Influence of Cadmium Substitution on Structural and Mechanical Properties of Co‐Ni Nano Ferrite Synthesized by Co‐Precipitation Method
The objective of this work is to synthesize cadmium doped cobalt nickel ferrite (Co0.5Ni0.5Cd1.5xFe2‐xO4) series with x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 by co‐precipitation method and analysis of structural properties using X‐ray diffraction (XRD), Fourier‐transform infrared spectroscopy (FTIR), and s...
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| Veröffentlicht in: | Macromolecular symposia. 2020-10, Vol.393 (1), p.n/a |
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| creator | Kulkarni, Akshay B. Hegde, Nagaraj D. Gowda H., Shashidhara Mathad, S. N. |
| description | The objective of this work is to synthesize cadmium doped cobalt nickel ferrite (Co0.5Ni0.5Cd1.5xFe2‐xO4) series with x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 by co‐precipitation method and analysis of structural properties using X‐ray diffraction (XRD), Fourier‐transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) characterization. The XRD characterization of the samples confirms the cubic spinel structure. Grains in the samples are granular in nature as depicted by SEM images. The FTIR spectra of synthesized ferrites show two strong absorption bands (ν1 and ν2) in the range 400–600 cm‐1 belonging to tetrahedral (A) and octahedral (B) interstitial sites. Williamson Hall and size‐strain plot results show the variation in the grain size with change in doping concentration. Crystallite size D, lattice constant a, micro strain ε, x‐ray density Δx, dislocation density ρD, hopping lengths(LA and LB), bond lengths (A–O and B–O), ionic radii (rA and rB), texture coefficients [TC(hkl)], and mechanical properties are also reported. |
| doi_str_mv | 10.1002/masy.201900213 |
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N.</creator><creatorcontrib>Kulkarni, Akshay B. ; Hegde, Nagaraj D. ; Gowda H., Shashidhara ; Mathad, S. N.</creatorcontrib><description>The objective of this work is to synthesize cadmium doped cobalt nickel ferrite (Co0.5Ni0.5Cd1.5xFe2‐xO4) series with x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 by co‐precipitation method and analysis of structural properties using X‐ray diffraction (XRD), Fourier‐transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) characterization. The XRD characterization of the samples confirms the cubic spinel structure. Grains in the samples are granular in nature as depicted by SEM images. The FTIR spectra of synthesized ferrites show two strong absorption bands (ν1 and ν2) in the range 400–600 cm‐1 belonging to tetrahedral (A) and octahedral (B) interstitial sites. Williamson Hall and size‐strain plot results show the variation in the grain size with change in doping concentration. Crystallite size D, lattice constant a, micro strain ε, x‐ray density Δx, dislocation density ρD, hopping lengths(LA and LB), bond lengths (A–O and B–O), ionic radii (rA and rB), texture coefficients [TC(hkl)], and mechanical properties are also reported.</description><identifier>ISSN: 1022-1360</identifier><identifier>EISSN: 1521-3900</identifier><identifier>DOI: 10.1002/masy.201900213</identifier><language>eng</language><publisher>Weinheim: Wiley Subscription Services, Inc</publisher><subject>Absorption spectra ; Cadmium ; Chemical precipitation ; Cobalt ; Co‐Ni ferrite ; Crystallites ; Crystals ; Dislocation density ; Fourier transforms ; FT‐IR ; Grain size ; Infrared spectroscopy ; Lattice parameters ; Mechanical properties ; Nickel ; Nickel ferrites ; Scanning electron microscopy ; SEM ; Spectrum analysis ; Synthesis ; X-ray diffraction ; XRD</subject><ispartof>Macromolecular symposia., 2020-10, Vol.393 (1), p.n/a</ispartof><rights>2020 Wiley‐VCH GmbH</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3543-6d79cfe9c58a0d638253d1c0cf21061ddabca36787cd947f5eaad53b8f6961e53</citedby><cites>FETCH-LOGICAL-c3543-6d79cfe9c58a0d638253d1c0cf21061ddabca36787cd947f5eaad53b8f6961e53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fmasy.201900213$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fmasy.201900213$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids></links><search><creatorcontrib>Kulkarni, Akshay B.</creatorcontrib><creatorcontrib>Hegde, Nagaraj D.</creatorcontrib><creatorcontrib>Gowda H., Shashidhara</creatorcontrib><creatorcontrib>Mathad, S. N.</creatorcontrib><title>Influence of Cadmium Substitution on Structural and Mechanical Properties of Co‐Ni Nano Ferrite Synthesized by Co‐Precipitation Method</title><title>Macromolecular symposia.</title><description>The objective of this work is to synthesize cadmium doped cobalt nickel ferrite (Co0.5Ni0.5Cd1.5xFe2‐xO4) series with x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 by co‐precipitation method and analysis of structural properties using X‐ray diffraction (XRD), Fourier‐transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) characterization. The XRD characterization of the samples confirms the cubic spinel structure. Grains in the samples are granular in nature as depicted by SEM images. The FTIR spectra of synthesized ferrites show two strong absorption bands (ν1 and ν2) in the range 400–600 cm‐1 belonging to tetrahedral (A) and octahedral (B) interstitial sites. Williamson Hall and size‐strain plot results show the variation in the grain size with change in doping concentration. Crystallite size D, lattice constant a, micro strain ε, x‐ray density Δx, dislocation density ρD, hopping lengths(LA and LB), bond lengths (A–O and B–O), ionic radii (rA and rB), texture coefficients [TC(hkl)], and mechanical properties are also reported.</description><subject>Absorption spectra</subject><subject>Cadmium</subject><subject>Chemical precipitation</subject><subject>Cobalt</subject><subject>Co‐Ni ferrite</subject><subject>Crystallites</subject><subject>Crystals</subject><subject>Dislocation density</subject><subject>Fourier transforms</subject><subject>FT‐IR</subject><subject>Grain size</subject><subject>Infrared spectroscopy</subject><subject>Lattice parameters</subject><subject>Mechanical properties</subject><subject>Nickel</subject><subject>Nickel ferrites</subject><subject>Scanning electron microscopy</subject><subject>SEM</subject><subject>Spectrum analysis</subject><subject>Synthesis</subject><subject>X-ray diffraction</subject><subject>XRD</subject><issn>1022-1360</issn><issn>1521-3900</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNqFkEtLw0AUhYMoWKtb1wOuU-fRyWNZio9CWwvRhaswmbmhU9JMnZkgceXalb_RX2LaiC6FC_ce-M49cILgkuARwZheb4VrRxSTtBOEHQUDwikJWSePuxtTGhIW4dPgzLkNxjhNYzIIPmZ1WTVQS0CmRFOhtrrZoqwpnNe-8drUqJvM20b6xooKiVqhBci1qLXs5MqaHVivwR385uv9c6nRUtQG3YK12gPK2tqvwek3UKhoe2ZlQeqd9uKQsAC_Nuo8OClF5eDiZw-Dp9ubx-l9OH-4m00n81AyPmZhpOJUlpBKngisIpZQzhSRWJaU4IgoJQopWBQnsVTpOC45CKE4K5IySiMCnA2Dq_7vzpqXBpzPN6axdReZ0zHHhPKIso4a9ZS0xjkLZb6zeitsmxOc7_vO933nv313hrQ3vOoK2n_ofDHJnv-83wcYiOw</recordid><startdate>202010</startdate><enddate>202010</enddate><creator>Kulkarni, Akshay B.</creator><creator>Hegde, Nagaraj D.</creator><creator>Gowda H., Shashidhara</creator><creator>Mathad, S. 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N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3543-6d79cfe9c58a0d638253d1c0cf21061ddabca36787cd947f5eaad53b8f6961e53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Absorption spectra</topic><topic>Cadmium</topic><topic>Chemical precipitation</topic><topic>Cobalt</topic><topic>Co‐Ni ferrite</topic><topic>Crystallites</topic><topic>Crystals</topic><topic>Dislocation density</topic><topic>Fourier transforms</topic><topic>FT‐IR</topic><topic>Grain size</topic><topic>Infrared spectroscopy</topic><topic>Lattice parameters</topic><topic>Mechanical properties</topic><topic>Nickel</topic><topic>Nickel ferrites</topic><topic>Scanning electron microscopy</topic><topic>SEM</topic><topic>Spectrum analysis</topic><topic>Synthesis</topic><topic>X-ray diffraction</topic><topic>XRD</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kulkarni, Akshay B.</creatorcontrib><creatorcontrib>Hegde, Nagaraj D.</creatorcontrib><creatorcontrib>Gowda H., Shashidhara</creatorcontrib><creatorcontrib>Mathad, S. 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N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Influence of Cadmium Substitution on Structural and Mechanical Properties of Co‐Ni Nano Ferrite Synthesized by Co‐Precipitation Method</atitle><jtitle>Macromolecular symposia.</jtitle><date>2020-10</date><risdate>2020</risdate><volume>393</volume><issue>1</issue><epage>n/a</epage><issn>1022-1360</issn><eissn>1521-3900</eissn><abstract>The objective of this work is to synthesize cadmium doped cobalt nickel ferrite (Co0.5Ni0.5Cd1.5xFe2‐xO4) series with x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 by co‐precipitation method and analysis of structural properties using X‐ray diffraction (XRD), Fourier‐transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) characterization. The XRD characterization of the samples confirms the cubic spinel structure. Grains in the samples are granular in nature as depicted by SEM images. The FTIR spectra of synthesized ferrites show two strong absorption bands (ν1 and ν2) in the range 400–600 cm‐1 belonging to tetrahedral (A) and octahedral (B) interstitial sites. Williamson Hall and size‐strain plot results show the variation in the grain size with change in doping concentration. Crystallite size D, lattice constant a, micro strain ε, x‐ray density Δx, dislocation density ρD, hopping lengths(LA and LB), bond lengths (A–O and B–O), ionic radii (rA and rB), texture coefficients [TC(hkl)], and mechanical properties are also reported.</abstract><cop>Weinheim</cop><pub>Wiley Subscription Services, Inc</pub><doi>10.1002/masy.201900213</doi><tpages>7</tpages></addata></record> |
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| subjects | Absorption spectra Cadmium Chemical precipitation Cobalt Co‐Ni ferrite Crystallites Crystals Dislocation density Fourier transforms FT‐IR Grain size Infrared spectroscopy Lattice parameters Mechanical properties Nickel Nickel ferrites Scanning electron microscopy SEM Spectrum analysis Synthesis X-ray diffraction XRD |
| title | Influence of Cadmium Substitution on Structural and Mechanical Properties of Co‐Ni Nano Ferrite Synthesized by Co‐Precipitation Method |
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