UaJtkZBCqqwgFSnLppW46sse44aUvKZjcLH3zcEfg4qJrdwQbI5kpKybihBE26yie5UMLsageuaDXvOwYRixXQFsxX4LYLsC2L6ATF3vKZU_8KlVYFFqZfNjdF5RYp3T__I_VtyTzA</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2478622039</pqid></control><display><type>article</type><title>XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches</title><source>ScienceDirect Journals (5 years ago - present)</source><creator>Shunmuga Sundaram, P. ; Sangeetha, T. ; Rajakarthihan, S. ; Vijayalaksmi, R. ; Elangovan, A. ; Arivazhagan, G.</creator><creatorcontrib>Shunmuga Sundaram, P. ; Sangeetha, T. ; Rajakarthihan, S. ; Vijayalaksmi, R. ; Elangovan, A. ; Arivazhagan, G.</creatorcontrib><description>Cobalt doped Zinc Oxide (Zn1-xCoxO) (x = 0.03) nanoparticles have been synthesized by chemical co-precipitation method at room temperature and characterized by X-ray diffraction (XRD) study. The XRD pattern indicates that Co doped ZnO NPs are with hexagonal wurtzite geometry and diffraction peaks get shifted to higher angles which is the characteristic influence of dopant Co that has an ionic radius smaller than the host cation. The true values of lattice constants have been calculated using Nelson–Riley Function. Crystallite size calculated using Scherrer formula has been compared with that estimated by uniform deformation (UDM), uniform stress deformation (USDM) and uniform deformation energy density (UDEDM) models of Williamson – Hall method, and also by size-strain plot (SSP) method. The lattice strain has also been calculated. The surface morphology and elemental analysis of the product have been characterized by field emission scanning electron microscopy (FESEM) and energy dispersive (EDAX) spectra.</description><identifier>ISSN: 0921-4526</identifier><identifier>EISSN: 1873-2135</identifier><identifier>DOI: 10.1016/j.physb.2020.412342</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Angles (geometry) ; Chemical precipitation ; Chemical synthesis ; Co-precipitation ; Co:ZnO Nanoparticles ; Cobalt ; Coprecipitation ; Crystallites ; Deformation ; Diffraction ; Diffraction patterns ; Emission analysis ; Field emission microscopy ; Flux density ; Lattice parameters ; Lattice strain ; Mathematical morphology ; Nanoparticles ; Nelson-Riley plot ; Room temperature ; Size-strain plot ; Studies ; Wurtzite ; W–H Analysis ; X-ray diffraction ; Zinc oxide ; Zinc oxides</subject><ispartof>Physica. B, Condensed matter, 2020-10, Vol.595, p.412342, Article 412342</ispartof><rights>2020 Elsevier B.V.</rights><rights>Copyright Elsevier BV Oct 15, 2020</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c331t-fcc8315db067ac6b78206acb90e3f72eb990bcbcedb02624489c16f4f11824a73</citedby><cites>FETCH-LOGICAL-c331t-fcc8315db067ac6b78206acb90e3f72eb990bcbcedb02624489c16f4f11824a73</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.physb.2020.412342$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Shunmuga Sundaram, P.</creatorcontrib><creatorcontrib>Sangeetha, T.</creatorcontrib><creatorcontrib>Rajakarthihan, S.</creatorcontrib><creatorcontrib>Vijayalaksmi, R.</creatorcontrib><creatorcontrib>Elangovan, A.</creatorcontrib><creatorcontrib>Arivazhagan, G.</creatorcontrib><title>XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches</title><title>Physica. B, Condensed matter</title><description>Cobalt doped Zinc Oxide (Zn1-xCoxO) (x = 0.03) nanoparticles have been synthesized by chemical co-precipitation method at room temperature and characterized by X-ray diffraction (XRD) study. The XRD pattern indicates that Co doped ZnO NPs are with hexagonal wurtzite geometry and diffraction peaks get shifted to higher angles which is the characteristic influence of dopant Co that has an ionic radius smaller than the host cation. The true values of lattice constants have been calculated using Nelson–Riley Function. Crystallite size calculated using Scherrer formula has been compared with that estimated by uniform deformation (UDM), uniform stress deformation (USDM) and uniform deformation energy density (UDEDM) models of Williamson – Hall method, and also by size-strain plot (SSP) method. The lattice strain has also been calculated. The surface morphology and elemental analysis of the product have been characterized by field emission scanning electron microscopy (FESEM) and energy dispersive (EDAX) spectra.</description><subject>Angles (geometry)</subject><subject>Chemical precipitation</subject><subject>Chemical synthesis</subject><subject>Co-precipitation</subject><subject>Co:ZnO Nanoparticles</subject><subject>Cobalt</subject><subject>Coprecipitation</subject><subject>Crystallites</subject><subject>Deformation</subject><subject>Diffraction</subject><subject>Diffraction patterns</subject><subject>Emission analysis</subject><subject>Field emission microscopy</subject><subject>Flux density</subject><subject>Lattice parameters</subject><subject>Lattice strain</subject><subject>Mathematical morphology</subject><subject>Nanoparticles</subject><subject>Nelson-Riley plot</subject><subject>Room temperature</subject><subject>Size-strain plot</subject><subject>Studies</subject><subject>Wurtzite</subject><subject>W–H Analysis</subject><subject>X-ray diffraction</subject><subject>Zinc oxide</subject><subject>Zinc oxides</subject><issn>0921-4526</issn><issn>1873-2135</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kctOAyEYhYnRxFp9Ajckrqdymc7FxIWpl5o0MTEa3RFgmJSGAgJjbB_E55Va17L5WZzvHPgPAOcYTTDC1eVq4pebKCYEETQpMaElOQAj3NS0IJhOD8EItQQX5ZRUx-AkxhXKB9d4BL7fn29hTGGQaQjc5OvQaRWhs1A6wU2CnfOqg1ttJXRfulPQcus8D0lLk4VxY9NSRb3NIrHJkA9Kaq8TTzqbrFVauu4KvmljNF9HZ4s5NwZy28EdVORsri30xiXIvQ-Oy2x3Co56bqI6-5tj8Hp_9zKbF4unh8fZzaKQlOJU9FI2FE87gaqay0rUDUEVl6JFivY1UaJtkZBCqqwgFSnLppW46sse44aUvKZjcLH3zcEfg4qJrdwQbI5kpKybihBE26yie5UMLsageuaDXvOwYRixXQFsxX4LYLsC2L6ATF3vKZU_8KlVYFFqZfNjdF5RYp3T__I_VtyTzA</recordid><startdate>20201015</startdate><enddate>20201015</enddate><creator>Shunmuga Sundaram, P.</creator><creator>Sangeetha, T.</creator><creator>Rajakarthihan, S.</creator><creator>Vijayalaksmi, R.</creator><creator>Elangovan, A.</creator><creator>Arivazhagan, G.</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20201015</creationdate><title>XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches</title><author>Shunmuga Sundaram, P. ; Sangeetha, T. ; Rajakarthihan, S. ; Vijayalaksmi, R. ; Elangovan, A. ; Arivazhagan, G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c331t-fcc8315db067ac6b78206acb90e3f72eb990bcbcedb02624489c16f4f11824a73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Angles (geometry)</topic><topic>Chemical precipitation</topic><topic>Chemical synthesis</topic><topic>Co-precipitation</topic><topic>Co:ZnO Nanoparticles</topic><topic>Cobalt</topic><topic>Coprecipitation</topic><topic>Crystallites</topic><topic>Deformation</topic><topic>Diffraction</topic><topic>Diffraction patterns</topic><topic>Emission analysis</topic><topic>Field emission microscopy</topic><topic>Flux density</topic><topic>Lattice parameters</topic><topic>Lattice strain</topic><topic>Mathematical morphology</topic><topic>Nanoparticles</topic><topic>Nelson-Riley plot</topic><topic>Room temperature</topic><topic>Size-strain plot</topic><topic>Studies</topic><topic>Wurtzite</topic><topic>W–H Analysis</topic><topic>X-ray diffraction</topic><topic>Zinc oxide</topic><topic>Zinc oxides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Shunmuga Sundaram, P.</creatorcontrib><creatorcontrib>Sangeetha, T.</creatorcontrib><creatorcontrib>Rajakarthihan, S.</creatorcontrib><creatorcontrib>Vijayalaksmi, R.</creatorcontrib><creatorcontrib>Elangovan, A.</creatorcontrib><creatorcontrib>Arivazhagan, G.</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Physica. B, Condensed matter</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Shunmuga Sundaram, P.</au><au>Sangeetha, T.</au><au>Rajakarthihan, S.</au><au>Vijayalaksmi, R.</au><au>Elangovan, A.</au><au>Arivazhagan, G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches</atitle><jtitle>Physica. B, Condensed matter</jtitle><date>2020-10-15</date><risdate>2020</risdate><volume>595</volume><spage>412342</spage><pages>412342-</pages><artnum>412342</artnum><issn>0921-4526</issn><eissn>1873-2135</eissn><abstract>Cobalt doped Zinc Oxide (Zn1-xCoxO) (x = 0.03) nanoparticles have been synthesized by chemical co-precipitation method at room temperature and characterized by X-ray diffraction (XRD) study. The XRD pattern indicates that Co doped ZnO NPs are with hexagonal wurtzite geometry and diffraction peaks get shifted to higher angles which is the characteristic influence of dopant Co that has an ionic radius smaller than the host cation. The true values of lattice constants have been calculated using Nelson–Riley Function. Crystallite size calculated using Scherrer formula has been compared with that estimated by uniform deformation (UDM), uniform stress deformation (USDM) and uniform deformation energy density (UDEDM) models of Williamson – Hall method, and also by size-strain plot (SSP) method. The lattice strain has also been calculated. The surface morphology and elemental analysis of the product have been characterized by field emission scanning electron microscopy (FESEM) and energy dispersive (EDAX) spectra.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.physb.2020.412342</doi></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0921-4526 |
| ispartof | Physica. B, Condensed matter, 2020-10, Vol.595, p.412342, Article 412342 |
| issn | 0921-4526 1873-2135 |
| language | eng |
| recordid | cdi_proquest_journals_2478622039 |
| source | ScienceDirect Journals (5 years ago - present) |
| subjects | Angles (geometry) Chemical precipitation Chemical synthesis Co-precipitation Co:ZnO Nanoparticles Cobalt Coprecipitation Crystallites Deformation Diffraction Diffraction patterns Emission analysis Field emission microscopy Flux density Lattice parameters Lattice strain Mathematical morphology Nanoparticles Nelson-Riley plot Room temperature Size-strain plot Studies Wurtzite W–H Analysis X-ray diffraction Zinc oxide Zinc oxides |
| title | XRD structural studies on cobalt doped zinc oxide nanoparticles synthesized by coprecipitation method: Williamson-Hall and size-strain plot approaches |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-06T22%3A53%3A43IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=XRD%20structural%20studies%20on%20cobalt%20doped%20zinc%20oxide%20nanoparticles%20synthesized%20by%20coprecipitation%20method:%20Williamson-Hall%20and%20size-strain%20plot%20approaches&rft.jtitle=Physica.%20B,%20Condensed%20matter&rft.au=Shunmuga%20Sundaram,%20P.&rft.date=2020-10-15&rft.volume=595&rft.spage=412342&rft.pages=412342-&rft.artnum=412342&rft.issn=0921-4526&rft.eissn=1873-2135&rft_id=info:doi/10.1016/j.physb.2020.412342&rft_dat=%3Cproquest_cross%3E2478622039%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2478622039&rft_id=info:pmid/&rft_els_id=S0921452620303537&rfr_iscdi=true |