Synthesis of Vanadium Diboride Nanoparticles via Reaction of VCl3 with NaBH4
— It has been shown using X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy, and elemental analysis that phase-pure VB 2 with an average particle size in the range 20–35 nm can be prepared in the temperature range 595–930°C by rea...
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| Veröffentlicht in: | Inorganic materials 2020-02, Vol.56 (2), p.126-131 |
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| container_title | Inorganic materials |
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| creator | Korobov, I. I. Kovalev, D. Yu Kalinnikov, G. V. Konovalikhin, S. V. Khomenko, N. Yu Vinokurov, A. A. Ivanov, A. V. Shilkin, S. P. |
| description | —
It has been shown using X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy, and elemental analysis that phase-pure VB
2
with an average particle size in the range 20–35 nm can be prepared in the temperature range 595–930°C by reacting vanadium(III) chloride and sodium borohydride in the molar ratio 1 : 10 in an argon atmosphere for 14–28 h. |
| doi_str_mv | 10.1134/S0020168520020065 |
| format | Article |
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It has been shown using X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy, and elemental analysis that phase-pure VB
2
with an average particle size in the range 20–35 nm can be prepared in the temperature range 595–930°C by reacting vanadium(III) chloride and sodium borohydride in the molar ratio 1 : 10 in an argon atmosphere for 14–28 h.</description><identifier>ISSN: 0020-1685</identifier><identifier>EISSN: 1608-3172</identifier><identifier>DOI: 10.1134/S0020168520020065</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Argon ; Chemistry ; Chemistry and Materials Science ; Industrial Chemistry/Chemical Engineering ; Inorganic Chemistry ; Materials Science ; Nanoparticles ; Photoelectrons ; Spectrum analysis ; Vanadium ; X-ray spectroscopy</subject><ispartof>Inorganic materials, 2020-02, Vol.56 (2), p.126-131</ispartof><rights>Pleiades Publishing, Ltd. 2020</rights><rights>2020© Pleiades Publishing, Ltd. 2020</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c396t-ffe2355d1e9e0ad4acf681fb0d56053d218d97f62b81a06907305074cf0a49143</citedby><cites>FETCH-LOGICAL-c396t-ffe2355d1e9e0ad4acf681fb0d56053d218d97f62b81a06907305074cf0a49143</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0020168520020065$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0020168520020065$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Korobov, I. I.</creatorcontrib><creatorcontrib>Kovalev, D. Yu</creatorcontrib><creatorcontrib>Kalinnikov, G. V.</creatorcontrib><creatorcontrib>Konovalikhin, S. V.</creatorcontrib><creatorcontrib>Khomenko, N. Yu</creatorcontrib><creatorcontrib>Vinokurov, A. A.</creatorcontrib><creatorcontrib>Ivanov, A. V.</creatorcontrib><creatorcontrib>Shilkin, S. P.</creatorcontrib><title>Synthesis of Vanadium Diboride Nanoparticles via Reaction of VCl3 with NaBH4</title><title>Inorganic materials</title><addtitle>Inorg Mater</addtitle><description>—
It has been shown using X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy, and elemental analysis that phase-pure VB
2
with an average particle size in the range 20–35 nm can be prepared in the temperature range 595–930°C by reacting vanadium(III) chloride and sodium borohydride in the molar ratio 1 : 10 in an argon atmosphere for 14–28 h.</description><subject>Argon</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Inorganic Chemistry</subject><subject>Materials Science</subject><subject>Nanoparticles</subject><subject>Photoelectrons</subject><subject>Spectrum analysis</subject><subject>Vanadium</subject><subject>X-ray spectroscopy</subject><issn>0020-1685</issn><issn>1608-3172</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1kE1LAzEQhoMoWKs_wFvA8-rkc5Oj1o8KRcGq1yXdJDal3dRkq_Tfu2sFD-JphpnnmYEXoVMC54QwfjEFoECkErRvQIo9NCASVMFISffRoJ8W_f4QHeW8AAAulB6gyXTbtHOXQ8bR41fTGBs2K3wdZjEF6_CDaeLapDbUS5fxRzD4yZm6DbH55kdLhj9DO--4qzE_RgfeLLM7-alD9HJ78zwaF5PHu_vR5aSomZZt4b2jTAhLnHZgLDe1l4r4GVghQTBLibK69JLOFDEgNZQMBJS89mC4JpwN0dnu7jrF943LbbWIm9R0LyvKSqU5ZZ0zRGRH1SnmnJyv1imsTNpWBKo-tOpPaJ1Dd07u2ObNpd_L_0tf-Bdrng</recordid><startdate>20200201</startdate><enddate>20200201</enddate><creator>Korobov, I. I.</creator><creator>Kovalev, D. Yu</creator><creator>Kalinnikov, G. V.</creator><creator>Konovalikhin, S. V.</creator><creator>Khomenko, N. Yu</creator><creator>Vinokurov, A. A.</creator><creator>Ivanov, A. V.</creator><creator>Shilkin, S. P.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20200201</creationdate><title>Synthesis of Vanadium Diboride Nanoparticles via Reaction of VCl3 with NaBH4</title><author>Korobov, I. I. ; Kovalev, D. Yu ; Kalinnikov, G. V. ; Konovalikhin, S. V. ; Khomenko, N. Yu ; Vinokurov, A. A. ; Ivanov, A. V. ; Shilkin, S. P.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c396t-ffe2355d1e9e0ad4acf681fb0d56053d218d97f62b81a06907305074cf0a49143</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Argon</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Inorganic Chemistry</topic><topic>Materials Science</topic><topic>Nanoparticles</topic><topic>Photoelectrons</topic><topic>Spectrum analysis</topic><topic>Vanadium</topic><topic>X-ray spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Korobov, I. I.</creatorcontrib><creatorcontrib>Kovalev, D. Yu</creatorcontrib><creatorcontrib>Kalinnikov, G. V.</creatorcontrib><creatorcontrib>Konovalikhin, S. V.</creatorcontrib><creatorcontrib>Khomenko, N. Yu</creatorcontrib><creatorcontrib>Vinokurov, A. A.</creatorcontrib><creatorcontrib>Ivanov, A. V.</creatorcontrib><creatorcontrib>Shilkin, S. P.</creatorcontrib><collection>CrossRef</collection><jtitle>Inorganic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Korobov, I. I.</au><au>Kovalev, D. Yu</au><au>Kalinnikov, G. V.</au><au>Konovalikhin, S. V.</au><au>Khomenko, N. Yu</au><au>Vinokurov, A. A.</au><au>Ivanov, A. V.</au><au>Shilkin, S. P.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Vanadium Diboride Nanoparticles via Reaction of VCl3 with NaBH4</atitle><jtitle>Inorganic materials</jtitle><stitle>Inorg Mater</stitle><date>2020-02-01</date><risdate>2020</risdate><volume>56</volume><issue>2</issue><spage>126</spage><epage>131</epage><pages>126-131</pages><issn>0020-1685</issn><eissn>1608-3172</eissn><abstract>—
It has been shown using X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, energy dispersive X-ray spectroscopy, and elemental analysis that phase-pure VB
2
with an average particle size in the range 20–35 nm can be prepared in the temperature range 595–930°C by reacting vanadium(III) chloride and sodium borohydride in the molar ratio 1 : 10 in an argon atmosphere for 14–28 h.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S0020168520020065</doi><tpages>6</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Argon Chemistry Chemistry and Materials Science Industrial Chemistry/Chemical Engineering Inorganic Chemistry Materials Science Nanoparticles Photoelectrons Spectrum analysis Vanadium X-ray spectroscopy |
| title | Synthesis of Vanadium Diboride Nanoparticles via Reaction of VCl3 with NaBH4 |
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