Iron deficient BaNixMnxFe12−2xO19 (x = 0.0–0.5) hexagonal plates: single-domain magnetic structure and dielectric properties

The current investigation was carried out in order to present the structural, magnetic and dielectric properties of BaNi x Mn x Fe 12−2 x O 19 ( x  = 0.0–0.5) (BNMFO) hexagonal microplates prepared via hydrothermal method followed by calcination at 950 °C for 5 h. The X-ray diffraction patterns of x...

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Veröffentlicht in:Applied physics. A, Materials science & processing Materials science & processing, 2020-07, Vol.126 (7), Article 511
Hauptverfasser: Chandra Sekhar, D., Subba Rao, T., Chandra Babu Naidu, K.
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Subba Rao, T.
Chandra Babu Naidu, K.
description The current investigation was carried out in order to present the structural, magnetic and dielectric properties of BaNi x Mn x Fe 12−2 x O 19 ( x  = 0.0–0.5) (BNMFO) hexagonal microplates prepared via hydrothermal method followed by calcination at 950 °C for 5 h. The X-ray diffraction patterns of x  = 0.0–0.5 contents confirmed the formation of hexagonal phases. The morphology and grain size of the BNMFO was examined by the field emission of scanning electron microscope. The results indicated that the BNMFO exhibited the hexagonal platelet like grains of size ranging from 2.4 to 3.5 µm. Two peaks were formed in the Fourier transform infrared spectra at 585 and 427 cm −1 and indicated the formation of metal–oxygen bonds. It was observed that the band gap was decreased with the increase in ‘ x ’. From the room temperature M–H curves, it was observed that the high saturation magnetization (45.8–53.9 emu/g) was recorded for all samples. Further, the coercive field was decreased from 3133 to 1098 Oe as a function of ‘ x ’. The real and imaginary parts of dielectric permittivity parameters were found to be increased with the increase in ‘ x ’.
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subjects Applied physics
Characterization and Evaluation of Materials
Coercivity
Condensed Matter Physics
Dielectric properties
Diffraction patterns
Field emission microscopy
Fourier transforms
Grain size
Infrared spectra
Machines
Magnetic properties
Magnetic saturation
Magnetic structure
Manufacturing
Materials science
Morphology
Nanotechnology
Optical and Electronic Materials
Physics
Physics and Astronomy
Processes
Room temperature
Surfaces and Interfaces
Thin Films
title Iron deficient BaNixMnxFe12−2xO19 (x = 0.0–0.5) hexagonal plates: single-domain magnetic structure and dielectric properties
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