Interaction of N,N'-Di(4-chlorophenyl)diimide 1,1'-Binaphtyl-4,4',5,5',8,8'-hexacarboxylic Acid with Thiourea Dioxide in Solution and Thin Film
The reactions of interaction of N , N '-di(4-chlorophenyl)diimide 1,1'-binaphtyl-4,4',5,5',8,8'-hexa-carboxylic acid (cubogen red) with thiourea dioxide in a water-alkaline solution and a Langmuir–Blodgett thin film, obtained on quartz and silicon substrates, have been inves...
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| Veröffentlicht in: | Crystallography reports 2020-09, Vol.65 (5), p.779-785 |
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| container_title | Crystallography reports |
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| creator | Nikitin, K. S. Polenov, Yu. V. Kazak, A. V. Egorova, E. V. Usol’tseva, N. V. |
| description | The reactions of interaction of
N
,
N
'-di(4-chlorophenyl)diimide 1,1'-binaphtyl-4,4',5,5',8,8'-hexa-carboxylic acid (cubogen red) with thiourea dioxide in a water-alkaline solution and a Langmuir–Blodgett thin film, obtained on quartz and silicon substrates, have been investigated. Electron absorption spectroscopy have revealed that the reaction of reductive cyclization of cubogen with formation of perylenetetracarboxylic acid diimide derivatives occurs in a water-alkaline solution. At the same time, the interaction of thiourea dioxide with a cubogen thin film does not lead to the formation of cyclization products; nevertheless, it changes the film structure. One might suggest that soluble leuco forms of J aggregates are formed in this case, whereas H aggregates remain intact in the structure. |
| doi_str_mv | 10.1134/S1063774520050156 |
| format | Article |
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N
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N
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N
'-di(4-chlorophenyl)diimide 1,1'-binaphtyl-4,4',5,5',8,8'-hexa-carboxylic acid (cubogen red) with thiourea dioxide in a water-alkaline solution and a Langmuir–Blodgett thin film, obtained on quartz and silicon substrates, have been investigated. Electron absorption spectroscopy have revealed that the reaction of reductive cyclization of cubogen with formation of perylenetetracarboxylic acid diimide derivatives occurs in a water-alkaline solution. At the same time, the interaction of thiourea dioxide with a cubogen thin film does not lead to the formation of cyclization products; nevertheless, it changes the film structure. One might suggest that soluble leuco forms of J aggregates are formed in this case, whereas H aggregates remain intact in the structure.</description><subject>Aggregates</subject><subject>Carboxylic acids</subject><subject>Crystallography and Scattering Methods</subject><subject>Diimide</subject><subject>Dioxides</subject><subject>Langmuir-Blodgett films</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Silicon substrates</subject><subject>Surface and Thin Films</subject><subject>Thin films</subject><subject>Thioureas</subject><issn>1063-7745</issn><issn>1562-689X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1UE9LwzAUL6LgnH4AbwEPVWg0aZK2O87N6WDMwyZ4K2ma2owuqWmH66fwK5s6wYN4ee_B79_j53mXGN1iTOjdCqOIxDFlIUIMYRYdeQM3Qxglo9djdzsY9vipd9Y0G4RQkmA68D7nupWWi1YZDUwBlsHSh1N1TaEoK2NNXUrdVTe5UluVS4AD7MN7pXldtl0FaUD9gAXMD5Ig8WEp91xwm5l9VykBxkLl4EO1JViXyuys5GCqzL73URqsTLX7TuU67wkazFS1PfdOCl418uJnD72X2cN68gQXz4_zyXgBRUhwBCMZhQXHkiY8ZJJnGRkxxgUmBQkFQXEc53lEGU4kJlJkVAjJItdNkY-yLBMJGXpXB9_amvedbNp04z7ULjINKUMEI0KQY-EDS1jTNFYWaW3VltsuxSjte0__9O404UHTOK5-k_bX-X_RF7reghA</recordid><startdate>20200901</startdate><enddate>20200901</enddate><creator>Nikitin, K. S.</creator><creator>Polenov, Yu. V.</creator><creator>Kazak, A. V.</creator><creator>Egorova, E. V.</creator><creator>Usol’tseva, N. V.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20200901</creationdate><title>Interaction of N,N'-Di(4-chlorophenyl)diimide 1,1'-Binaphtyl-4,4',5,5',8,8'-hexacarboxylic Acid with Thiourea Dioxide in Solution and Thin Film</title><author>Nikitin, K. S. ; Polenov, Yu. V. ; Kazak, A. V. ; Egorova, E. V. ; Usol’tseva, N. V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2316-6e62fa1e48a25eabb3955ac13f32c30777dd64518e13ecb4cce56520fd9bbbc83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Aggregates</topic><topic>Carboxylic acids</topic><topic>Crystallography and Scattering Methods</topic><topic>Diimide</topic><topic>Dioxides</topic><topic>Langmuir-Blodgett films</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Silicon substrates</topic><topic>Surface and Thin Films</topic><topic>Thin films</topic><topic>Thioureas</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nikitin, K. S.</creatorcontrib><creatorcontrib>Polenov, Yu. V.</creatorcontrib><creatorcontrib>Kazak, A. V.</creatorcontrib><creatorcontrib>Egorova, E. V.</creatorcontrib><creatorcontrib>Usol’tseva, N. V.</creatorcontrib><collection>CrossRef</collection><jtitle>Crystallography reports</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nikitin, K. S.</au><au>Polenov, Yu. V.</au><au>Kazak, A. V.</au><au>Egorova, E. V.</au><au>Usol’tseva, N. V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Interaction of N,N'-Di(4-chlorophenyl)diimide 1,1'-Binaphtyl-4,4',5,5',8,8'-hexacarboxylic Acid with Thiourea Dioxide in Solution and Thin Film</atitle><jtitle>Crystallography reports</jtitle><stitle>Crystallogr. Rep</stitle><date>2020-09-01</date><risdate>2020</risdate><volume>65</volume><issue>5</issue><spage>779</spage><epage>785</epage><pages>779-785</pages><issn>1063-7745</issn><eissn>1562-689X</eissn><abstract>The reactions of interaction of
N
,
N
'-di(4-chlorophenyl)diimide 1,1'-binaphtyl-4,4',5,5',8,8'-hexa-carboxylic acid (cubogen red) with thiourea dioxide in a water-alkaline solution and a Langmuir–Blodgett thin film, obtained on quartz and silicon substrates, have been investigated. Electron absorption spectroscopy have revealed that the reaction of reductive cyclization of cubogen with formation of perylenetetracarboxylic acid diimide derivatives occurs in a water-alkaline solution. At the same time, the interaction of thiourea dioxide with a cubogen thin film does not lead to the formation of cyclization products; nevertheless, it changes the film structure. One might suggest that soluble leuco forms of J aggregates are formed in this case, whereas H aggregates remain intact in the structure.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1063774520050156</doi><tpages>7</tpages></addata></record> |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Aggregates Carboxylic acids Crystallography and Scattering Methods Diimide Dioxides Langmuir-Blodgett films Physics Physics and Astronomy Silicon substrates Surface and Thin Films Thin films Thioureas |
| title | Interaction of N,N'-Di(4-chlorophenyl)diimide 1,1'-Binaphtyl-4,4',5,5',8,8'-hexacarboxylic Acid with Thiourea Dioxide in Solution and Thin Film |
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