Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature
In this study, catalyst formation [Pb(H 2 O) 6 ][ATZ]·H 2 O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H 2...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2020, Vol.140 (1), p.373-379 |
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| container_title | Journal of thermal analysis and calorimetry |
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| creator | Han, Zhiyue Gong, Li Du, Zhiming Tong, Wenchao Jiang, Qi Wen, Yu |
| description | In this study, catalyst formation [Pb(H
2
O)
6
][ATZ]·H
2
O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H
2
O)
6
][ATZ]·H
2
O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H
2
O)
6
][ATZ]·H
2
O can effectively reduce the decomposition temperature. In other words, [Pb(H
2
O)
6
][ATZ]·H
2
O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H
2
O)
6
][ATZ]·H
2
O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering. |
| doi_str_mv | 10.1007/s10973-019-08864-8 |
| format | Article |
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2
O)
6
][ATZ]·H
2
O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H
2
O)
6
][ATZ]·H
2
O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H
2
O)
6
][ATZ]·H
2
O can effectively reduce the decomposition temperature. In other words, [Pb(H
2
O)
6
][ATZ]·H
2
O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H
2
O)
6
][ATZ]·H
2
O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>DOI: 10.1007/s10973-019-08864-8</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Analytical Chemistry ; Catalysts ; Chemistry ; Chemistry and Materials Science ; Crystal structure ; Crystals ; Decomposition ; Explosive devices ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Nitrates ; Physical Chemistry ; Polymer Sciences ; Potassium ; Single crystals</subject><ispartof>Journal of thermal analysis and calorimetry, 2020, Vol.140 (1), p.373-379</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2019</rights><rights>2019© Akadémiai Kiadó, Budapest, Hungary 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2718-231dab73ce495127f61c5979932c3ac53a95754bb885eb2ba7769794230d42703</citedby><cites>FETCH-LOGICAL-c2718-231dab73ce495127f61c5979932c3ac53a95754bb885eb2ba7769794230d42703</cites><orcidid>0000-0002-8517-5760</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10973-019-08864-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10973-019-08864-8$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Han, Zhiyue</creatorcontrib><creatorcontrib>Gong, Li</creatorcontrib><creatorcontrib>Du, Zhiming</creatorcontrib><creatorcontrib>Tong, Wenchao</creatorcontrib><creatorcontrib>Jiang, Qi</creatorcontrib><creatorcontrib>Wen, Yu</creatorcontrib><title>Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>In this study, catalyst formation [Pb(H
2
O)
6
][ATZ]·H
2
O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H
2
O)
6
][ATZ]·H
2
O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H
2
O)
6
][ATZ]·H
2
O can effectively reduce the decomposition temperature. In other words, [Pb(H
2
O)
6
][ATZ]·H
2
O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H
2
O)
6
][ATZ]·H
2
O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.</description><subject>Analytical Chemistry</subject><subject>Catalysts</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Crystal structure</subject><subject>Crystals</subject><subject>Decomposition</subject><subject>Explosive devices</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Nitrates</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Potassium</subject><subject>Single crystals</subject><issn>1388-6150</issn><issn>1588-2926</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9UMlKAzEYHkTBuryAp4AXPYxmmWzHUtQKhQrWi6WETCajKc5ikjn0ybz7ZEZH8ObpX77l__my7AzBKwQhvw4ISk5yiGQOhWBFLvayCaJC5Fhitp96knqGKDzMjkLYQgilhGiSqcddG19tcAF0NVg_lBdzvLxkm_V09bz5_EgD0G0FXAzANb02EXQt6LuoQ3BDA1oXvY4WVNZ0Td8FF13Co216m_aDtyfZQa3fgj39rcfZ0-3NajbPF8u7-9l0kRvMUfqSoEqXnBhbSIowrxkyVHIpCTZEG0q0pJwWZSkEtSUuNecswQUmsCowh-Q4Ox99e9-9DzZEte0G36aTChMuGYeIFYmFR5bxXQje1qr3rtF-pxBU30GqMUiVglQ_QSqRRGQUhURuX6z_s_5H9QUTR3Vb</recordid><startdate>2020</startdate><enddate>2020</enddate><creator>Han, Zhiyue</creator><creator>Gong, Li</creator><creator>Du, Zhiming</creator><creator>Tong, Wenchao</creator><creator>Jiang, Qi</creator><creator>Wen, Yu</creator><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0002-8517-5760</orcidid></search><sort><creationdate>2020</creationdate><title>Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature</title><author>Han, Zhiyue ; Gong, Li ; Du, Zhiming ; Tong, Wenchao ; Jiang, Qi ; Wen, Yu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2718-231dab73ce495127f61c5979932c3ac53a95754bb885eb2ba7769794230d42703</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Analytical Chemistry</topic><topic>Catalysts</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Crystal structure</topic><topic>Crystals</topic><topic>Decomposition</topic><topic>Explosive devices</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Nitrates</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Potassium</topic><topic>Single crystals</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Han, Zhiyue</creatorcontrib><creatorcontrib>Gong, Li</creatorcontrib><creatorcontrib>Du, Zhiming</creatorcontrib><creatorcontrib>Tong, Wenchao</creatorcontrib><creatorcontrib>Jiang, Qi</creatorcontrib><creatorcontrib>Wen, Yu</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Han, Zhiyue</au><au>Gong, Li</au><au>Du, Zhiming</au><au>Tong, Wenchao</au><au>Jiang, Qi</au><au>Wen, Yu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2020</date><risdate>2020</risdate><volume>140</volume><issue>1</issue><spage>373</spage><epage>379</epage><pages>373-379</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><abstract>In this study, catalyst formation [Pb(H
2
O)
6
][ATZ]·H
2
O (ATZ = azo tetrazolium anion) was successfully synthesized originally; meanwhile, the single-crystal structure of the compound was cultivated and analyzed by diffraction single-crystal method. The influence of the compound in which [Pb(H
2
O)
6
][ATZ]·H
2
O was used as combustion catalyst on the decomposition temperature of potassium nitrate was studied by TG–DSC. The result proved that [Pb(H
2
O)
6
][ATZ]·H
2
O can effectively reduce the decomposition temperature. In other words, [Pb(H
2
O)
6
][ATZ]·H
2
O can reduce the decomposition temperature of potassium nitrate, so the addition of [Pb(H
2
O)
6
][ATZ]·H
2
O can make potassium nitrate better to be used in the fields of initiating explosive device and fire engineering.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s10973-019-08864-8</doi><tpages>7</tpages><orcidid>https://orcid.org/0000-0002-8517-5760</orcidid></addata></record> |
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| issn | 1388-6150 1588-2926 |
| language | eng |
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| source | SpringerNature Journals |
| subjects | Analytical Chemistry Catalysts Chemistry Chemistry and Materials Science Crystal structure Crystals Decomposition Explosive devices Inorganic Chemistry Measurement Science and Instrumentation Nitrates Physical Chemistry Polymer Sciences Potassium Single crystals |
| title | Synthesis of [Pb(H2O)6][ATZ]·H2O and its impact on potassium nitrate decomposition temperature |
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