Synthesis of YB2C2 by high‐energy ball milling and reactive spark plasma sintering
X‐ray pure yttrium diborodicarbide (YB2C2) was synthesized for the first time via modified spark plasma sintering (SPS) using Y2O3, B4C, and carbon as starting materials. Homogeneous intermixing of the raw powder by high energy ball milling (HEBM) promoted the formation of YB2C2 powder with layered...
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| Veröffentlicht in: | Journal of the American Ceramic Society 2021-03, Vol.104 (3), p.1229-1236 |
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| container_title | Journal of the American Ceramic Society |
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| creator | Nguyen, Van‐Quyet Kim, Jun‐Seop Lee, Sea‐Hoon |
| description | X‐ray pure yttrium diborodicarbide (YB2C2) was synthesized for the first time via modified spark plasma sintering (SPS) using Y2O3, B4C, and carbon as starting materials. Homogeneous intermixing of the raw powder by high energy ball milling (HEBM) promoted the formation of YB2C2 powder with layered structure by boro/carbo‐thermal reduction. The average particle size of the synthesized powder at an optimum synthesis temperature (1625℃) was 568 nm. Small amount of YB2C was formed by consuming YB4 at and above 1625°C. The metal basis purity of the synthesized YB2C2 powder was 99.84%. X‐ray pure YB2C2 was obtained by densifying the synthesized YB2C2 powder at 1900°C for 60 minutes at a pressure of 80 MPa using SPS. This study reports a simple method for the fabrication of X‐ray pure rare earth metal diborodicarbides (ReB2C2). |
| doi_str_mv | 10.1111/jace.17524 |
| format | Article |
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Homogeneous intermixing of the raw powder by high energy ball milling (HEBM) promoted the formation of YB2C2 powder with layered structure by boro/carbo‐thermal reduction. The average particle size of the synthesized powder at an optimum synthesis temperature (1625℃) was 568 nm. Small amount of YB2C was formed by consuming YB4 at and above 1625°C. The metal basis purity of the synthesized YB2C2 powder was 99.84%. X‐ray pure YB2C2 was obtained by densifying the synthesized YB2C2 powder at 1900°C for 60 minutes at a pressure of 80 MPa using SPS. This study reports a simple method for the fabrication of X‐ray pure rare earth metal diborodicarbides (ReB2C2).</description><identifier>ISSN: 0002-7820</identifier><identifier>EISSN: 1551-2916</identifier><identifier>DOI: 10.1111/jace.17524</identifier><language>eng</language><publisher>Columbus: Wiley Subscription Services, Inc</publisher><subject>Ball milling ; Boron carbide ; high energy ball milling ; Plasma sintering ; powder ; Rare earth elements ; Spark plasma sintering ; Synthesis ; Thermal reduction ; Yttrium ; yttrium diborodicarbides ; Yttrium oxide</subject><ispartof>Journal of the American Ceramic Society, 2021-03, Vol.104 (3), p.1229-1236</ispartof><rights>2020 American Ceramic Society (ACERS)</rights><rights>2021 American Ceramic Society</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><orcidid>0000-0001-7783-9865 ; 0000-0002-7276-3264</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Fjace.17524$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Fjace.17524$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids></links><search><creatorcontrib>Nguyen, Van‐Quyet</creatorcontrib><creatorcontrib>Kim, Jun‐Seop</creatorcontrib><creatorcontrib>Lee, Sea‐Hoon</creatorcontrib><title>Synthesis of YB2C2 by high‐energy ball milling and reactive spark plasma sintering</title><title>Journal of the American Ceramic Society</title><description>X‐ray pure yttrium diborodicarbide (YB2C2) was synthesized for the first time via modified spark plasma sintering (SPS) using Y2O3, B4C, and carbon as starting materials. Homogeneous intermixing of the raw powder by high energy ball milling (HEBM) promoted the formation of YB2C2 powder with layered structure by boro/carbo‐thermal reduction. The average particle size of the synthesized powder at an optimum synthesis temperature (1625℃) was 568 nm. Small amount of YB2C was formed by consuming YB4 at and above 1625°C. The metal basis purity of the synthesized YB2C2 powder was 99.84%. X‐ray pure YB2C2 was obtained by densifying the synthesized YB2C2 powder at 1900°C for 60 minutes at a pressure of 80 MPa using SPS. This study reports a simple method for the fabrication of X‐ray pure rare earth metal diborodicarbides (ReB2C2).</description><subject>Ball milling</subject><subject>Boron carbide</subject><subject>high energy ball milling</subject><subject>Plasma sintering</subject><subject>powder</subject><subject>Rare earth elements</subject><subject>Spark plasma sintering</subject><subject>Synthesis</subject><subject>Thermal reduction</subject><subject>Yttrium</subject><subject>yttrium diborodicarbides</subject><subject>Yttrium oxide</subject><issn>0002-7820</issn><issn>1551-2916</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNotkE1OwzAQRi0EEqWw4QSWWKfYjp3EyxKVAqrEgrJgZTn-SV3cNNgpKDuOwBk5CWnLbGZGevo-6QFwjdEED3O7lspMcM4IPQEjzBhOCMfZKRghhEiSFwSdg4sY18OLeUFHYPnSN93KRBfh1sK3O1ISWPVw5erV7_ePaUyoe1hJ7-HGee-aGspGw2Ck6tyngbGV4R22XsaNhNE1nQkDcwnOrPTRXP3vMXi9ny3Lh2TxPH8sp4ukJhmhSZFyKhUnldWskCS3ulIZowoZjrS2lBQ5xpojUxGtpGRW8awglCGdWVVJno7BzTG3DduPnYmdWG93oRkqBaF5mjOa8Xyg8JH6ct70og1uI0MvMBJ7ZWKvTByUiadpOTtc6R8uRmI9</recordid><startdate>202103</startdate><enddate>202103</enddate><creator>Nguyen, Van‐Quyet</creator><creator>Kim, Jun‐Seop</creator><creator>Lee, Sea‐Hoon</creator><general>Wiley Subscription Services, Inc</general><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0001-7783-9865</orcidid><orcidid>https://orcid.org/0000-0002-7276-3264</orcidid></search><sort><creationdate>202103</creationdate><title>Synthesis of YB2C2 by high‐energy ball milling and reactive spark plasma sintering</title><author>Nguyen, Van‐Quyet ; Kim, Jun‐Seop ; Lee, Sea‐Hoon</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g2624-8394ac92bfd58a27fdbc654c0e90ddf428711d90eb2dcaa5fc9682450d6fcba93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Ball milling</topic><topic>Boron carbide</topic><topic>high energy ball milling</topic><topic>Plasma sintering</topic><topic>powder</topic><topic>Rare earth elements</topic><topic>Spark plasma sintering</topic><topic>Synthesis</topic><topic>Thermal reduction</topic><topic>Yttrium</topic><topic>yttrium diborodicarbides</topic><topic>Yttrium oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nguyen, Van‐Quyet</creatorcontrib><creatorcontrib>Kim, Jun‐Seop</creatorcontrib><creatorcontrib>Lee, Sea‐Hoon</creatorcontrib><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of the American Ceramic Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nguyen, Van‐Quyet</au><au>Kim, Jun‐Seop</au><au>Lee, Sea‐Hoon</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of YB2C2 by high‐energy ball milling and reactive spark plasma sintering</atitle><jtitle>Journal of the American Ceramic Society</jtitle><date>2021-03</date><risdate>2021</risdate><volume>104</volume><issue>3</issue><spage>1229</spage><epage>1236</epage><pages>1229-1236</pages><issn>0002-7820</issn><eissn>1551-2916</eissn><abstract>X‐ray pure yttrium diborodicarbide (YB2C2) was synthesized for the first time via modified spark plasma sintering (SPS) using Y2O3, B4C, and carbon as starting materials. Homogeneous intermixing of the raw powder by high energy ball milling (HEBM) promoted the formation of YB2C2 powder with layered structure by boro/carbo‐thermal reduction. The average particle size of the synthesized powder at an optimum synthesis temperature (1625℃) was 568 nm. Small amount of YB2C was formed by consuming YB4 at and above 1625°C. The metal basis purity of the synthesized YB2C2 powder was 99.84%. X‐ray pure YB2C2 was obtained by densifying the synthesized YB2C2 powder at 1900°C for 60 minutes at a pressure of 80 MPa using SPS. This study reports a simple method for the fabrication of X‐ray pure rare earth metal diborodicarbides (ReB2C2).</abstract><cop>Columbus</cop><pub>Wiley Subscription Services, Inc</pub><doi>10.1111/jace.17524</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0001-7783-9865</orcidid><orcidid>https://orcid.org/0000-0002-7276-3264</orcidid></addata></record> |
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| language | eng |
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| subjects | Ball milling Boron carbide high energy ball milling Plasma sintering powder Rare earth elements Spark plasma sintering Synthesis Thermal reduction Yttrium yttrium diborodicarbides Yttrium oxide |
| title | Synthesis of YB2C2 by high‐energy ball milling and reactive spark plasma sintering |
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