Preparation and characterization of electrode from annealed nano-diamond particles with boric acid for anodic oxidation process
This work is reported the incorporation of boron on diamond particles by annealing process using boric acid as boron source at different temperatures 700, 900, and 1100 °C. Moreover, the electrodes were prepared from pristine diamond (P-ND) and annealed diamond particles (A-ND). Raman, XRD, and FTIR...
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| Veröffentlicht in: | Electrochimica acta 2020-12, Vol.362, p.137221, Article 137221 |
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| container_title | Electrochimica acta |
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| creator | Ajeel, Mohammed A. Mahdi, Rahman Ismael Aroua, Mohamed Kheireddine Taeib Abd Majid, WH |
| description | This work is reported the incorporation of boron on diamond particles by annealing process using boric acid as boron source at different temperatures 700, 900, and 1100 °C. Moreover, the electrodes were prepared from pristine diamond (P-ND) and annealed diamond particles (A-ND). Raman, XRD, and FTIR techniques were used to investigate the effect of doping boron in diamond particles. Analysis of the results showed that the boron doping in diamond particles accord at 1100 °C. Cyclic voltammeter and impedance techniques were used to characterize the diamond anode properties after (P-ND) and before (A-ND) annealing treatment. A-ND electrode demonstrated high oxidation power which is suitable for anodic oxidation process. Moreover, reactivity of A-ND anode was higher than that of P-ND anode as a consequence of the presence of boron in the diamond particles of A-ND electrode. 2-chlorophenol was selected as pollutant to investigate the performance of A-ND anode for electro-degradation treatment. The result shows the removal rate of 2-chlorophenol attained 98% after 6 h. |
| doi_str_mv | 10.1016/j.electacta.2020.137221 |
| format | Article |
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Moreover, the electrodes were prepared from pristine diamond (P-ND) and annealed diamond particles (A-ND). Raman, XRD, and FTIR techniques were used to investigate the effect of doping boron in diamond particles. Analysis of the results showed that the boron doping in diamond particles accord at 1100 °C. Cyclic voltammeter and impedance techniques were used to characterize the diamond anode properties after (P-ND) and before (A-ND) annealing treatment. A-ND electrode demonstrated high oxidation power which is suitable for anodic oxidation process. Moreover, reactivity of A-ND anode was higher than that of P-ND anode as a consequence of the presence of boron in the diamond particles of A-ND electrode. 2-chlorophenol was selected as pollutant to investigate the performance of A-ND anode for electro-degradation treatment. The result shows the removal rate of 2-chlorophenol attained 98% after 6 h.</description><identifier>ISSN: 0013-4686</identifier><identifier>EISSN: 1873-3859</identifier><identifier>DOI: 10.1016/j.electacta.2020.137221</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>2-Chlorophenol degradation ; Annealing ; Annealing treatment ; Anodes ; Anodizing ; Boron ; Diamond ; Diamonds ; Doping ; Electrochemical oxidation ; Electrodes ; Knives ; Nanostructure ; Ortho-chlorophenol ; Oxidation ; Pollutants</subject><ispartof>Electrochimica acta, 2020-12, Vol.362, p.137221, Article 137221</ispartof><rights>2020</rights><rights>Copyright Elsevier BV Dec 1, 2020</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c343t-fd4aa27f2e59fd75b0357ee011df5fe34757dbdd0d9d912e2072065c32bbc6a03</citedby><cites>FETCH-LOGICAL-c343t-fd4aa27f2e59fd75b0357ee011df5fe34757dbdd0d9d912e2072065c32bbc6a03</cites><orcidid>0000-0001-8273-5892 ; 0000-0002-9388-5439</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.electacta.2020.137221$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3536,27903,27904,45974</link.rule.ids></links><search><creatorcontrib>Ajeel, Mohammed A.</creatorcontrib><creatorcontrib>Mahdi, Rahman Ismael</creatorcontrib><creatorcontrib>Aroua, Mohamed Kheireddine Taeib</creatorcontrib><creatorcontrib>Abd Majid, WH</creatorcontrib><title>Preparation and characterization of electrode from annealed nano-diamond particles with boric acid for anodic oxidation process</title><title>Electrochimica acta</title><description>This work is reported the incorporation of boron on diamond particles by annealing process using boric acid as boron source at different temperatures 700, 900, and 1100 °C. Moreover, the electrodes were prepared from pristine diamond (P-ND) and annealed diamond particles (A-ND). Raman, XRD, and FTIR techniques were used to investigate the effect of doping boron in diamond particles. Analysis of the results showed that the boron doping in diamond particles accord at 1100 °C. Cyclic voltammeter and impedance techniques were used to characterize the diamond anode properties after (P-ND) and before (A-ND) annealing treatment. A-ND electrode demonstrated high oxidation power which is suitable for anodic oxidation process. Moreover, reactivity of A-ND anode was higher than that of P-ND anode as a consequence of the presence of boron in the diamond particles of A-ND electrode. 2-chlorophenol was selected as pollutant to investigate the performance of A-ND anode for electro-degradation treatment. The result shows the removal rate of 2-chlorophenol attained 98% after 6 h.</description><subject>2-Chlorophenol degradation</subject><subject>Annealing</subject><subject>Annealing treatment</subject><subject>Anodes</subject><subject>Anodizing</subject><subject>Boron</subject><subject>Diamond</subject><subject>Diamonds</subject><subject>Doping</subject><subject>Electrochemical oxidation</subject><subject>Electrodes</subject><subject>Knives</subject><subject>Nanostructure</subject><subject>Ortho-chlorophenol</subject><subject>Oxidation</subject><subject>Pollutants</subject><issn>0013-4686</issn><issn>1873-3859</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNqFkEtLAzEQx4MoWKufwYDnrXk0m_ZYii8Q9KDnkM1MaJZ2U5Otr4tf3dQVr0IgzPB_MD9CzjmbcMbry3aCa3S9LW8imChbqYXgB2TEZ1pWcqbmh2TEGJfVtJ7Vx-Qk55YxpmvNRuTrMeHWJtuH2FHbAXWrMrkeU_gcltHTn4IUAalPcVNkHdo1Au1sFysIdhOLsaT0wa0x07fQr2gTU3DUugDUx1Q8Ecoc3wMMsdsUHeZ8So68XWc8-_3H5Pn66ml5W90_3NwtF_eVk1PZVx6m1grtBaq5B60aJpVGZJyDVx7lVCsNDQCDOcy5QMG0YLVyUjSNqy2TY3Ix5Jbelx3m3rRxl7pSaUTBImdCKV1UelC5FHNO6M02hY1NH4Yzs6dtWvNH2-xpm4F2cS4GJ5YjXgMmk13AziGEVPQGYvg34xu7JI-j</recordid><startdate>20201201</startdate><enddate>20201201</enddate><creator>Ajeel, Mohammed A.</creator><creator>Mahdi, Rahman Ismael</creator><creator>Aroua, Mohamed Kheireddine Taeib</creator><creator>Abd Majid, WH</creator><general>Elsevier Ltd</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0001-8273-5892</orcidid><orcidid>https://orcid.org/0000-0002-9388-5439</orcidid></search><sort><creationdate>20201201</creationdate><title>Preparation and characterization of electrode from annealed nano-diamond particles with boric acid for anodic oxidation process</title><author>Ajeel, Mohammed A. ; Mahdi, Rahman Ismael ; Aroua, Mohamed Kheireddine Taeib ; Abd Majid, WH</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c343t-fd4aa27f2e59fd75b0357ee011df5fe34757dbdd0d9d912e2072065c32bbc6a03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>2-Chlorophenol degradation</topic><topic>Annealing</topic><topic>Annealing treatment</topic><topic>Anodes</topic><topic>Anodizing</topic><topic>Boron</topic><topic>Diamond</topic><topic>Diamonds</topic><topic>Doping</topic><topic>Electrochemical oxidation</topic><topic>Electrodes</topic><topic>Knives</topic><topic>Nanostructure</topic><topic>Ortho-chlorophenol</topic><topic>Oxidation</topic><topic>Pollutants</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ajeel, Mohammed A.</creatorcontrib><creatorcontrib>Mahdi, Rahman Ismael</creatorcontrib><creatorcontrib>Aroua, Mohamed Kheireddine Taeib</creatorcontrib><creatorcontrib>Abd Majid, WH</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Electrochimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ajeel, Mohammed A.</au><au>Mahdi, Rahman Ismael</au><au>Aroua, Mohamed Kheireddine Taeib</au><au>Abd Majid, WH</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and characterization of electrode from annealed nano-diamond particles with boric acid for anodic oxidation process</atitle><jtitle>Electrochimica acta</jtitle><date>2020-12-01</date><risdate>2020</risdate><volume>362</volume><spage>137221</spage><pages>137221-</pages><artnum>137221</artnum><issn>0013-4686</issn><eissn>1873-3859</eissn><abstract>This work is reported the incorporation of boron on diamond particles by annealing process using boric acid as boron source at different temperatures 700, 900, and 1100 °C. Moreover, the electrodes were prepared from pristine diamond (P-ND) and annealed diamond particles (A-ND). Raman, XRD, and FTIR techniques were used to investigate the effect of doping boron in diamond particles. Analysis of the results showed that the boron doping in diamond particles accord at 1100 °C. Cyclic voltammeter and impedance techniques were used to characterize the diamond anode properties after (P-ND) and before (A-ND) annealing treatment. A-ND electrode demonstrated high oxidation power which is suitable for anodic oxidation process. Moreover, reactivity of A-ND anode was higher than that of P-ND anode as a consequence of the presence of boron in the diamond particles of A-ND electrode. 2-chlorophenol was selected as pollutant to investigate the performance of A-ND anode for electro-degradation treatment. 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| subjects | 2-Chlorophenol degradation Annealing Annealing treatment Anodes Anodizing Boron Diamond Diamonds Doping Electrochemical oxidation Electrodes Knives Nanostructure Ortho-chlorophenol Oxidation Pollutants |
| title | Preparation and characterization of electrode from annealed nano-diamond particles with boric acid for anodic oxidation process |
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