Synthesis zeolite y from kaolin: Activation of metakaolin with various concentration of sulfuric acid and its application for esterification

In this research, a zeolite Y was synthesized from Bangka-Belitung Kaoline. The synthesis was conducted through activation of metakaolin with sulfuric acid at various concentration of 3, 6, 9, 12, and 15 M. The aging and hydrothermal process was conducted at 100 °C for 24 h. The products were charac...

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Hauptverfasser:	Safitri, Leli Endah, Zuryati, Ulul Khairi, Rohma, Hannis Nur, Ni’mah, Yatim Lailun, Prasetyoko, Didik
Format:	Tagungsbericht
Sprache:	eng
Schlagworte:	Acetic acid Activated clay Activation Esterification Fourier transforms Infrared spectroscopy Kaolin Metakaolin Sulfuric acid Synthesis X-ray diffraction Zeolites
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creator	Safitri, Leli Endah Zuryati, Ulul Khairi Rohma, Hannis Nur Ni’mah, Yatim Lailun Prasetyoko, Didik
description	In this research, a zeolite Y was synthesized from Bangka-Belitung Kaoline. The synthesis was conducted through activation of metakaolin with sulfuric acid at various concentration of 3, 6, 9, 12, and 15 M. The aging and hydrothermal process was conducted at 100 °C for 24 h. The products were characterized by X-ray Diffraction (XRD), Infrared Spectroscopy (FTIR), and Scanning Electron Microscopy-Energy Dispersive X-ray (SEM-EDX) techniques. XRD and FTIR analysis show that the zeolite Y was formed at all acid variation. Acidity was determined by FTIR using pyridine as a molecular probe. The result shows that zeolite Y that was activated with 9 M sulfuric acid (HY-9) has a highest acid site of 0.26 mmol/g. Test of the prepared-catalyst for esterification also shows that HY-9 has the highest conversion of acetic acid, which is 60.06%.
doi_str_mv	10.1063/5.0005581
format	Conference Proceeding
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The synthesis was conducted through activation of metakaolin with sulfuric acid at various concentration of 3, 6, 9, 12, and 15 M. The aging and hydrothermal process was conducted at 100 °C for 24 h. The products were characterized by X-ray Diffraction (XRD), Infrared Spectroscopy (FTIR), and Scanning Electron Microscopy-Energy Dispersive X-ray (SEM-EDX) techniques. XRD and FTIR analysis show that the zeolite Y was formed at all acid variation. Acidity was determined by FTIR using pyridine as a molecular probe. The result shows that zeolite Y that was activated with 9 M sulfuric acid (HY-9) has a highest acid site of 0.26 mmol/g. Test of the prepared-catalyst for esterification also shows that HY-9 has the highest conversion of acetic acid, which is 60.06%.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/5.0005581</doi><tpages>7</tpages></addata></record>
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subjects	Acetic acid Activated clay Activation Esterification Fourier transforms Infrared spectroscopy Kaolin Metakaolin Sulfuric acid Synthesis X-ray diffraction Zeolites
title	Synthesis zeolite y from kaolin: Activation of metakaolin with various concentration of sulfuric acid and its application for esterification
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