A comparison of NO2 sensing characteristics of α- and γ-iron oxide-based solid-state gas sensors
In this work, we report on the successful synthesis of α- and γ-iron oxide (hematite and maghemite, respectively) nanopowders using a simple sol–gel technique followed by dries in supercritical ethanol. Microstructural and morphological characterizations were performed using X-ray diffraction (XRD)...
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Veröffentlicht in: | Applied physics. A, Materials science & processing Materials science & processing, 2020-10, Vol.126 (10), Article 788 |
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container_title | Applied physics. A, Materials science & processing |
container_volume | 126 |
creator | Hjiri, M. Zahmouli, N. Khouzami, K. Mir, L. El Aida, M. S. Moulaee, K. Lemine, O. M. Leonardi, S. G. Neri, G. |
description | In this work, we report on the successful synthesis of α- and γ-iron oxide (hematite and maghemite, respectively) nanopowders using a simple sol–gel technique followed by dries in supercritical ethanol. Microstructural and morphological characterizations were performed using X-ray diffraction (XRD) and transmission and scanning electron microscopies (TEM and SEM). The iron oxide semiconducting materials have been tested as sensing layer in solid-state conductometric planar sensors for the monitoring sof low NO
2
concentrations in air. This study demonstrated that the crystalline microstructure of the iron oxide nanopowders greatly affects the NO
2
sensing properties, allowing to tune the performances of the developed sensor towards the target gas. γ-Fe
2
O
3
nanopowder-based sensor resulted to have better performance than α-Fe
2
O
3
sensor for NO
2
monitoring. |
doi_str_mv | 10.1007/s00339-020-03829-3 |
format | Article |
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2
concentrations in air. This study demonstrated that the crystalline microstructure of the iron oxide nanopowders greatly affects the NO
2
sensing properties, allowing to tune the performances of the developed sensor towards the target gas. γ-Fe
2
O
3
nanopowder-based sensor resulted to have better performance than α-Fe
2
O
3
sensor for NO
2
monitoring.</description><identifier>ISSN: 0947-8396</identifier><identifier>EISSN: 1432-0630</identifier><identifier>DOI: 10.1007/s00339-020-03829-3</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Applied physics ; Characterization and Evaluation of Materials ; Condensed Matter Physics ; Ethanol ; Gas sensors ; Hematite ; Iron oxides ; Machines ; Manufacturing ; Materials science ; Microstructure ; Monitoring ; Nanotechnology ; Nitrogen dioxide ; Optical and Electronic Materials ; Physics ; Physics and Astronomy ; Processes ; Sensors ; Sol-gel processes ; Solid state ; Surfaces and Interfaces ; Thin Films</subject><ispartof>Applied physics. A, Materials science & processing, 2020-10, Vol.126 (10), Article 788</ispartof><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020</rights><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-f74681682cc4c021fb1f45b1627e1e08d6332f2c28905d93afcacbf1aedb5dfc3</citedby><cites>FETCH-LOGICAL-c319t-f74681682cc4c021fb1f45b1627e1e08d6332f2c28905d93afcacbf1aedb5dfc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00339-020-03829-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00339-020-03829-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27926,27927,41490,42559,51321</link.rule.ids></links><search><creatorcontrib>Hjiri, M.</creatorcontrib><creatorcontrib>Zahmouli, N.</creatorcontrib><creatorcontrib>Khouzami, K.</creatorcontrib><creatorcontrib>Mir, L. El</creatorcontrib><creatorcontrib>Aida, M. S.</creatorcontrib><creatorcontrib>Moulaee, K.</creatorcontrib><creatorcontrib>Lemine, O. M.</creatorcontrib><creatorcontrib>Leonardi, S. G.</creatorcontrib><creatorcontrib>Neri, G.</creatorcontrib><title>A comparison of NO2 sensing characteristics of α- and γ-iron oxide-based solid-state gas sensors</title><title>Applied physics. A, Materials science & processing</title><addtitle>Appl. Phys. A</addtitle><description>In this work, we report on the successful synthesis of α- and γ-iron oxide (hematite and maghemite, respectively) nanopowders using a simple sol–gel technique followed by dries in supercritical ethanol. Microstructural and morphological characterizations were performed using X-ray diffraction (XRD) and transmission and scanning electron microscopies (TEM and SEM). The iron oxide semiconducting materials have been tested as sensing layer in solid-state conductometric planar sensors for the monitoring sof low NO
2
concentrations in air. This study demonstrated that the crystalline microstructure of the iron oxide nanopowders greatly affects the NO
2
sensing properties, allowing to tune the performances of the developed sensor towards the target gas. γ-Fe
2
O
3
nanopowder-based sensor resulted to have better performance than α-Fe
2
O
3
sensor for NO
2
monitoring.</description><subject>Applied physics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Condensed Matter Physics</subject><subject>Ethanol</subject><subject>Gas sensors</subject><subject>Hematite</subject><subject>Iron oxides</subject><subject>Machines</subject><subject>Manufacturing</subject><subject>Materials science</subject><subject>Microstructure</subject><subject>Monitoring</subject><subject>Nanotechnology</subject><subject>Nitrogen dioxide</subject><subject>Optical and Electronic Materials</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Processes</subject><subject>Sensors</subject><subject>Sol-gel processes</subject><subject>Solid state</subject><subject>Surfaces and Interfaces</subject><subject>Thin Films</subject><issn>0947-8396</issn><issn>1432-0630</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kE1OwzAQRi0EEqVwAVaWWBvG48RJllXFn1TBBtaW49glVRsXTyrBsRD36JlIWyR2zGYW871vpMfYpYRrCVDcEIBSlQAEAarESqgjNpKZQgFawTEbQZUVolSVPmVnRAsYJkMcsXrCXVytbWopdjwG_vSMnHxHbTfn7s0m63o_HPvW0e68_RLcdg3ffos27YiPtvGituQbTnHZNoJ623s-t7SviYnO2UmwS_IXv3vMXu9uX6YPYvZ8_zidzIRTsupFKDJdSl2ic5kDlKGWIctrqbHw0kPZaKUwoMOygryplA3OujpI65s6b4JTY3Z16F2n-L7x1JtF3KRueGkwywG1VlgOKTykXIpEyQezTu3Kpk8jwexcmoNLM7g0e5dGDZA6QDSEu7lPf9X_UD9pwXig</recordid><startdate>20201001</startdate><enddate>20201001</enddate><creator>Hjiri, M.</creator><creator>Zahmouli, N.</creator><creator>Khouzami, K.</creator><creator>Mir, L. El</creator><creator>Aida, M. S.</creator><creator>Moulaee, K.</creator><creator>Lemine, O. M.</creator><creator>Leonardi, S. G.</creator><creator>Neri, G.</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20201001</creationdate><title>A comparison of NO2 sensing characteristics of α- and γ-iron oxide-based solid-state gas sensors</title><author>Hjiri, M. ; Zahmouli, N. ; Khouzami, K. ; Mir, L. El ; Aida, M. S. ; Moulaee, K. ; Lemine, O. M. ; Leonardi, S. G. ; Neri, G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-f74681682cc4c021fb1f45b1627e1e08d6332f2c28905d93afcacbf1aedb5dfc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Applied physics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Condensed Matter Physics</topic><topic>Ethanol</topic><topic>Gas sensors</topic><topic>Hematite</topic><topic>Iron oxides</topic><topic>Machines</topic><topic>Manufacturing</topic><topic>Materials science</topic><topic>Microstructure</topic><topic>Monitoring</topic><topic>Nanotechnology</topic><topic>Nitrogen dioxide</topic><topic>Optical and Electronic Materials</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Processes</topic><topic>Sensors</topic><topic>Sol-gel processes</topic><topic>Solid state</topic><topic>Surfaces and Interfaces</topic><topic>Thin Films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hjiri, M.</creatorcontrib><creatorcontrib>Zahmouli, N.</creatorcontrib><creatorcontrib>Khouzami, K.</creatorcontrib><creatorcontrib>Mir, L. El</creatorcontrib><creatorcontrib>Aida, M. S.</creatorcontrib><creatorcontrib>Moulaee, K.</creatorcontrib><creatorcontrib>Lemine, O. M.</creatorcontrib><creatorcontrib>Leonardi, S. G.</creatorcontrib><creatorcontrib>Neri, G.</creatorcontrib><collection>CrossRef</collection><jtitle>Applied physics. A, Materials science & processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hjiri, M.</au><au>Zahmouli, N.</au><au>Khouzami, K.</au><au>Mir, L. El</au><au>Aida, M. S.</au><au>Moulaee, K.</au><au>Lemine, O. M.</au><au>Leonardi, S. G.</au><au>Neri, G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A comparison of NO2 sensing characteristics of α- and γ-iron oxide-based solid-state gas sensors</atitle><jtitle>Applied physics. A, Materials science & processing</jtitle><stitle>Appl. Phys. A</stitle><date>2020-10-01</date><risdate>2020</risdate><volume>126</volume><issue>10</issue><artnum>788</artnum><issn>0947-8396</issn><eissn>1432-0630</eissn><abstract>In this work, we report on the successful synthesis of α- and γ-iron oxide (hematite and maghemite, respectively) nanopowders using a simple sol–gel technique followed by dries in supercritical ethanol. Microstructural and morphological characterizations were performed using X-ray diffraction (XRD) and transmission and scanning electron microscopies (TEM and SEM). The iron oxide semiconducting materials have been tested as sensing layer in solid-state conductometric planar sensors for the monitoring sof low NO
2
concentrations in air. This study demonstrated that the crystalline microstructure of the iron oxide nanopowders greatly affects the NO
2
sensing properties, allowing to tune the performances of the developed sensor towards the target gas. γ-Fe
2
O
3
nanopowder-based sensor resulted to have better performance than α-Fe
2
O
3
sensor for NO
2
monitoring.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s00339-020-03829-3</doi></addata></record> |
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subjects | Applied physics Characterization and Evaluation of Materials Condensed Matter Physics Ethanol Gas sensors Hematite Iron oxides Machines Manufacturing Materials science Microstructure Monitoring Nanotechnology Nitrogen dioxide Optical and Electronic Materials Physics Physics and Astronomy Processes Sensors Sol-gel processes Solid state Surfaces and Interfaces Thin Films |
title | A comparison of NO2 sensing characteristics of α- and γ-iron oxide-based solid-state gas sensors |
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