Effects of Biopolymer Surfactants on the Morphology and Optical Properties of Zinc Sulphide (ZnS) Nanocrystalline Thin Film
Particle sizes of nanoparticles have significant effects on thin film properties such as the morphological and optical properties. However, controlling the size and morphology is a challenging task. One of the approaches towards overcoming these challenges is by using surfactants. This study reporte...
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| Veröffentlicht in: | Journal of physical science 2019-01, Vol.30 (3), p.191-206 |
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| creator | Avit, Dorathy Awing Chin, Suk-Fun Mohd Arif, Noor Azie Azura Shaari, Sahbudin |
| description | Particle sizes of nanoparticles have significant effects on thin film properties such as the morphological and optical properties. However, controlling the size and morphology is a challenging task. One of the approaches towards overcoming these challenges is by using surfactants. This study reported the effects of several types of biopolymer surfactants on the size of zinc sulphide (ZnS) nanoparticles and the morphology of ZnS nanocrystalline thin films. The ZnS nanocrystalline thin films were fabricated by the spin-coating of ZnS nanoparticles on APTES [(3-aminopropyl) triethoxysilane] functionalised silica glass. Alginic acid, chitosan and starch were used as the surfactants to control the morphological and optical properties of the thin films. The XRD analysis confirmed the cubic structure and crystalline nature of the ZnS thin films. The field emission scanning electron microscope (FESEM) analysis revealed that the mean particle size of the ZnS nanocrystalline thin film to be with in the range of20-30 nm. The optical measurements revealed that all ZnS thin films exhibited a high transmittance of 92%-99% in the visible range. Photoluminescence (PL) spectra for all thin films were determined and exhibited their respective peaks at 470 nm and 620 nm. |
| doi_str_mv | 10.21315/jps2019.30.3.12 |
| format | Article |
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However, controlling the size and morphology is a challenging task. One of the approaches towards overcoming these challenges is by using surfactants. This study reported the effects of several types of biopolymer surfactants on the size of zinc sulphide (ZnS) nanoparticles and the morphology of ZnS nanocrystalline thin films. The ZnS nanocrystalline thin films were fabricated by the spin-coating of ZnS nanoparticles on APTES [(3-aminopropyl) triethoxysilane] functionalised silica glass. Alginic acid, chitosan and starch were used as the surfactants to control the morphological and optical properties of the thin films. The XRD analysis confirmed the cubic structure and crystalline nature of the ZnS thin films. The field emission scanning electron microscope (FESEM) analysis revealed that the mean particle size of the ZnS nanocrystalline thin film to be with in the range of20-30 nm. The optical measurements revealed that all ZnS thin films exhibited a high transmittance of 92%-99% in the visible range. Photoluminescence (PL) spectra for all thin films were determined and exhibited their respective peaks at 470 nm and 620 nm.</description><identifier>ISSN: 1675-3402</identifier><identifier>EISSN: 2180-4230</identifier><identifier>DOI: 10.21315/jps2019.30.3.12</identifier><language>eng</language><publisher>Pinang: Universiti Sains Malaysia Press</publisher><subject>Acids ; Aminopropyltriethoxysilane ; Biopolymers ; Chitosan ; Emission analysis ; Field emission microscopy ; Morphology ; Nanocrystals ; Nanoparticles ; Optical measurement ; Optical properties ; Particle size ; Photoluminescence ; Polyethylene glycol ; Polyvinyl alcohol ; Silica glass ; Silicon dioxide ; Spin coating ; Surfactants ; Thin films ; Zinc sulfide</subject><ispartof>Journal of physical science, 2019-01, Vol.30 (3), p.191-206</ispartof><rights>2019. 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However, controlling the size and morphology is a challenging task. One of the approaches towards overcoming these challenges is by using surfactants. This study reported the effects of several types of biopolymer surfactants on the size of zinc sulphide (ZnS) nanoparticles and the morphology of ZnS nanocrystalline thin films. The ZnS nanocrystalline thin films were fabricated by the spin-coating of ZnS nanoparticles on APTES [(3-aminopropyl) triethoxysilane] functionalised silica glass. Alginic acid, chitosan and starch were used as the surfactants to control the morphological and optical properties of the thin films. The XRD analysis confirmed the cubic structure and crystalline nature of the ZnS thin films. The field emission scanning electron microscope (FESEM) analysis revealed that the mean particle size of the ZnS nanocrystalline thin film to be with in the range of20-30 nm. 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Photoluminescence (PL) spectra for all thin films were determined and exhibited their respective peaks at 470 nm and 620 nm.</description><subject>Acids</subject><subject>Aminopropyltriethoxysilane</subject><subject>Biopolymers</subject><subject>Chitosan</subject><subject>Emission analysis</subject><subject>Field emission microscopy</subject><subject>Morphology</subject><subject>Nanocrystals</subject><subject>Nanoparticles</subject><subject>Optical measurement</subject><subject>Optical properties</subject><subject>Particle size</subject><subject>Photoluminescence</subject><subject>Polyethylene glycol</subject><subject>Polyvinyl alcohol</subject><subject>Silica glass</subject><subject>Silicon dioxide</subject><subject>Spin coating</subject><subject>Surfactants</subject><subject>Thin films</subject><subject>Zinc sulfide</subject><issn>1675-3402</issn><issn>2180-4230</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNotkD1PwzAURS0EElXpzmiJBYYEfyRNPELVAlKhSC1LF8uxHeIqtY2dDhF_ntD2LW94554nXQBuMUoJpjh_3PlIEGYpRSlNMbkAI4JLlGSEokswwtMiT2iGyDWYxLhDw1BGGM5H4Hde11p2EboaPhvnXdvvdYDrQ6iF7IT9v1jYNRq-u-Ab17rvHgqr4Mp3RooWfgbndeiMPiq2xsoh3PrGKA3vt3b9AD-EdTL0sRNta6yGm8ZYuDDt_gZc1aKNenLeY_C1mG9mr8ly9fI2e1omkmLaJVWFy4rJaY40y3BZ56jSeVUrIrIyY6woBFYsLzKmKqlzxMopqgqhSkoKTKhSdAzuTl4f3M9Bx47v3CHY4SUn2cAzxFAxUOhEyeBiDLrmPpi9CD3HiB9b5ueWOUWc8sH9B9gKcNg</recordid><startdate>20190101</startdate><enddate>20190101</enddate><creator>Avit, Dorathy Awing</creator><creator>Chin, Suk-Fun</creator><creator>Mohd Arif, Noor Azie Azura</creator><creator>Shaari, Sahbudin</creator><general>Universiti Sains Malaysia Press</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BVBZV</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L6V</scope><scope>L7M</scope><scope>M7S</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope></search><sort><creationdate>20190101</creationdate><title>Effects of Biopolymer Surfactants on the Morphology and Optical Properties of Zinc Sulphide (ZnS) Nanocrystalline Thin Film</title><author>Avit, Dorathy Awing ; 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However, controlling the size and morphology is a challenging task. One of the approaches towards overcoming these challenges is by using surfactants. This study reported the effects of several types of biopolymer surfactants on the size of zinc sulphide (ZnS) nanoparticles and the morphology of ZnS nanocrystalline thin films. The ZnS nanocrystalline thin films were fabricated by the spin-coating of ZnS nanoparticles on APTES [(3-aminopropyl) triethoxysilane] functionalised silica glass. Alginic acid, chitosan and starch were used as the surfactants to control the morphological and optical properties of the thin films. The XRD analysis confirmed the cubic structure and crystalline nature of the ZnS thin films. The field emission scanning electron microscope (FESEM) analysis revealed that the mean particle size of the ZnS nanocrystalline thin film to be with in the range of20-30 nm. The optical measurements revealed that all ZnS thin films exhibited a high transmittance of 92%-99% in the visible range. Photoluminescence (PL) spectra for all thin films were determined and exhibited their respective peaks at 470 nm and 620 nm.</abstract><cop>Pinang</cop><pub>Universiti Sains Malaysia Press</pub><doi>10.21315/jps2019.30.3.12</doi><tpages>16</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Acids Aminopropyltriethoxysilane Biopolymers Chitosan Emission analysis Field emission microscopy Morphology Nanocrystals Nanoparticles Optical measurement Optical properties Particle size Photoluminescence Polyethylene glycol Polyvinyl alcohol Silica glass Silicon dioxide Spin coating Surfactants Thin films Zinc sulfide |
| title | Effects of Biopolymer Surfactants on the Morphology and Optical Properties of Zinc Sulphide (ZnS) Nanocrystalline Thin Film |
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