Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin
In this research, a novel renewable biomaterial spongin of marine sponge origin has been used as adsorbent in a miniaturized method based on solid-phase extraction (SPE) for the pre-concentration and determination of ketamine. The subsequent determinations of ketamine have been performed by high-per...
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| Veröffentlicht in: | Applied physics. A, Materials science & processing Materials science & processing, 2020, Vol.126 (6), Article 421 |
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| container_title | Applied physics. A, Materials science & processing |
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| creator | Ashouri, Vahid Rahimi-Nasrabadi, Mehdi Attaran Fariman, Gilan Adib, Kourosh Zahedi, Mir Mahdi Ganjali, Mohammad Reza Marzi Khosrowshahi, Elnaz |
| description | In this research, a novel renewable biomaterial spongin of marine sponge origin has been used as adsorbent in a miniaturized method based on solid-phase extraction (SPE) for the pre-concentration and determination of ketamine. The subsequent determinations of ketamine have been performed by high-performance liquid chromatography. Various potential effective factors during extraction procedure including pH value, amount of adsorbent, elution volume and its type, washing volume and its ratio, extraction time and salt concentration of the sample solution were optimized. Under the optimized conditions, the linear dynamic range for ketamine determination was 10–1000 ng mL
−1
. The relative standard deviation (RSD%,
n
= 5) for determination of ketamine (20 ng mL
−1
) was 2.8%, and the calculated limit of detection was 1.7 ng mL
−1
. The developed SPE procedure has been successfully applied for analysis of ketamine in water, urine and apple juice samples with high precision and accuracy. |
| doi_str_mv | 10.1007/s00339-020-03598-z |
| format | Article |
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−1
. The relative standard deviation (RSD%,
n
= 5) for determination of ketamine (20 ng mL
−1
) was 2.8%, and the calculated limit of detection was 1.7 ng mL
−1
. The developed SPE procedure has been successfully applied for analysis of ketamine in water, urine and apple juice samples with high precision and accuracy.</description><identifier>ISSN: 0947-8396</identifier><identifier>EISSN: 1432-0630</identifier><identifier>DOI: 10.1007/s00339-020-03598-z</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Adsorbents ; Applied physics ; Biological and Biomimetic Materials – Honoring Prof. A. Darvizeh ; Biomedical materials ; Characterization and Evaluation of Materials ; Condensed Matter Physics ; Elution ; High performance liquid chromatography ; Ketamine ; Machines ; Manufacturing ; Materials science ; Nanotechnology ; Optical and Electronic Materials ; Physics ; Physics and Astronomy ; Processes ; Solid phases ; Surfaces and Interfaces ; T.C. Biological and Biomimetic Materials ; Thin Films</subject><ispartof>Applied physics. A, Materials science & processing, 2020, Vol.126 (6), Article 421</ispartof><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020</rights><rights>Springer-Verlag GmbH Germany, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c356t-8916ca2cb3c7b0067c667a66d63be46f51c8b9af5d9c6dde93d9399381b815e23</citedby><cites>FETCH-LOGICAL-c356t-8916ca2cb3c7b0067c667a66d63be46f51c8b9af5d9c6dde93d9399381b815e23</cites><orcidid>0000-0003-4926-2696</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00339-020-03598-z$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00339-020-03598-z$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Ashouri, Vahid</creatorcontrib><creatorcontrib>Rahimi-Nasrabadi, Mehdi</creatorcontrib><creatorcontrib>Attaran Fariman, Gilan</creatorcontrib><creatorcontrib>Adib, Kourosh</creatorcontrib><creatorcontrib>Zahedi, Mir Mahdi</creatorcontrib><creatorcontrib>Ganjali, Mohammad Reza</creatorcontrib><creatorcontrib>Marzi Khosrowshahi, Elnaz</creatorcontrib><title>Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin</title><title>Applied physics. A, Materials science & processing</title><addtitle>Appl. Phys. A</addtitle><description>In this research, a novel renewable biomaterial spongin of marine sponge origin has been used as adsorbent in a miniaturized method based on solid-phase extraction (SPE) for the pre-concentration and determination of ketamine. The subsequent determinations of ketamine have been performed by high-performance liquid chromatography. Various potential effective factors during extraction procedure including pH value, amount of adsorbent, elution volume and its type, washing volume and its ratio, extraction time and salt concentration of the sample solution were optimized. Under the optimized conditions, the linear dynamic range for ketamine determination was 10–1000 ng mL
−1
. The relative standard deviation (RSD%,
n
= 5) for determination of ketamine (20 ng mL
−1
) was 2.8%, and the calculated limit of detection was 1.7 ng mL
−1
. The developed SPE procedure has been successfully applied for analysis of ketamine in water, urine and apple juice samples with high precision and accuracy.</description><subject>Adsorbents</subject><subject>Applied physics</subject><subject>Biological and Biomimetic Materials – Honoring Prof. A. Darvizeh</subject><subject>Biomedical materials</subject><subject>Characterization and Evaluation of Materials</subject><subject>Condensed Matter Physics</subject><subject>Elution</subject><subject>High performance liquid chromatography</subject><subject>Ketamine</subject><subject>Machines</subject><subject>Manufacturing</subject><subject>Materials science</subject><subject>Nanotechnology</subject><subject>Optical and Electronic Materials</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Processes</subject><subject>Solid phases</subject><subject>Surfaces and Interfaces</subject><subject>T.C. Biological and Biomimetic Materials</subject><subject>Thin Films</subject><issn>0947-8396</issn><issn>1432-0630</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kM1KAzEURoMoWH9ewFXAdWoymclMllKqFQpudB0yyZ126kxSkynYPoTPbNoR3JnNhcs5H7kfQneMThml5UOklHNJaEYJ5YWsyOEMTVjOM0IFp-doQmVekopLcYmuYtzQ9PIsm6Dv-dcQtBla77B2Fm8DEOOdAZfWp61v8AcMum8d4HqPd7F1K6zxsA4AxLY9uJgw3eG49W7VOlLrCBZHo5vGd_boD2vAC921pktg4qa41-GYZ6H3Jw2wD22Sb9BFo7sIt7_zGr0_zd9mC7J8fX6ZPS6J4YUYSCWZMDozNTdlTakojRClFsIKXkMumoKZqpa6Kaw0wlqQ3EouJa9YXbECMn6N7sfcbfCfO4iD2vhdSFdEleWUM1YxeaSykTLBxxigUdvQpq_vFaPq2Lsae1epd3XqXR2SxEcpJjhdFv6i_7F-AIOliRs</recordid><startdate>2020</startdate><enddate>2020</enddate><creator>Ashouri, Vahid</creator><creator>Rahimi-Nasrabadi, Mehdi</creator><creator>Attaran Fariman, Gilan</creator><creator>Adib, Kourosh</creator><creator>Zahedi, Mir Mahdi</creator><creator>Ganjali, Mohammad Reza</creator><creator>Marzi Khosrowshahi, Elnaz</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-4926-2696</orcidid></search><sort><creationdate>2020</creationdate><title>Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin</title><author>Ashouri, Vahid ; Rahimi-Nasrabadi, Mehdi ; Attaran Fariman, Gilan ; Adib, Kourosh ; Zahedi, Mir Mahdi ; Ganjali, Mohammad Reza ; Marzi Khosrowshahi, Elnaz</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c356t-8916ca2cb3c7b0067c667a66d63be46f51c8b9af5d9c6dde93d9399381b815e23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Adsorbents</topic><topic>Applied physics</topic><topic>Biological and Biomimetic Materials – Honoring Prof. A. Darvizeh</topic><topic>Biomedical materials</topic><topic>Characterization and Evaluation of Materials</topic><topic>Condensed Matter Physics</topic><topic>Elution</topic><topic>High performance liquid chromatography</topic><topic>Ketamine</topic><topic>Machines</topic><topic>Manufacturing</topic><topic>Materials science</topic><topic>Nanotechnology</topic><topic>Optical and Electronic Materials</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Processes</topic><topic>Solid phases</topic><topic>Surfaces and Interfaces</topic><topic>T.C. Biological and Biomimetic Materials</topic><topic>Thin Films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ashouri, Vahid</creatorcontrib><creatorcontrib>Rahimi-Nasrabadi, Mehdi</creatorcontrib><creatorcontrib>Attaran Fariman, Gilan</creatorcontrib><creatorcontrib>Adib, Kourosh</creatorcontrib><creatorcontrib>Zahedi, Mir Mahdi</creatorcontrib><creatorcontrib>Ganjali, Mohammad Reza</creatorcontrib><creatorcontrib>Marzi Khosrowshahi, Elnaz</creatorcontrib><collection>CrossRef</collection><jtitle>Applied physics. A, Materials science & processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ashouri, Vahid</au><au>Rahimi-Nasrabadi, Mehdi</au><au>Attaran Fariman, Gilan</au><au>Adib, Kourosh</au><au>Zahedi, Mir Mahdi</au><au>Ganjali, Mohammad Reza</au><au>Marzi Khosrowshahi, Elnaz</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin</atitle><jtitle>Applied physics. A, Materials science & processing</jtitle><stitle>Appl. Phys. A</stitle><date>2020</date><risdate>2020</risdate><volume>126</volume><issue>6</issue><artnum>421</artnum><issn>0947-8396</issn><eissn>1432-0630</eissn><abstract>In this research, a novel renewable biomaterial spongin of marine sponge origin has been used as adsorbent in a miniaturized method based on solid-phase extraction (SPE) for the pre-concentration and determination of ketamine. The subsequent determinations of ketamine have been performed by high-performance liquid chromatography. Various potential effective factors during extraction procedure including pH value, amount of adsorbent, elution volume and its type, washing volume and its ratio, extraction time and salt concentration of the sample solution were optimized. Under the optimized conditions, the linear dynamic range for ketamine determination was 10–1000 ng mL
−1
. The relative standard deviation (RSD%,
n
= 5) for determination of ketamine (20 ng mL
−1
) was 2.8%, and the calculated limit of detection was 1.7 ng mL
−1
. The developed SPE procedure has been successfully applied for analysis of ketamine in water, urine and apple juice samples with high precision and accuracy.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s00339-020-03598-z</doi><orcidid>https://orcid.org/0000-0003-4926-2696</orcidid></addata></record> |
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| subjects | Adsorbents Applied physics Biological and Biomimetic Materials – Honoring Prof. A. Darvizeh Biomedical materials Characterization and Evaluation of Materials Condensed Matter Physics Elution High performance liquid chromatography Ketamine Machines Manufacturing Materials science Nanotechnology Optical and Electronic Materials Physics Physics and Astronomy Processes Solid phases Surfaces and Interfaces T.C. Biological and Biomimetic Materials Thin Films |
| title | Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin |
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