Synthesis of Zinc-Doped Lithium Tantalate Charge in the Technology of Novel Crystalline Functional Materials
A procedure was developed for preparing lithium tantalate (LiTaO 3 ) charge homogeneously doped with lithium from high-purity tantalum-containing solutions, based on heat treatment of lithium-, tantalum-, and zinc-containing citrate precursors. The thermolysis products were studied by thermal analys...
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| Veröffentlicht in: | Russian journal of applied chemistry 2020-05, Vol.93 (5), p.645-653 |
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| container_title | Russian journal of applied chemistry |
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| creator | Palatnikov, M. N. Masloboeva, S. M. Arutyunyan, L. G. |
| description | A procedure was developed for preparing lithium tantalate (LiTaO
3
) charge homogeneously doped with lithium from high-purity tantalum-containing solutions, based on heat treatment of lithium-, tantalum-, and zinc-containing citrate precursors. The thermolysis products were studied by thermal analysis, X-ray diffraction, and IR absorption spectroscopy. The optimum synthesis conditions and zinc concentration to obtain a single-phase LiTaO
3
:Zn charge were determined. Comparison with the properties of an isomorphic compound LiNbO
3
(LiNbO
3
:Zn) demonstrated the advantages of the synthesis procedure developed and practically important properties such as high optical stability of LiTaO
3
:Zn crystals and low coercive field, acquired by lithium tantalate upon doping with zinc. Samples of LiTaO
3
:Zn charge of various compositions, suitable both for the technology of LiTaO
3
:Zn crystals and for the preparation of piezoelectric ceramics based on zinc-doped lithium tantalate, were prepared by the developed procedure. |
| doi_str_mv | 10.1134/S1070427220050043 |
| format | Article |
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3
) charge homogeneously doped with lithium from high-purity tantalum-containing solutions, based on heat treatment of lithium-, tantalum-, and zinc-containing citrate precursors. The thermolysis products were studied by thermal analysis, X-ray diffraction, and IR absorption spectroscopy. The optimum synthesis conditions and zinc concentration to obtain a single-phase LiTaO
3
:Zn charge were determined. Comparison with the properties of an isomorphic compound LiNbO
3
(LiNbO
3
:Zn) demonstrated the advantages of the synthesis procedure developed and practically important properties such as high optical stability of LiTaO
3
:Zn crystals and low coercive field, acquired by lithium tantalate upon doping with zinc. Samples of LiTaO
3
:Zn charge of various compositions, suitable both for the technology of LiTaO
3
:Zn crystals and for the preparation of piezoelectric ceramics based on zinc-doped lithium tantalate, were prepared by the developed procedure.</description><identifier>ISSN: 1070-4272</identifier><identifier>EISSN: 1608-3296</identifier><identifier>DOI: 10.1134/S1070427220050043</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Coercivity ; Functional materials ; Heat treatment ; Industrial Chemistry/Chemical Engineering ; Infrared analysis ; Infrared spectroscopy ; Inorganic Synthesis and Industrial Inorganic Chemistry ; Lithium ; Lithium niobates ; Lithium tantalates ; Optical properties ; Piezoelectric ceramics ; Piezoelectricity ; Synthesis ; Tantalum ; Thermal analysis ; Zinc</subject><ispartof>Russian journal of applied chemistry, 2020-05, Vol.93 (5), p.645-653</ispartof><rights>Pleiades Publishing, Ltd. 2020</rights><rights>Pleiades Publishing, Ltd. 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c353t-fd8d064d956528ba35fd0a84b0ba7c900a5027ca17cf798a92355404664f1ab83</citedby><cites>FETCH-LOGICAL-c353t-fd8d064d956528ba35fd0a84b0ba7c900a5027ca17cf798a92355404664f1ab83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1070427220050043$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1070427220050043$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Palatnikov, M. N.</creatorcontrib><creatorcontrib>Masloboeva, S. M.</creatorcontrib><creatorcontrib>Arutyunyan, L. G.</creatorcontrib><title>Synthesis of Zinc-Doped Lithium Tantalate Charge in the Technology of Novel Crystalline Functional Materials</title><title>Russian journal of applied chemistry</title><addtitle>Russ J Appl Chem</addtitle><description>A procedure was developed for preparing lithium tantalate (LiTaO
3
) charge homogeneously doped with lithium from high-purity tantalum-containing solutions, based on heat treatment of lithium-, tantalum-, and zinc-containing citrate precursors. The thermolysis products were studied by thermal analysis, X-ray diffraction, and IR absorption spectroscopy. The optimum synthesis conditions and zinc concentration to obtain a single-phase LiTaO
3
:Zn charge were determined. Comparison with the properties of an isomorphic compound LiNbO
3
(LiNbO
3
:Zn) demonstrated the advantages of the synthesis procedure developed and practically important properties such as high optical stability of LiTaO
3
:Zn crystals and low coercive field, acquired by lithium tantalate upon doping with zinc. Samples of LiTaO
3
:Zn charge of various compositions, suitable both for the technology of LiTaO
3
:Zn crystals and for the preparation of piezoelectric ceramics based on zinc-doped lithium tantalate, were prepared by the developed procedure.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Coercivity</subject><subject>Functional materials</subject><subject>Heat treatment</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Inorganic Synthesis and Industrial Inorganic Chemistry</subject><subject>Lithium</subject><subject>Lithium niobates</subject><subject>Lithium tantalates</subject><subject>Optical properties</subject><subject>Piezoelectric ceramics</subject><subject>Piezoelectricity</subject><subject>Synthesis</subject><subject>Tantalum</subject><subject>Thermal analysis</subject><subject>Zinc</subject><issn>1070-4272</issn><issn>1608-3296</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1kEtLxDAUhYsoOI7-AHcB19WbZ9ul1CeMuphx46akaTrN0EnGpBX6780wggvxbs6Fc77D5SbJJYZrjCm7WWLIgJGMEAAOwOhRMsMC8pSSQhzHPdrp3j9NzkLYAEAhRD5L-uVkh04HE5Br0YexKr1zO92ghRk6M27RStpB9nLQqOykX2tkLIoAWmnVWde79bQHX92X7lHppxDDvbEaPYxWDcZZ2aOXSHsj-3CenLRR9MWPzpP3h_tV-ZQu3h6fy9tFqiinQ9o2eQOCNQUXnOS1pLxtQOashlpmqgCQHEimJM5UmxW5LAjlnAETgrVY1jmdJ1eH3p13n6MOQ7Vxo4-nhIownGVFHIgpfEgp70Lwuq123mylnyoM1f6p1Z-nRoYcmBCzdq39b_P_0DcmJnib</recordid><startdate>20200501</startdate><enddate>20200501</enddate><creator>Palatnikov, M. N.</creator><creator>Masloboeva, S. M.</creator><creator>Arutyunyan, L. G.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20200501</creationdate><title>Synthesis of Zinc-Doped Lithium Tantalate Charge in the Technology of Novel Crystalline Functional Materials</title><author>Palatnikov, M. N. ; Masloboeva, S. M. ; Arutyunyan, L. G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c353t-fd8d064d956528ba35fd0a84b0ba7c900a5027ca17cf798a92355404664f1ab83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Coercivity</topic><topic>Functional materials</topic><topic>Heat treatment</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Inorganic Synthesis and Industrial Inorganic Chemistry</topic><topic>Lithium</topic><topic>Lithium niobates</topic><topic>Lithium tantalates</topic><topic>Optical properties</topic><topic>Piezoelectric ceramics</topic><topic>Piezoelectricity</topic><topic>Synthesis</topic><topic>Tantalum</topic><topic>Thermal analysis</topic><topic>Zinc</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Palatnikov, M. N.</creatorcontrib><creatorcontrib>Masloboeva, S. M.</creatorcontrib><creatorcontrib>Arutyunyan, L. G.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of applied chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Palatnikov, M. N.</au><au>Masloboeva, S. M.</au><au>Arutyunyan, L. G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Zinc-Doped Lithium Tantalate Charge in the Technology of Novel Crystalline Functional Materials</atitle><jtitle>Russian journal of applied chemistry</jtitle><stitle>Russ J Appl Chem</stitle><date>2020-05-01</date><risdate>2020</risdate><volume>93</volume><issue>5</issue><spage>645</spage><epage>653</epage><pages>645-653</pages><issn>1070-4272</issn><eissn>1608-3296</eissn><abstract>A procedure was developed for preparing lithium tantalate (LiTaO
3
) charge homogeneously doped with lithium from high-purity tantalum-containing solutions, based on heat treatment of lithium-, tantalum-, and zinc-containing citrate precursors. The thermolysis products were studied by thermal analysis, X-ray diffraction, and IR absorption spectroscopy. The optimum synthesis conditions and zinc concentration to obtain a single-phase LiTaO
3
:Zn charge were determined. Comparison with the properties of an isomorphic compound LiNbO
3
(LiNbO
3
:Zn) demonstrated the advantages of the synthesis procedure developed and practically important properties such as high optical stability of LiTaO
3
:Zn crystals and low coercive field, acquired by lithium tantalate upon doping with zinc. Samples of LiTaO
3
:Zn charge of various compositions, suitable both for the technology of LiTaO
3
:Zn crystals and for the preparation of piezoelectric ceramics based on zinc-doped lithium tantalate, were prepared by the developed procedure.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1070427220050043</doi><tpages>9</tpages></addata></record> |
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| language | eng |
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| subjects | Chemistry Chemistry and Materials Science Chemistry/Food Science Coercivity Functional materials Heat treatment Industrial Chemistry/Chemical Engineering Infrared analysis Infrared spectroscopy Inorganic Synthesis and Industrial Inorganic Chemistry Lithium Lithium niobates Lithium tantalates Optical properties Piezoelectric ceramics Piezoelectricity Synthesis Tantalum Thermal analysis Zinc |
| title | Synthesis of Zinc-Doped Lithium Tantalate Charge in the Technology of Novel Crystalline Functional Materials |
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