Synthesis of novel AgO-doped vanadium–borophosphate semiconducting glasses and investigation of their optical, structural, and thermal properties
Ag-doped vanadium–borophosphate glasses having 46V 2 O 5 –46P 2 O 5 –(8 − x )B 2 O 3 – x AgO as the base structure have been successfully synthesized with different compositions of AgO ( x = 0, 2, 4, 6, 8 mol%) by the conventional melt-quenching technique. Density and molar volume values were calcu...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2020-06, Vol.31 (11), p.8986-8995 |
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| creator | Ilik, Erkan Kilic, Gokhan Issever, U. Gokhan |
| description | Ag-doped vanadium–borophosphate glasses having 46V
2
O
5
–46P
2
O
5
–(8 −
x
)B
2
O
3
–
x
AgO as the base structure have been successfully synthesized with different compositions of AgO (
x
= 0, 2, 4, 6, 8 mol%) by the conventional melt-quenching technique. Density and molar volume values were calculated by Archimedes principle. The transmittance and absorbance spectra, XRD, and FTIR measurements of the glasses were performed at room temperature. While XRD data showed that the glasses had an amorphous structure away from crystallization, FTIR spectra showed that vanadium and phosphate compounds forming the glass network consisted of VO
4
, VO
5
and PO
3
, PO
2
structural units, respectively. It was observed that AgO, which replaces B
2
O
3
, acted as a modifier in the glass network. Direct and indirect band gaps of synthesized glasses were calculated using Tauc method. Urbach energies were also calculated. The glass transition temperature, crystallization temperature, and melting temperature values of the samples were determined with differential scanning calorimetry (DSC) in the range of room temperature to 1000 °C. |
| doi_str_mv | 10.1007/s10854-020-03432-5 |
| format | Article |
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2
O
5
–46P
2
O
5
–(8 −
x
)B
2
O
3
–
x
AgO as the base structure have been successfully synthesized with different compositions of AgO (
x
= 0, 2, 4, 6, 8 mol%) by the conventional melt-quenching technique. Density and molar volume values were calculated by Archimedes principle. The transmittance and absorbance spectra, XRD, and FTIR measurements of the glasses were performed at room temperature. While XRD data showed that the glasses had an amorphous structure away from crystallization, FTIR spectra showed that vanadium and phosphate compounds forming the glass network consisted of VO
4
, VO
5
and PO
3
, PO
2
structural units, respectively. It was observed that AgO, which replaces B
2
O
3
, acted as a modifier in the glass network. Direct and indirect band gaps of synthesized glasses were calculated using Tauc method. Urbach energies were also calculated. The glass transition temperature, crystallization temperature, and melting temperature values of the samples were determined with differential scanning calorimetry (DSC) in the range of room temperature to 1000 °C.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-020-03432-5</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Boron oxides ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Crystallization ; Glass transition temperature ; Materials Science ; Mathematical analysis ; Melt temperature ; Molar volume ; Optical and Electronic Materials ; Optical properties ; Room temperature ; Silver ; Synthesis ; Temperature ; Thermodynamic properties ; Vanadium compounds</subject><ispartof>Journal of materials science. Materials in electronics, 2020-06, Vol.31 (11), p.8986-8995</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-fc60752d54d9426dfe4726b586cbbc916d321659a4d46ab6e728acde1be8de293</citedby><cites>FETCH-LOGICAL-c319t-fc60752d54d9426dfe4726b586cbbc916d321659a4d46ab6e728acde1be8de293</cites><orcidid>0000-0001-7145-4999 ; 0000-0003-2986-0015 ; 0000-0002-6762-6898</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-020-03432-5$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-020-03432-5$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Ilik, Erkan</creatorcontrib><creatorcontrib>Kilic, Gokhan</creatorcontrib><creatorcontrib>Issever, U. Gokhan</creatorcontrib><title>Synthesis of novel AgO-doped vanadium–borophosphate semiconducting glasses and investigation of their optical, structural, and thermal properties</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Ag-doped vanadium–borophosphate glasses having 46V
2
O
5
–46P
2
O
5
–(8 −
x
)B
2
O
3
–
x
AgO as the base structure have been successfully synthesized with different compositions of AgO (
x
= 0, 2, 4, 6, 8 mol%) by the conventional melt-quenching technique. Density and molar volume values were calculated by Archimedes principle. The transmittance and absorbance spectra, XRD, and FTIR measurements of the glasses were performed at room temperature. While XRD data showed that the glasses had an amorphous structure away from crystallization, FTIR spectra showed that vanadium and phosphate compounds forming the glass network consisted of VO
4
, VO
5
and PO
3
, PO
2
structural units, respectively. It was observed that AgO, which replaces B
2
O
3
, acted as a modifier in the glass network. Direct and indirect band gaps of synthesized glasses were calculated using Tauc method. Urbach energies were also calculated. The glass transition temperature, crystallization temperature, and melting temperature values of the samples were determined with differential scanning calorimetry (DSC) in the range of room temperature to 1000 °C.</description><subject>Boron oxides</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Crystallization</subject><subject>Glass transition temperature</subject><subject>Materials Science</subject><subject>Mathematical analysis</subject><subject>Melt temperature</subject><subject>Molar volume</subject><subject>Optical and Electronic Materials</subject><subject>Optical properties</subject><subject>Room temperature</subject><subject>Silver</subject><subject>Synthesis</subject><subject>Temperature</subject><subject>Thermodynamic properties</subject><subject>Vanadium compounds</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kMFqFTEUhoNY8Fp9AVcBt8YmmSQzsyxFq1DoQgvdhUySmZsyNxlzMhe68x36hn0SM16hO1fnwPn_7z_8CH1g9DOjtL0ARjspCOWU0EY0nMhXaMdk2xDR8fvXaEd72RIhOX-D3gI8UEqVaLodevrxGMveQwCcRhzT0c_4crolLi3e4aOJxoX18Pz7aUg5LfsEy94Uj8Efgk3RrbaEOOFpNgAesIkOh3j0UMJkSkhxg1Z8yDgtJVgzf8JQcnWteds3fT3ng5nxUvk-l-DhHTobzQz-_b95ju6-fvl59Y3c3F5_v7q8IbZhfSGjVbSV3EnhesGVG71ouRpkp-ww2J4p13CmZG-EE8oMyre8M9Z5NvjOed435-jjiVujf631af2Q1hxrpOaCqp61ksmq4ieVzQkg-1EvORxMftSM6q18fSpf1_L13_L1ZmpOJqjiOPn8gv6P6w9dPozO</recordid><startdate>20200601</startdate><enddate>20200601</enddate><creator>Ilik, Erkan</creator><creator>Kilic, Gokhan</creator><creator>Issever, U. Gokhan</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope><orcidid>https://orcid.org/0000-0001-7145-4999</orcidid><orcidid>https://orcid.org/0000-0003-2986-0015</orcidid><orcidid>https://orcid.org/0000-0002-6762-6898</orcidid></search><sort><creationdate>20200601</creationdate><title>Synthesis of novel AgO-doped vanadium–borophosphate semiconducting glasses and investigation of their optical, structural, and thermal properties</title><author>Ilik, Erkan ; Kilic, Gokhan ; Issever, U. Gokhan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-fc60752d54d9426dfe4726b586cbbc916d321659a4d46ab6e728acde1be8de293</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Boron oxides</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Crystallization</topic><topic>Glass transition temperature</topic><topic>Materials Science</topic><topic>Mathematical analysis</topic><topic>Melt temperature</topic><topic>Molar volume</topic><topic>Optical and Electronic Materials</topic><topic>Optical properties</topic><topic>Room temperature</topic><topic>Silver</topic><topic>Synthesis</topic><topic>Temperature</topic><topic>Thermodynamic properties</topic><topic>Vanadium compounds</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ilik, Erkan</creatorcontrib><creatorcontrib>Kilic, Gokhan</creatorcontrib><creatorcontrib>Issever, U. Gokhan</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ilik, Erkan</au><au>Kilic, Gokhan</au><au>Issever, U. Gokhan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of novel AgO-doped vanadium–borophosphate semiconducting glasses and investigation of their optical, structural, and thermal properties</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2020-06-01</date><risdate>2020</risdate><volume>31</volume><issue>11</issue><spage>8986</spage><epage>8995</epage><pages>8986-8995</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Ag-doped vanadium–borophosphate glasses having 46V
2
O
5
–46P
2
O
5
–(8 −
x
)B
2
O
3
–
x
AgO as the base structure have been successfully synthesized with different compositions of AgO (
x
= 0, 2, 4, 6, 8 mol%) by the conventional melt-quenching technique. Density and molar volume values were calculated by Archimedes principle. The transmittance and absorbance spectra, XRD, and FTIR measurements of the glasses were performed at room temperature. While XRD data showed that the glasses had an amorphous structure away from crystallization, FTIR spectra showed that vanadium and phosphate compounds forming the glass network consisted of VO
4
, VO
5
and PO
3
, PO
2
structural units, respectively. It was observed that AgO, which replaces B
2
O
3
, acted as a modifier in the glass network. Direct and indirect band gaps of synthesized glasses were calculated using Tauc method. Urbach energies were also calculated. The glass transition temperature, crystallization temperature, and melting temperature values of the samples were determined with differential scanning calorimetry (DSC) in the range of room temperature to 1000 °C.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-020-03432-5</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0001-7145-4999</orcidid><orcidid>https://orcid.org/0000-0003-2986-0015</orcidid><orcidid>https://orcid.org/0000-0002-6762-6898</orcidid></addata></record> |
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| ispartof | Journal of materials science. Materials in electronics, 2020-06, Vol.31 (11), p.8986-8995 |
| issn | 0957-4522 1573-482X |
| language | eng |
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| source | SpringerNature Journals |
| subjects | Boron oxides Characterization and Evaluation of Materials Chemistry and Materials Science Crystallization Glass transition temperature Materials Science Mathematical analysis Melt temperature Molar volume Optical and Electronic Materials Optical properties Room temperature Silver Synthesis Temperature Thermodynamic properties Vanadium compounds |
| title | Synthesis of novel AgO-doped vanadium–borophosphate semiconducting glasses and investigation of their optical, structural, and thermal properties |
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