Microstructure and mechanical behavior of as-built and heat-treated Ti–6Al–7Nb produced by laser powder bed fusion
Ti–6Al–4V and Ti–6Al–7Nb were manufactured with laser powder bed fusion (LPBF). Microstructural comparison study between Ti–6Al–4V and Ti6Al–6Nb was used to understand processability similarities between two different titanium alloys. Quantitative similarities between two alloys revealed that Ti–6Al...
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Veröffentlicht in: | Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2020-08, Vol.793, p.139978, Article 139978 |
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container_title | Materials science & engineering. A, Structural materials : properties, microstructure and processing |
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creator | Xu, Chao Sikan, Fatih Atabay, Sila Ece Muñiz-Lerma, Jose Alberto Sanchez-Mata, Oscar Wang, Xianglong Brochu, Mathieu |
description | Ti–6Al–4V and Ti–6Al–7Nb were manufactured with laser powder bed fusion (LPBF). Microstructural comparison study between Ti–6Al–4V and Ti6Al–6Nb was used to understand processability similarities between two different titanium alloys. Quantitative similarities between two alloys revealed that Ti–6Al–4V processing parameters can be used for optimization of Ti–6Al–7Nb. The microstructure, processing, properties relationship and the influence of heat treatments were investigated for Ti–6Al–7Nb. The as-built microstructure was composed of a columnar prior β grains with fine acicular α′ martensite resulting in a yield strength of 1082 MPa and an ultimate tensile strength of 1160 MPa with an elongation of 9.7%. Solutionizing at 1055 °C and aging at 540 °C completely transformed the columnar structure of the prior β grains to equiaxed via phase transformation and grain growth, solutionized the α’ martensite into β and then created a fine lamellar α + β structure with air cooling. The resultant microstructure had reduced strength and hardness but increased ductility. The reduction in yield (871 MPa) and ultimate tensile (940 MPa) strength would be positive to minimize stress shielding of orthopedic implants. The improved elongation of 11.5% meets the requirements for biomedical applications which stipulates an elongation of at least 10% according to the ISO 5832-3 Standard. |
doi_str_mv | 10.1016/j.msea.2020.139978 |
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Microstructural comparison study between Ti–6Al–4V and Ti6Al–6Nb was used to understand processability similarities between two different titanium alloys. Quantitative similarities between two alloys revealed that Ti–6Al–4V processing parameters can be used for optimization of Ti–6Al–7Nb. The microstructure, processing, properties relationship and the influence of heat treatments were investigated for Ti–6Al–7Nb. The as-built microstructure was composed of a columnar prior β grains with fine acicular α′ martensite resulting in a yield strength of 1082 MPa and an ultimate tensile strength of 1160 MPa with an elongation of 9.7%. Solutionizing at 1055 °C and aging at 540 °C completely transformed the columnar structure of the prior β grains to equiaxed via phase transformation and grain growth, solutionized the α’ martensite into β and then created a fine lamellar α + β structure with air cooling. The resultant microstructure had reduced strength and hardness but increased ductility. The reduction in yield (871 MPa) and ultimate tensile (940 MPa) strength would be positive to minimize stress shielding of orthopedic implants. The improved elongation of 11.5% meets the requirements for biomedical applications which stipulates an elongation of at least 10% according to the ISO 5832-3 Standard.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2020.139978</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Additive manufacturing ; Air cooling ; Biomedical materials ; Columnar structure ; Elongation ; Grain growth ; Heat treating ; Heat treatment ; Lamellar structure ; Laser powder bed fusion ; Martensite ; Mechanical ; Mechanical properties ; Microstructure ; Optimization ; Orthopaedic implants ; Orthopedics ; Phase transitions ; Powder beds ; Process parameters ; Properties ; Similarity ; Stress shielding ; Surgical implants ; Titanium alloy ; Titanium alloys ; Titanium base alloys ; Ti–6Al–7Nb ; Ultimate tensile strength</subject><ispartof>Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2020-08, Vol.793, p.139978, Article 139978</ispartof><rights>2020 Elsevier B.V.</rights><rights>Copyright Elsevier BV Aug 19, 2020</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c328t-a797b3506b79c7021cad7f64c4f98cc223972f42bbb8509a9df65c9c0aab5f0e3</citedby><cites>FETCH-LOGICAL-c328t-a797b3506b79c7021cad7f64c4f98cc223972f42bbb8509a9df65c9c0aab5f0e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.msea.2020.139978$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Xu, Chao</creatorcontrib><creatorcontrib>Sikan, Fatih</creatorcontrib><creatorcontrib>Atabay, Sila Ece</creatorcontrib><creatorcontrib>Muñiz-Lerma, Jose Alberto</creatorcontrib><creatorcontrib>Sanchez-Mata, Oscar</creatorcontrib><creatorcontrib>Wang, Xianglong</creatorcontrib><creatorcontrib>Brochu, Mathieu</creatorcontrib><title>Microstructure and mechanical behavior of as-built and heat-treated Ti–6Al–7Nb produced by laser powder bed fusion</title><title>Materials science & engineering. A, Structural materials : properties, microstructure and processing</title><description>Ti–6Al–4V and Ti–6Al–7Nb were manufactured with laser powder bed fusion (LPBF). Microstructural comparison study between Ti–6Al–4V and Ti6Al–6Nb was used to understand processability similarities between two different titanium alloys. Quantitative similarities between two alloys revealed that Ti–6Al–4V processing parameters can be used for optimization of Ti–6Al–7Nb. The microstructure, processing, properties relationship and the influence of heat treatments were investigated for Ti–6Al–7Nb. The as-built microstructure was composed of a columnar prior β grains with fine acicular α′ martensite resulting in a yield strength of 1082 MPa and an ultimate tensile strength of 1160 MPa with an elongation of 9.7%. Solutionizing at 1055 °C and aging at 540 °C completely transformed the columnar structure of the prior β grains to equiaxed via phase transformation and grain growth, solutionized the α’ martensite into β and then created a fine lamellar α + β structure with air cooling. The resultant microstructure had reduced strength and hardness but increased ductility. The reduction in yield (871 MPa) and ultimate tensile (940 MPa) strength would be positive to minimize stress shielding of orthopedic implants. The improved elongation of 11.5% meets the requirements for biomedical applications which stipulates an elongation of at least 10% according to the ISO 5832-3 Standard.</description><subject>Additive manufacturing</subject><subject>Air cooling</subject><subject>Biomedical materials</subject><subject>Columnar structure</subject><subject>Elongation</subject><subject>Grain growth</subject><subject>Heat treating</subject><subject>Heat treatment</subject><subject>Lamellar structure</subject><subject>Laser powder bed fusion</subject><subject>Martensite</subject><subject>Mechanical</subject><subject>Mechanical properties</subject><subject>Microstructure</subject><subject>Optimization</subject><subject>Orthopaedic implants</subject><subject>Orthopedics</subject><subject>Phase transitions</subject><subject>Powder beds</subject><subject>Process parameters</subject><subject>Properties</subject><subject>Similarity</subject><subject>Stress shielding</subject><subject>Surgical implants</subject><subject>Titanium alloy</subject><subject>Titanium alloys</subject><subject>Titanium base alloys</subject><subject>Ti–6Al–7Nb</subject><subject>Ultimate tensile strength</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kL1OwzAUhS0EEqXwAkyWmFMcO4ljiaWq-JMKLGW2bMdWHaVxsZ0iNt6BN-RJcAgzy73S0Tn35wPgMkeLHOXVdbvYBS0WGOEkEMZofQRmeU1JVjBSHYMZYjjPSsTIKTgLoUUI5QUqZ-DwZJV3IfpBxcFrKPoG7rTait4q0UGpt-JgnYfOQBEyOdgu_nq2WsQs-lR1Azf2-_OrWnap0mcJ9941g0q6_ICdCNrDvXtvUpNJM0Owrj8HJ0Z0QV_89Tl4vbvdrB6y9cv942q5zhTBdcwEZVSSElWSMkURzpVoqKkKVRhWK4UxYRSbAksp6_ScYI2pSsUUEkKWBmkyB1fT3HTT26BD5K0bfJ9WclxUuKKEkjK58OQaUQSvDd97uxP-g-eIj3x5y0e-fOTLJ74pdDOFdLr_YLXnQVndp7-t1yryxtn_4j9FBIap</recordid><startdate>20200819</startdate><enddate>20200819</enddate><creator>Xu, Chao</creator><creator>Sikan, Fatih</creator><creator>Atabay, Sila Ece</creator><creator>Muñiz-Lerma, Jose Alberto</creator><creator>Sanchez-Mata, Oscar</creator><creator>Wang, Xianglong</creator><creator>Brochu, Mathieu</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20200819</creationdate><title>Microstructure and mechanical behavior of as-built and heat-treated Ti–6Al–7Nb produced by laser powder bed fusion</title><author>Xu, Chao ; Sikan, Fatih ; Atabay, Sila Ece ; Muñiz-Lerma, Jose Alberto ; Sanchez-Mata, Oscar ; Wang, Xianglong ; Brochu, Mathieu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c328t-a797b3506b79c7021cad7f64c4f98cc223972f42bbb8509a9df65c9c0aab5f0e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Additive manufacturing</topic><topic>Air cooling</topic><topic>Biomedical materials</topic><topic>Columnar structure</topic><topic>Elongation</topic><topic>Grain growth</topic><topic>Heat treating</topic><topic>Heat treatment</topic><topic>Lamellar structure</topic><topic>Laser powder bed fusion</topic><topic>Martensite</topic><topic>Mechanical</topic><topic>Mechanical properties</topic><topic>Microstructure</topic><topic>Optimization</topic><topic>Orthopaedic implants</topic><topic>Orthopedics</topic><topic>Phase transitions</topic><topic>Powder beds</topic><topic>Process parameters</topic><topic>Properties</topic><topic>Similarity</topic><topic>Stress shielding</topic><topic>Surgical implants</topic><topic>Titanium alloy</topic><topic>Titanium alloys</topic><topic>Titanium base alloys</topic><topic>Ti–6Al–7Nb</topic><topic>Ultimate tensile strength</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xu, Chao</creatorcontrib><creatorcontrib>Sikan, Fatih</creatorcontrib><creatorcontrib>Atabay, Sila Ece</creatorcontrib><creatorcontrib>Muñiz-Lerma, Jose Alberto</creatorcontrib><creatorcontrib>Sanchez-Mata, Oscar</creatorcontrib><creatorcontrib>Wang, Xianglong</creatorcontrib><creatorcontrib>Brochu, Mathieu</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xu, Chao</au><au>Sikan, Fatih</au><au>Atabay, Sila Ece</au><au>Muñiz-Lerma, Jose Alberto</au><au>Sanchez-Mata, Oscar</au><au>Wang, Xianglong</au><au>Brochu, Mathieu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microstructure and mechanical behavior of as-built and heat-treated Ti–6Al–7Nb produced by laser powder bed fusion</atitle><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2020-08-19</date><risdate>2020</risdate><volume>793</volume><spage>139978</spage><pages>139978-</pages><artnum>139978</artnum><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>Ti–6Al–4V and Ti–6Al–7Nb were manufactured with laser powder bed fusion (LPBF). Microstructural comparison study between Ti–6Al–4V and Ti6Al–6Nb was used to understand processability similarities between two different titanium alloys. Quantitative similarities between two alloys revealed that Ti–6Al–4V processing parameters can be used for optimization of Ti–6Al–7Nb. The microstructure, processing, properties relationship and the influence of heat treatments were investigated for Ti–6Al–7Nb. The as-built microstructure was composed of a columnar prior β grains with fine acicular α′ martensite resulting in a yield strength of 1082 MPa and an ultimate tensile strength of 1160 MPa with an elongation of 9.7%. Solutionizing at 1055 °C and aging at 540 °C completely transformed the columnar structure of the prior β grains to equiaxed via phase transformation and grain growth, solutionized the α’ martensite into β and then created a fine lamellar α + β structure with air cooling. The resultant microstructure had reduced strength and hardness but increased ductility. The reduction in yield (871 MPa) and ultimate tensile (940 MPa) strength would be positive to minimize stress shielding of orthopedic implants. The improved elongation of 11.5% meets the requirements for biomedical applications which stipulates an elongation of at least 10% according to the ISO 5832-3 Standard.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2020.139978</doi></addata></record> |
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subjects | Additive manufacturing Air cooling Biomedical materials Columnar structure Elongation Grain growth Heat treating Heat treatment Lamellar structure Laser powder bed fusion Martensite Mechanical Mechanical properties Microstructure Optimization Orthopaedic implants Orthopedics Phase transitions Powder beds Process parameters Properties Similarity Stress shielding Surgical implants Titanium alloy Titanium alloys Titanium base alloys Ti–6Al–7Nb Ultimate tensile strength |
title | Microstructure and mechanical behavior of as-built and heat-treated Ti–6Al–7Nb produced by laser powder bed fusion |
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