Procedure for the Precipitation of Iron, Chromium, Molybdenum, and Tungsten in the Determination of Arsenic and Antimony in Alloy Steels
A possibility of the separation of trace amounts of arsenic and antimony and macroquantities iron, chromium, molybdenum, and tungsten by the precipitation of the latter was investigated; regularities of the coprecipitation of arsenic and antimony are studied. The coprecipitation of arsenic and antim...
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| Veröffentlicht in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2020-05, Vol.75 (5), p.587-594 |
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| container_issue | 5 |
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| container_title | Journal of analytical chemistry (New York, N.Y.) |
| container_volume | 75 |
| creator | Maiorova, A. V. Belozerova, A. A. Okuneva, T. G. Shunyaev, K. Yu |
| description | A possibility of the separation of trace amounts of arsenic and antimony and macroquantities iron, chromium, molybdenum, and tungsten by the precipitation of the latter was investigated; regularities of the coprecipitation of arsenic and antimony are studied. The coprecipitation of arsenic and antimony in the precipitation of iron, chromium, molybdenum, and tungsten can be inhibited by introducing a certain amount of hydrofluoric acid. This decreases the specific surface and porosity of the precipitates and inhibits the coprecipitation process. A method is developed for the simultaneous determination of arsenic and antimony in alloy steels by inductively coupled plasma atomic emission spectrometry with preliminary separation of the main components of iron, chromium, molybdenum, and tungsten. |
| doi_str_mv | 10.1134/S1061934820050111 |
| format | Article |
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V.</creatorcontrib><creatorcontrib>Belozerova, A. A.</creatorcontrib><creatorcontrib>Okuneva, T. G.</creatorcontrib><creatorcontrib>Shunyaev, K. Yu</creatorcontrib><title>Procedure for the Precipitation of Iron, Chromium, Molybdenum, and Tungsten in the Determination of Arsenic and Antimony in Alloy Steels</title><title>Journal of analytical chemistry (New York, N.Y.)</title><addtitle>J Anal Chem</addtitle><description>A possibility of the separation of trace amounts of arsenic and antimony and macroquantities iron, chromium, molybdenum, and tungsten by the precipitation of the latter was investigated; regularities of the coprecipitation of arsenic and antimony are studied. The coprecipitation of arsenic and antimony in the precipitation of iron, chromium, molybdenum, and tungsten can be inhibited by introducing a certain amount of hydrofluoric acid. This decreases the specific surface and porosity of the precipitates and inhibits the coprecipitation process. A method is developed for the simultaneous determination of arsenic and antimony in alloy steels by inductively coupled plasma atomic emission spectrometry with preliminary separation of the main components of iron, chromium, molybdenum, and tungsten.</description><subject>Alloy steels</subject><subject>Alloys</subject><subject>Analytical Chemistry</subject><subject>Antimony</subject><subject>Arsenic</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromium</subject><subject>Coprecipitation</subject><subject>Ethylenediaminetetraacetic acid</subject><subject>Fluorides</subject><subject>Hydrofluoric acid</subject><subject>Inductively coupled plasma</subject><subject>Metallic elements</subject><subject>Molybdenum</subject><subject>Nonferrous metals</subject><subject>Porosity</subject><subject>Precipitates</subject><subject>Separation</subject><subject>Specialty metals industry</subject><subject>Tungsten</subject><issn>1061-9348</issn><issn>1608-3199</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1ks9q3DAQxk1poWmaB-hN0FMhTiRZtqWj2f5bSGjIpmchy2NHwZa2kgzdN-hjV86GhqUbzUGD5vd9YobJsg8EXxBSsMsNwRURBeMU4xITQl5lJ6TCPC-IEK9Tnsr5Un-bvQvhAWMsOKlOsj833mnoZg-odx7Fe0A3HrTZmqiicRa5Hq29s-dode_dZObpHF27cdd2YJdc2Q7dzXYIESwy9tHgM0Twk7H_DBofwBr9CDc2msnZ3QI34-h2aBMBxvA-e9OrMcDZ032a_fz65W71Pb_68W29aq5yzcoy5qxOHXLKFa3bWlSMpX5VOqJqS0UFA6YwA16WugIOvC_qtqIc6q6tu5rUojjNPu59t979miFE-eBmb9OXkhZCFIRVuHymBjWCNLZ30Ss9maBlU1EqCl7QhcqPUANY8Gp0FnqTng_4iyN8ig4mo48KPh0IEhPhdxzUHIJcb24PWbJntXcheOjl1ptJ-Z0kWC47Iv_bkaShe01IrB3APw_jZdFfy8C6lQ</recordid><startdate>20200501</startdate><enddate>20200501</enddate><creator>Maiorova, A. 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V.</creatorcontrib><creatorcontrib>Belozerova, A. A.</creatorcontrib><creatorcontrib>Okuneva, T. G.</creatorcontrib><creatorcontrib>Shunyaev, K. Yu</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maiorova, A. V.</au><au>Belozerova, A. A.</au><au>Okuneva, T. G.</au><au>Shunyaev, K. Yu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Procedure for the Precipitation of Iron, Chromium, Molybdenum, and Tungsten in the Determination of Arsenic and Antimony in Alloy Steels</atitle><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle><stitle>J Anal Chem</stitle><date>2020-05-01</date><risdate>2020</risdate><volume>75</volume><issue>5</issue><spage>587</spage><epage>594</epage><pages>587-594</pages><issn>1061-9348</issn><eissn>1608-3199</eissn><abstract>A possibility of the separation of trace amounts of arsenic and antimony and macroquantities iron, chromium, molybdenum, and tungsten by the precipitation of the latter was investigated; regularities of the coprecipitation of arsenic and antimony are studied. The coprecipitation of arsenic and antimony in the precipitation of iron, chromium, molybdenum, and tungsten can be inhibited by introducing a certain amount of hydrofluoric acid. This decreases the specific surface and porosity of the precipitates and inhibits the coprecipitation process. A method is developed for the simultaneous determination of arsenic and antimony in alloy steels by inductively coupled plasma atomic emission spectrometry with preliminary separation of the main components of iron, chromium, molybdenum, and tungsten.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1061934820050111</doi><tpages>8</tpages></addata></record> |
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| identifier | ISSN: 1061-9348 |
| ispartof | Journal of analytical chemistry (New York, N.Y.), 2020-05, Vol.75 (5), p.587-594 |
| issn | 1061-9348 1608-3199 |
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| subjects | Alloy steels Alloys Analytical Chemistry Antimony Arsenic Chemistry Chemistry and Materials Science Chromium Coprecipitation Ethylenediaminetetraacetic acid Fluorides Hydrofluoric acid Inductively coupled plasma Metallic elements Molybdenum Nonferrous metals Porosity Precipitates Separation Specialty metals industry Tungsten |
| title | Procedure for the Precipitation of Iron, Chromium, Molybdenum, and Tungsten in the Determination of Arsenic and Antimony in Alloy Steels |
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