Synthesis and Properties of 1,3-Disubstituted Ureas and Their Isosteric Analogs Containing Polycyclic Fragments: I. Synthesis of 1-(Adamantan-1-yl)-3-(fluoro, chlorophenyl)ureas
A series of 1,3-disubstituted ureas with a phenyl fragment containing fluorine and/or chlorine substituents in different positions were synthesized with yields of 33–80%. 1-Isocyanatoadamantane was prepared for the first time by the reaction of diphenylphosphoryl azide with (adamantan-1-yl)carboxyli...
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| Veröffentlicht in: | Russian journal of organic chemistry 2020-05, Vol.56 (5), p.735-740 |
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| container_issue | 5 |
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| container_title | Russian journal of organic chemistry |
| container_volume | 56 |
| creator | Burmistrov, V. V. Danilov, D. V. D’yachenko, V. S. Rasskazova, E. V. Butov, G. M. |
| description | A series of 1,3-disubstituted ureas with a phenyl fragment containing fluorine and/or chlorine substituents in different positions were synthesized with yields of 33–80%. 1-Isocyanatoadamantane was prepared for the first time by the reaction of diphenylphosphoryl azide with (adamantan-1-yl)carboxylic acid in a yield of 85%. |
| doi_str_mv | 10.1134/S1070428020050024 |
| format | Article |
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| subjects | Carboxylic acids Chemistry Chemistry and Materials Science Chlorine Fluorine Organic Chemistry Synthesis Ureas |
| title | Synthesis and Properties of 1,3-Disubstituted Ureas and Their Isosteric Analogs Containing Polycyclic Fragments: I. Synthesis of 1-(Adamantan-1-yl)-3-(fluoro, chlorophenyl)ureas |
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