Investigation of nickel slag waste as a modifier on graphene-TiO2 microstructure for sensing phenolic compound
In the present work, the potential of nickel slag waste (NSW) was performed as a modifier of graphene-TiO 2 material for sensing phenolic compound under an electrochemical system. It was provided to produce variations of mineral components to improve electrochemical sensing in its application for a...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2020-09, Vol.31 (17), p.14375-14383 |
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| container_title | Journal of materials science. Materials in electronics |
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| creator | Wibowo, Dwiprayogo Sufandy, Yayuk Irwan, Irwan Azis, Thamrin Maulidiyah, Maulidiyah Nurdin, Muhammad |
| description | In the present work, the potential of nickel slag waste (NSW) was performed as a modifier of graphene-TiO
2
material for sensing phenolic compound under an electrochemical system. It was provided to produce variations of mineral components to improve electrochemical sensing in its application for a sensor device. Preparation of composite material (slag-graphene-TiO
2
) was prepared through solid-state reaction by mixing of NSW, graphene, and TiO
2
anatase crystal. Based on these results, we discover the composition of NSW with various mineral contents and produced anatase TiO
2
crystal prepared via thermal method at 500 °C for 3 h. Subsequently, the slag-G-TiO
2
composite has been homogeneous and characterized using SEM–EDX shows the microstructure formed with the variation of elements content. Moreover, the electrochemical test for sensing phenol compound exhibits the exceptionally sensitivity towards phenol detection in electrolyte solution by the limit of detection (LoD) is 0.0367 ppm and % RSD value of 0.016%. The electrode also produce excellent stability properties by repeatability of 1 to 21 times and the average of oxidation current at 183.57 µA. Finally, we test with a real sample to obtain the ability of phenol detection. |
| doi_str_mv | 10.1007/s10854-020-03996-2 |
| format | Article |
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2
material for sensing phenolic compound under an electrochemical system. It was provided to produce variations of mineral components to improve electrochemical sensing in its application for a sensor device. Preparation of composite material (slag-graphene-TiO
2
) was prepared through solid-state reaction by mixing of NSW, graphene, and TiO
2
anatase crystal. Based on these results, we discover the composition of NSW with various mineral contents and produced anatase TiO
2
crystal prepared via thermal method at 500 °C for 3 h. Subsequently, the slag-G-TiO
2
composite has been homogeneous and characterized using SEM–EDX shows the microstructure formed with the variation of elements content. Moreover, the electrochemical test for sensing phenol compound exhibits the exceptionally sensitivity towards phenol detection in electrolyte solution by the limit of detection (LoD) is 0.0367 ppm and % RSD value of 0.016%. The electrode also produce excellent stability properties by repeatability of 1 to 21 times and the average of oxidation current at 183.57 µA. Finally, we test with a real sample to obtain the ability of phenol detection.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-020-03996-2</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Anatase ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Composite materials ; Detection ; Graphene ; Materials Science ; Microstructure ; Nickel ; Optical and Electronic Materials ; Oxidation ; Phenols ; Slag ; Titanium dioxide</subject><ispartof>Journal of materials science. Materials in electronics, 2020-09, Vol.31 (17), p.14375-14383</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c385t-666ed1e6b1cfab8585fa848d0eb174e37ae4c402ca0978fbc9961f44d26dab533</citedby><cites>FETCH-LOGICAL-c385t-666ed1e6b1cfab8585fa848d0eb174e37ae4c402ca0978fbc9961f44d26dab533</cites><orcidid>0000-0002-6727-9283</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-020-03996-2$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-020-03996-2$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Wibowo, Dwiprayogo</creatorcontrib><creatorcontrib>Sufandy, Yayuk</creatorcontrib><creatorcontrib>Irwan, Irwan</creatorcontrib><creatorcontrib>Azis, Thamrin</creatorcontrib><creatorcontrib>Maulidiyah, Maulidiyah</creatorcontrib><creatorcontrib>Nurdin, Muhammad</creatorcontrib><title>Investigation of nickel slag waste as a modifier on graphene-TiO2 microstructure for sensing phenolic compound</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>In the present work, the potential of nickel slag waste (NSW) was performed as a modifier of graphene-TiO
2
material for sensing phenolic compound under an electrochemical system. It was provided to produce variations of mineral components to improve electrochemical sensing in its application for a sensor device. Preparation of composite material (slag-graphene-TiO
2
) was prepared through solid-state reaction by mixing of NSW, graphene, and TiO
2
anatase crystal. Based on these results, we discover the composition of NSW with various mineral contents and produced anatase TiO
2
crystal prepared via thermal method at 500 °C for 3 h. Subsequently, the slag-G-TiO
2
composite has been homogeneous and characterized using SEM–EDX shows the microstructure formed with the variation of elements content. Moreover, the electrochemical test for sensing phenol compound exhibits the exceptionally sensitivity towards phenol detection in electrolyte solution by the limit of detection (LoD) is 0.0367 ppm and % RSD value of 0.016%. The electrode also produce excellent stability properties by repeatability of 1 to 21 times and the average of oxidation current at 183.57 µA. Finally, we test with a real sample to obtain the ability of phenol detection.</description><subject>Anatase</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Composite materials</subject><subject>Detection</subject><subject>Graphene</subject><subject>Materials Science</subject><subject>Microstructure</subject><subject>Nickel</subject><subject>Optical and Electronic Materials</subject><subject>Oxidation</subject><subject>Phenols</subject><subject>Slag</subject><subject>Titanium dioxide</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9kM1KAzEYRYMoWKsv4CrgOprfmXQpxZ-C0E0FdyGTScbUTlKTGcW3N3UEd66-zbn34x4ALgm-JhjXN5lgKTjCFCPMFosK0SMwI6JmiEv6cgxmeCFqxAWlp-As5y3GuOJMzkBYhQ-bB9_pwccAo4PBmze7g3mnO_ip82ChzlDDPrbeeZtgobqk9682WLTxawp7b1LMQxrNMCYLXUww25B96OCBijtvoIn9Po6hPQcnTu-yvfi9c_B8f7dZPqKn9cNqefuEDJNiQFVV2ZbYqiHG6UYKKZyWXLbYNqTmltXacsMxNRovaukaUyYTx3lLq1Y3grE5uJp69ym-j2Wg2sYxhfJS0bKbMC4ILxSdqMOAnKxT--R7nb4UwergVU1eVfGqfrwqWkJsCuUCh86mv-p_Ut-HUH0o</recordid><startdate>20200901</startdate><enddate>20200901</enddate><creator>Wibowo, Dwiprayogo</creator><creator>Sufandy, Yayuk</creator><creator>Irwan, Irwan</creator><creator>Azis, Thamrin</creator><creator>Maulidiyah, Maulidiyah</creator><creator>Nurdin, Muhammad</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope><orcidid>https://orcid.org/0000-0002-6727-9283</orcidid></search><sort><creationdate>20200901</creationdate><title>Investigation of nickel slag waste as a modifier on graphene-TiO2 microstructure for sensing phenolic compound</title><author>Wibowo, Dwiprayogo ; Sufandy, Yayuk ; Irwan, Irwan ; Azis, Thamrin ; Maulidiyah, Maulidiyah ; Nurdin, Muhammad</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c385t-666ed1e6b1cfab8585fa848d0eb174e37ae4c402ca0978fbc9961f44d26dab533</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Anatase</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Composite materials</topic><topic>Detection</topic><topic>Graphene</topic><topic>Materials Science</topic><topic>Microstructure</topic><topic>Nickel</topic><topic>Optical and Electronic Materials</topic><topic>Oxidation</topic><topic>Phenols</topic><topic>Slag</topic><topic>Titanium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wibowo, Dwiprayogo</creatorcontrib><creatorcontrib>Sufandy, Yayuk</creatorcontrib><creatorcontrib>Irwan, Irwan</creatorcontrib><creatorcontrib>Azis, Thamrin</creatorcontrib><creatorcontrib>Maulidiyah, Maulidiyah</creatorcontrib><creatorcontrib>Nurdin, Muhammad</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wibowo, Dwiprayogo</au><au>Sufandy, Yayuk</au><au>Irwan, Irwan</au><au>Azis, Thamrin</au><au>Maulidiyah, Maulidiyah</au><au>Nurdin, Muhammad</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigation of nickel slag waste as a modifier on graphene-TiO2 microstructure for sensing phenolic compound</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2020-09-01</date><risdate>2020</risdate><volume>31</volume><issue>17</issue><spage>14375</spage><epage>14383</epage><pages>14375-14383</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>In the present work, the potential of nickel slag waste (NSW) was performed as a modifier of graphene-TiO
2
material for sensing phenolic compound under an electrochemical system. It was provided to produce variations of mineral components to improve electrochemical sensing in its application for a sensor device. Preparation of composite material (slag-graphene-TiO
2
) was prepared through solid-state reaction by mixing of NSW, graphene, and TiO
2
anatase crystal. Based on these results, we discover the composition of NSW with various mineral contents and produced anatase TiO
2
crystal prepared via thermal method at 500 °C for 3 h. Subsequently, the slag-G-TiO
2
composite has been homogeneous and characterized using SEM–EDX shows the microstructure formed with the variation of elements content. Moreover, the electrochemical test for sensing phenol compound exhibits the exceptionally sensitivity towards phenol detection in electrolyte solution by the limit of detection (LoD) is 0.0367 ppm and % RSD value of 0.016%. The electrode also produce excellent stability properties by repeatability of 1 to 21 times and the average of oxidation current at 183.57 µA. Finally, we test with a real sample to obtain the ability of phenol detection.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-020-03996-2</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0002-6727-9283</orcidid></addata></record> |
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| subjects | Anatase Characterization and Evaluation of Materials Chemistry and Materials Science Composite materials Detection Graphene Materials Science Microstructure Nickel Optical and Electronic Materials Oxidation Phenols Slag Titanium dioxide |
| title | Investigation of nickel slag waste as a modifier on graphene-TiO2 microstructure for sensing phenolic compound |
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