Transforming the amorphous Ti-Al-C coatings to high-purity Ti2AlC MAX phase coatings by prolonged annealing at 550 °C

•The synthesized temperature of Ti2AlC coating was significantly reduced here.•Ti2AlC coating was prepared by annealing amorphous Ti-Al-C coatings.•The formation mechanisms of Ti2AlC MAX phase were proposed in this study.•Prolonged annealing played a key role in reducing the synthesized temperature....

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Veröffentlicht in:Materials letters 2020-02, Vol.261, p.127160, Article 127160
Hauptverfasser: Wang, Zhenyu, Li, Wentao, Wang, Cuicui, Wu, Haichen, Ke, Peiling, Wang, Aiying
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container_start_page 127160
container_title Materials letters
container_volume 261
creator Wang, Zhenyu
Li, Wentao
Wang, Cuicui
Wu, Haichen
Ke, Peiling
Wang, Aiying
description •The synthesized temperature of Ti2AlC coating was significantly reduced here.•Ti2AlC coating was prepared by annealing amorphous Ti-Al-C coatings.•The formation mechanisms of Ti2AlC MAX phase were proposed in this study.•Prolonged annealing played a key role in reducing the synthesized temperature. Ti2AlC MAX phases have been considered as the promising protective coating materials in nuclear energy and other harsh environments due to their unique properties. However, high preparation temperatures of Ti2AlC coatings, generally ≥700 °C, are the main barriers to their further application on temperature-sensitive substrates. Taking the concept of surface dynamics during prolonged annealing at low-temperatures, herein we reported a quite facile strategy to fabricate high-purity Ti2AlC coatings by transforming amorphous Ti-Al-C coatings at 550 °C. The transformation mechanisms of Ti2AlC MAX phase were also discussed in terms of their microstructural evolutions.
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Ti2AlC MAX phases have been considered as the promising protective coating materials in nuclear energy and other harsh environments due to their unique properties. However, high preparation temperatures of Ti2AlC coatings, generally ≥700 °C, are the main barriers to their further application on temperature-sensitive substrates. Taking the concept of surface dynamics during prolonged annealing at low-temperatures, herein we reported a quite facile strategy to fabricate high-purity Ti2AlC coatings by transforming amorphous Ti-Al-C coatings at 550 °C. 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Ti2AlC MAX phases have been considered as the promising protective coating materials in nuclear energy and other harsh environments due to their unique properties. However, high preparation temperatures of Ti2AlC coatings, generally ≥700 °C, are the main barriers to their further application on temperature-sensitive substrates. Taking the concept of surface dynamics during prolonged annealing at low-temperatures, herein we reported a quite facile strategy to fabricate high-purity Ti2AlC coatings by transforming amorphous Ti-Al-C coatings at 550 °C. 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subjects Aluminum
Annealing
Ceramics
Low temperature
Materials science
MAX phase
Nuclear engineering
Nuclear reactors
Protective coatings
Purity
Structural
Substrates
Surface dynamics
Synthesis temperature
Ti2AlC coatings
Titanium
title Transforming the amorphous Ti-Al-C coatings to high-purity Ti2AlC MAX phase coatings by prolonged annealing at 550 °C
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