Cs desorption behavior during hydrothermal treatment of illite with oxalic acid
The desorption of radioactive cesium (Cs) in soil is influenced by the clay mineral type, adsorption site, and concentration of Cs. In this study, experiments to detect desorption of non-radioactive and radioactive Cs from illite using oxalic acid were performed for 2 days at 70 °C in hydrothermal c...
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| Veröffentlicht in: | Environmental science and pollution research international 2020-10, Vol.27 (28), p.35580-35590 |
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| creator | Kim, Sung-Man Yoon, In-Ho Kim, Il-Gook Park, Chan Woo Sihn, YoungHo Kim, June-Hyun Park, So-Jin |
| description | The desorption of radioactive cesium (Cs) in soil is influenced by the clay mineral type, adsorption site, and concentration of Cs. In this study, experiments to detect desorption of non-radioactive and radioactive Cs from illite using oxalic acid were performed for 2 days at 70 °C in hydrothermal conditions. The results showed that the
133
Cs removal efficiency by oxalic acid and inorganic acid treatment was similar at high concentration (22.86 mmol/kg) of non-radioactive
133
Cs. In the radioactive
137
Cs experiment, the removal efficiency by oxalic acid was higher than that by inorganic acid at low concentration (0.79 × 10
−6
mmol/kg) of radioactive
137
Cs. Based on the illite hypothetical frayed edge site (FES) concentration of 0.612 mmol/kg, the results suggested that
137
Cs was preferentially adsorbed to FES on illite. The
137
Cs at low concentration was difficult to remove because it was irreversible adsorption to FES, while the non-radioactive Cs at high concentration was mainly adsorbed to planar sites, and so was easy to desorb by ion exchange. Based on the results of NMR, FTIR, and XPS analyses, we concluded that the higher efficiency of
137
Cs removal at low concentration by oxalic acid treatment than by treatment with inorganic acid was because of chelation effects associated with the complexation of oxalic acid (ligands) and metal ions in irreversible site (FES). |
| doi_str_mv | 10.1007/s11356-020-09675-3 |
| format | Article |
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133
Cs removal efficiency by oxalic acid and inorganic acid treatment was similar at high concentration (22.86 mmol/kg) of non-radioactive
133
Cs. In the radioactive
137
Cs experiment, the removal efficiency by oxalic acid was higher than that by inorganic acid at low concentration (0.79 × 10
−6
mmol/kg) of radioactive
137
Cs. Based on the illite hypothetical frayed edge site (FES) concentration of 0.612 mmol/kg, the results suggested that
137
Cs was preferentially adsorbed to FES on illite. The
137
Cs at low concentration was difficult to remove because it was irreversible adsorption to FES, while the non-radioactive Cs at high concentration was mainly adsorbed to planar sites, and so was easy to desorb by ion exchange. Based on the results of NMR, FTIR, and XPS analyses, we concluded that the higher efficiency of
137
Cs removal at low concentration by oxalic acid treatment than by treatment with inorganic acid was because of chelation effects associated with the complexation of oxalic acid (ligands) and metal ions in irreversible site (FES).</description><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-020-09675-3</identifier><identifier>PMID: 32594435</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Acids ; Adsorption ; Aquatic Pollution ; Atmospheric Protection/Air Quality Control/Air Pollution ; Cesium ; Cesium 133 ; Cesium 137 ; Cesium isotopes ; Cesium radioisotopes ; Chelation ; Clay minerals ; Desorption ; Earth and Environmental Science ; Ecotoxicology ; Efficiency ; Environment ; Environmental Chemistry ; Environmental Health ; Environmental science ; Hydrothermal treatment ; Illite ; Inorganic acids ; Ion exchange ; Metal ions ; Minerals ; NMR ; Nuclear magnetic resonance ; Oxalic Acid ; Research Article ; Waste Water Technology ; Water Management ; Water Pollutants, Radioactive - analysis ; Water Pollution Control ; X ray photoelectron spectroscopy</subject><ispartof>Environmental science and pollution research international, 2020-10, Vol.27 (28), p.35580-35590</ispartof><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020</rights><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c412t-4964fc211c7dd6526ea08a3ce0f2e3945a51545481feabb75618a70cc3f2ecd93</citedby><cites>FETCH-LOGICAL-c412t-4964fc211c7dd6526ea08a3ce0f2e3945a51545481feabb75618a70cc3f2ecd93</cites><orcidid>0000-0001-8740-0573</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-020-09675-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-020-09675-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/32594435$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Kim, Sung-Man</creatorcontrib><creatorcontrib>Yoon, In-Ho</creatorcontrib><creatorcontrib>Kim, Il-Gook</creatorcontrib><creatorcontrib>Park, Chan Woo</creatorcontrib><creatorcontrib>Sihn, YoungHo</creatorcontrib><creatorcontrib>Kim, June-Hyun</creatorcontrib><creatorcontrib>Park, So-Jin</creatorcontrib><title>Cs desorption behavior during hydrothermal treatment of illite with oxalic acid</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><addtitle>Environ Sci Pollut Res Int</addtitle><description>The desorption of radioactive cesium (Cs) in soil is influenced by the clay mineral type, adsorption site, and concentration of Cs. In this study, experiments to detect desorption of non-radioactive and radioactive Cs from illite using oxalic acid were performed for 2 days at 70 °C in hydrothermal conditions. The results showed that the
133
Cs removal efficiency by oxalic acid and inorganic acid treatment was similar at high concentration (22.86 mmol/kg) of non-radioactive
133
Cs. In the radioactive
137
Cs experiment, the removal efficiency by oxalic acid was higher than that by inorganic acid at low concentration (0.79 × 10
−6
mmol/kg) of radioactive
137
Cs. Based on the illite hypothetical frayed edge site (FES) concentration of 0.612 mmol/kg, the results suggested that
137
Cs was preferentially adsorbed to FES on illite. The
137
Cs at low concentration was difficult to remove because it was irreversible adsorption to FES, while the non-radioactive Cs at high concentration was mainly adsorbed to planar sites, and so was easy to desorb by ion exchange. Based on the results of NMR, FTIR, and XPS analyses, we concluded that the higher efficiency of
137
Cs removal at low concentration by oxalic acid treatment than by treatment with inorganic acid was because of chelation effects associated with the complexation of oxalic acid (ligands) and metal ions in irreversible site (FES).</description><subject>Acids</subject><subject>Adsorption</subject><subject>Aquatic Pollution</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>Cesium</subject><subject>Cesium 133</subject><subject>Cesium 137</subject><subject>Cesium isotopes</subject><subject>Cesium radioisotopes</subject><subject>Chelation</subject><subject>Clay minerals</subject><subject>Desorption</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Efficiency</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Environmental science</subject><subject>Hydrothermal treatment</subject><subject>Illite</subject><subject>Inorganic acids</subject><subject>Ion exchange</subject><subject>Metal ions</subject><subject>Minerals</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Oxalic Acid</subject><subject>Research Article</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollutants, Radioactive - analysis</subject><subject>Water Pollution Control</subject><subject>X ray photoelectron spectroscopy</subject><issn>0944-1344</issn><issn>1614-7499</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>BENPR</sourceid><recordid>eNp9kL1OwzAYRS0EoqXwAgzIEnPA_6lHVPEnIXWB2XIch7hK4mA7QN-elBTYmL7hnns_6QBwjtEVRii_jhhTLjJEUIakyHlGD8AcC8yynEl5COZIMpZhytgMnMS4QSMpSX4MZpTwMaJ8DtarCEsbfeiT8x0sbK3fnQ-wHILrXmG9LYNPtQ2tbmAKVqfWdgn6CrqmccnCD5dq6D914wzUxpWn4KjSTbRn-7sAL3e3z6uH7Gl9_7i6ecoMwyRlTApWGYKxyctScCKsRktNjUUVsVQyrjnmjLMlrqwuipwLvNQ5MoaOuSklXYDLabcP_m2wMamNH0I3vlSEUSFzQZY7ikyUCT7GYCvVB9fqsFUYqZ1DNTlUoxn17VDRsXSxnx6K1pa_lR9pI0AnIPY7STb8_f5n9guFsXzb</recordid><startdate>20201001</startdate><enddate>20201001</enddate><creator>Kim, Sung-Man</creator><creator>Yoon, In-Ho</creator><creator>Kim, Il-Gook</creator><creator>Park, Chan Woo</creator><creator>Sihn, YoungHo</creator><creator>Kim, June-Hyun</creator><creator>Park, So-Jin</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QL</scope><scope>7SN</scope><scope>7T7</scope><scope>7TV</scope><scope>7U7</scope><scope>7WY</scope><scope>7WZ</scope><scope>7X7</scope><scope>7XB</scope><scope>87Z</scope><scope>88E</scope><scope>88I</scope><scope>8AO</scope><scope>8C1</scope><scope>8FD</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>8FL</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FR3</scope><scope>FRNLG</scope><scope>FYUFA</scope><scope>F~G</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K60</scope><scope>K6~</scope><scope>K9.</scope><scope>L.-</scope><scope>M0C</scope><scope>M0S</scope><scope>M1P</scope><scope>M2P</scope><scope>M7N</scope><scope>P64</scope><scope>PATMY</scope><scope>PQBIZ</scope><scope>PQBZA</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PYCSY</scope><scope>Q9U</scope><orcidid>https://orcid.org/0000-0001-8740-0573</orcidid></search><sort><creationdate>20201001</creationdate><title>Cs desorption behavior during hydrothermal treatment of illite with oxalic acid</title><author>Kim, Sung-Man ; Yoon, In-Ho ; Kim, Il-Gook ; Park, Chan Woo ; Sihn, YoungHo ; Kim, June-Hyun ; Park, So-Jin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c412t-4964fc211c7dd6526ea08a3ce0f2e3945a51545481feabb75618a70cc3f2ecd93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Acids</topic><topic>Adsorption</topic><topic>Aquatic Pollution</topic><topic>Atmospheric Protection/Air Quality Control/Air Pollution</topic><topic>Cesium</topic><topic>Cesium 133</topic><topic>Cesium 137</topic><topic>Cesium isotopes</topic><topic>Cesium radioisotopes</topic><topic>Chelation</topic><topic>Clay minerals</topic><topic>Desorption</topic><topic>Earth and Environmental Science</topic><topic>Ecotoxicology</topic><topic>Efficiency</topic><topic>Environment</topic><topic>Environmental Chemistry</topic><topic>Environmental Health</topic><topic>Environmental science</topic><topic>Hydrothermal treatment</topic><topic>Illite</topic><topic>Inorganic acids</topic><topic>Ion exchange</topic><topic>Metal ions</topic><topic>Minerals</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Oxalic Acid</topic><topic>Research Article</topic><topic>Waste Water Technology</topic><topic>Water Management</topic><topic>Water Pollutants, Radioactive - analysis</topic><topic>Water Pollution Control</topic><topic>X ray photoelectron spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kim, Sung-Man</creatorcontrib><creatorcontrib>Yoon, In-Ho</creatorcontrib><creatorcontrib>Kim, Il-Gook</creatorcontrib><creatorcontrib>Park, Chan Woo</creatorcontrib><creatorcontrib>Sihn, YoungHo</creatorcontrib><creatorcontrib>Kim, June-Hyun</creatorcontrib><creatorcontrib>Park, So-Jin</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Bacteriology Abstracts (Microbiology B)</collection><collection>Ecology Abstracts</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Pollution Abstracts</collection><collection>Toxicology Abstracts</collection><collection>ABI/INFORM Collection</collection><collection>ABI/INFORM Global (PDF only)</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ABI/INFORM Global (Alumni Edition)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest Pharma Collection</collection><collection>Public Health Database</collection><collection>Technology Research Database</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ABI/INFORM Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Business Premium Collection</collection><collection>Natural Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Engineering Research Database</collection><collection>Business Premium Collection (Alumni)</collection><collection>Health Research Premium Collection</collection><collection>ABI/INFORM Global (Corporate)</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Business Collection (Alumni Edition)</collection><collection>ProQuest Business Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>ABI/INFORM Professional Advanced</collection><collection>ABI/INFORM Global</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Science Database</collection><collection>Algology Mycology and Protozoology Abstracts (Microbiology C)</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Environmental Science Database</collection><collection>ProQuest One Business</collection><collection>ProQuest One Business (Alumni)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Environmental Science Collection</collection><collection>ProQuest Central Basic</collection><jtitle>Environmental science and pollution research international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kim, Sung-Man</au><au>Yoon, In-Ho</au><au>Kim, Il-Gook</au><au>Park, Chan Woo</au><au>Sihn, YoungHo</au><au>Kim, June-Hyun</au><au>Park, So-Jin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Cs desorption behavior during hydrothermal treatment of illite with oxalic acid</atitle><jtitle>Environmental science and pollution research international</jtitle><stitle>Environ Sci Pollut Res</stitle><addtitle>Environ Sci Pollut Res Int</addtitle><date>2020-10-01</date><risdate>2020</risdate><volume>27</volume><issue>28</issue><spage>35580</spage><epage>35590</epage><pages>35580-35590</pages><issn>0944-1344</issn><eissn>1614-7499</eissn><abstract>The desorption of radioactive cesium (Cs) in soil is influenced by the clay mineral type, adsorption site, and concentration of Cs. In this study, experiments to detect desorption of non-radioactive and radioactive Cs from illite using oxalic acid were performed for 2 days at 70 °C in hydrothermal conditions. The results showed that the
133
Cs removal efficiency by oxalic acid and inorganic acid treatment was similar at high concentration (22.86 mmol/kg) of non-radioactive
133
Cs. In the radioactive
137
Cs experiment, the removal efficiency by oxalic acid was higher than that by inorganic acid at low concentration (0.79 × 10
−6
mmol/kg) of radioactive
137
Cs. Based on the illite hypothetical frayed edge site (FES) concentration of 0.612 mmol/kg, the results suggested that
137
Cs was preferentially adsorbed to FES on illite. The
137
Cs at low concentration was difficult to remove because it was irreversible adsorption to FES, while the non-radioactive Cs at high concentration was mainly adsorbed to planar sites, and so was easy to desorb by ion exchange. Based on the results of NMR, FTIR, and XPS analyses, we concluded that the higher efficiency of
137
Cs removal at low concentration by oxalic acid treatment than by treatment with inorganic acid was because of chelation effects associated with the complexation of oxalic acid (ligands) and metal ions in irreversible site (FES).</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>32594435</pmid><doi>10.1007/s11356-020-09675-3</doi><tpages>11</tpages><orcidid>https://orcid.org/0000-0001-8740-0573</orcidid></addata></record> |
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| identifier | ISSN: 0944-1344 |
| ispartof | Environmental science and pollution research international, 2020-10, Vol.27 (28), p.35580-35590 |
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| language | eng |
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| source | MEDLINE; SpringerLink Journals |
| subjects | Acids Adsorption Aquatic Pollution Atmospheric Protection/Air Quality Control/Air Pollution Cesium Cesium 133 Cesium 137 Cesium isotopes Cesium radioisotopes Chelation Clay minerals Desorption Earth and Environmental Science Ecotoxicology Efficiency Environment Environmental Chemistry Environmental Health Environmental science Hydrothermal treatment Illite Inorganic acids Ion exchange Metal ions Minerals NMR Nuclear magnetic resonance Oxalic Acid Research Article Waste Water Technology Water Management Water Pollutants, Radioactive - analysis Water Pollution Control X ray photoelectron spectroscopy |
| title | Cs desorption behavior during hydrothermal treatment of illite with oxalic acid |
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