Effect of Synthesis Conditions on Textural Characteristics of Mesoporous Cerium(IV) Oxide
Mesoporous CeO 2 has been prepared under hydrothermal conditions at 110–170°С in the presence of ionic and nonionic surfactants and characterized by SEM, low-temperature nitrogen adsorption–desorption, X-ray powder diffraction, and DTA–TG techniques. All synthesized samples had a specific surface ar...
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| Veröffentlicht in: | Petroleum chemistry 2020-08, Vol.60 (8), p.853-857 |
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| creator | Maerle, A. A. Rodionova, L. I. Moskovskaya, I. F. |
| description | Mesoporous CeO
2
has been prepared under hydrothermal conditions at 110–170°С in the presence of ionic and nonionic surfactants and characterized by SEM, low-temperature nitrogen adsorption–desorption, X-ray powder diffraction, and DTA–TG techniques. All synthesized samples had a specific surface area of up to 110 m
2
/g and a pore diameter of about 4 nm. It has been shown that the use of surfactants of various nature affects not only the final morphology of the oxide, but also its porous structure characteristics and chemical composition of its samples. It has been found that the use of ultrasound in the synthesis affects the specific surface area and average pore size of the samples. |
| doi_str_mv | 10.1134/S096554412008006X |
| format | Article |
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2
has been prepared under hydrothermal conditions at 110–170°С in the presence of ionic and nonionic surfactants and characterized by SEM, low-temperature nitrogen adsorption–desorption, X-ray powder diffraction, and DTA–TG techniques. All synthesized samples had a specific surface area of up to 110 m
2
/g and a pore diameter of about 4 nm. It has been shown that the use of surfactants of various nature affects not only the final morphology of the oxide, but also its porous structure characteristics and chemical composition of its samples. It has been found that the use of ultrasound in the synthesis affects the specific surface area and average pore size of the samples.</description><identifier>ISSN: 0965-5441</identifier><identifier>EISSN: 1555-6239</identifier><identifier>DOI: 10.1134/S096554412008006X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Adsorption ; Cerium ; Cerium oxides ; Chemical composition ; Chemistry ; Chemistry and Materials Science ; Diffraction ; Industrial Chemistry/Chemical Engineering ; Low temperature ; Morphology ; Pore size ; Porosity ; Specific surface ; Surface active agents ; Surface area ; Surfactants ; Synthesis ; X ray powder diffraction ; X-rays</subject><ispartof>Petroleum chemistry, 2020-08, Vol.60 (8), p.853-857</ispartof><rights>Pleiades Publishing, Ltd. 2020</rights><rights>COPYRIGHT 2020 Springer</rights><rights>Pleiades Publishing, Ltd. 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c392t-44813853d4912a94928caf99bdc71de98fedf270ee55c919319cc3d8db1564753</citedby><cites>FETCH-LOGICAL-c392t-44813853d4912a94928caf99bdc71de98fedf270ee55c919319cc3d8db1564753</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S096554412008006X$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S096554412008006X$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Maerle, A. A.</creatorcontrib><creatorcontrib>Rodionova, L. I.</creatorcontrib><creatorcontrib>Moskovskaya, I. F.</creatorcontrib><title>Effect of Synthesis Conditions on Textural Characteristics of Mesoporous Cerium(IV) Oxide</title><title>Petroleum chemistry</title><addtitle>Pet. Chem</addtitle><description>Mesoporous CeO
2
has been prepared under hydrothermal conditions at 110–170°С in the presence of ionic and nonionic surfactants and characterized by SEM, low-temperature nitrogen adsorption–desorption, X-ray powder diffraction, and DTA–TG techniques. All synthesized samples had a specific surface area of up to 110 m
2
/g and a pore diameter of about 4 nm. It has been shown that the use of surfactants of various nature affects not only the final morphology of the oxide, but also its porous structure characteristics and chemical composition of its samples. It has been found that the use of ultrasound in the synthesis affects the specific surface area and average pore size of the samples.</description><subject>Adsorption</subject><subject>Cerium</subject><subject>Cerium oxides</subject><subject>Chemical composition</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Diffraction</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Low temperature</subject><subject>Morphology</subject><subject>Pore size</subject><subject>Porosity</subject><subject>Specific surface</subject><subject>Surface active agents</subject><subject>Surface area</subject><subject>Surfactants</subject><subject>Synthesis</subject><subject>X ray powder diffraction</subject><subject>X-rays</subject><issn>0965-5441</issn><issn>1555-6239</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1kE1LAzEQhoMoWKs_wNuCFz1szed2cyylaqHSQ6voadkmkzal3dQkC-2_N6WCB5E5DMy8z3y8CN0S3COE8ccZloUQnBOKcYlx8XGGOkQIkReUyXPUObbzY_8SXYWwxpj0CWcd9DkyBlTMnMlmhyauINiQDV2jbbSuCZlrsjnsY-vrTTZc1b5WEbwN0apwZF4huJ3zrk1Qqrfb-_H7QzbdWw3X6MLUmwA3P7mL3p5G8-FLPpk-j4eDSa6YpDHnvCSsFExzSWgtuaSlqo2UC636RIMsDWhD-xhACCWJZEQqxXSpF0QUvC9YF92d5u68-2ohxGrtWt-klRXlrGRSFJQkVe-kWtYbqGxjXEy_pNCwtco1YGyqDwrGZLIvrekicgKUdyF4MNXO223tDxXB1dHy6o_liaEnJiRtswT_e8r_0DdcnYIT</recordid><startdate>20200801</startdate><enddate>20200801</enddate><creator>Maerle, A. A.</creator><creator>Rodionova, L. I.</creator><creator>Moskovskaya, I. F.</creator><general>Pleiades Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20200801</creationdate><title>Effect of Synthesis Conditions on Textural Characteristics of Mesoporous Cerium(IV) Oxide</title><author>Maerle, A. A. ; Rodionova, L. I. ; Moskovskaya, I. F.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c392t-44813853d4912a94928caf99bdc71de98fedf270ee55c919319cc3d8db1564753</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Adsorption</topic><topic>Cerium</topic><topic>Cerium oxides</topic><topic>Chemical composition</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Diffraction</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Low temperature</topic><topic>Morphology</topic><topic>Pore size</topic><topic>Porosity</topic><topic>Specific surface</topic><topic>Surface active agents</topic><topic>Surface area</topic><topic>Surfactants</topic><topic>Synthesis</topic><topic>X ray powder diffraction</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Maerle, A. A.</creatorcontrib><creatorcontrib>Rodionova, L. I.</creatorcontrib><creatorcontrib>Moskovskaya, I. F.</creatorcontrib><collection>CrossRef</collection><jtitle>Petroleum chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maerle, A. A.</au><au>Rodionova, L. I.</au><au>Moskovskaya, I. F.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of Synthesis Conditions on Textural Characteristics of Mesoporous Cerium(IV) Oxide</atitle><jtitle>Petroleum chemistry</jtitle><stitle>Pet. Chem</stitle><date>2020-08-01</date><risdate>2020</risdate><volume>60</volume><issue>8</issue><spage>853</spage><epage>857</epage><pages>853-857</pages><issn>0965-5441</issn><eissn>1555-6239</eissn><abstract>Mesoporous CeO
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has been prepared under hydrothermal conditions at 110–170°С in the presence of ionic and nonionic surfactants and characterized by SEM, low-temperature nitrogen adsorption–desorption, X-ray powder diffraction, and DTA–TG techniques. All synthesized samples had a specific surface area of up to 110 m
2
/g and a pore diameter of about 4 nm. It has been shown that the use of surfactants of various nature affects not only the final morphology of the oxide, but also its porous structure characteristics and chemical composition of its samples. It has been found that the use of ultrasound in the synthesis affects the specific surface area and average pore size of the samples.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S096554412008006X</doi><tpages>5</tpages></addata></record> |
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| source | SpringerLink Journals; EBSCOhost Business Source Complete |
| subjects | Adsorption Cerium Cerium oxides Chemical composition Chemistry Chemistry and Materials Science Diffraction Industrial Chemistry/Chemical Engineering Low temperature Morphology Pore size Porosity Specific surface Surface active agents Surface area Surfactants Synthesis X ray powder diffraction X-rays |
| title | Effect of Synthesis Conditions on Textural Characteristics of Mesoporous Cerium(IV) Oxide |
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