SYNTHESIS, CHARACTERIZATION, ANDCOMPUTATIONAL STUDIES OF N-[(9E)-8,10,17-TRIAZATETRACYCLO[8.7.0.02,7.011,16]HEPTADECA-1(17),2,4,6,11(16),12,14-HEPTAEN-9-YLIDENE]BENZAMIDE

SYNTHESIS, CHARACTERIZATION, ANDCOMPUTATIONAL STUDIES OF N-[(9E)-8,10,17-TRIAZATETRACYCLO[8.7.0.02,7.011,16]HEPTADECA-1(17),2,4,6,11(16),12,14-HEPTAEN-9-YLIDENE]BENZAMIDE

N-[(9E)-8,10,17-Triazatetracyclo[8.7.0.02,7.011,16]heptadeca-1(17),2,4,6,11(16),12,14-heptaen-9-ylidene] benzamide (I) is synthesized and characterized by spectroscopy, microanalysis, and single crystal X-ray diffractometry. Compound I crystallizes in the monoclinic space group P21/c with a = 15.898...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of structural chemistry 2020-01, Vol.61 (8), p.1177-1185
Hauptverfasser: Odame, F, Hosten, E C, Tshentu, Z R
Format: Artikel
Sprache:eng
Schlagworte:
Benzamide
Crystals
Single crystals
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:N-[(9E)-8,10,17-Triazatetracyclo[8.7.0.02,7.011,16]heptadeca-1(17),2,4,6,11(16),12,14-heptaen-9-ylidene] benzamide (I) is synthesized and characterized by spectroscopy, microanalysis, and single crystal X-ray diffractometry. Compound I crystallizes in the monoclinic space group P21/c with a = 15.8980(7) Å, b = 4.8067(2) Å, c = 21.0455(10) Å, β = 101.153(2)°, and Z = 4. The experimental bond lengths and bond angles are contrasted with computed bond lengths and bond angles.
ISSN:0022-4766
1573-8779
DOI:10.1134/S0022476620080016