Effects of tungsten disulfide on microstructure and mechanical properties of AZ91 magnesium alloy manufactured by stir casting

In this work, AZ91 magnesium alloy reinforced with a low fraction (0–1) wt.% tungsten disulfide(WS2) microparticles have been fabricated using stir casting method. Effects of WS2 microparticles on mechanical properties, microstructure, and their correlation have been analyzed. The microstructure of...

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Veröffentlicht in:Journal of alloys and compounds 2020-03, Vol.817, p.153321, Article 153321
Hauptverfasser: Huang, Song-Jeng, Abbas, Aqeel
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description In this work, AZ91 magnesium alloy reinforced with a low fraction (0–1) wt.% tungsten disulfide(WS2) microparticles have been fabricated using stir casting method. Effects of WS2 microparticles on mechanical properties, microstructure, and their correlation have been analyzed. The microstructure of composites has been investigated by scanning electron microscope (SEM) equipped with energy dispersive spectroscopy (EDS) and X-ray diffractometer. Results indicate that density, hardness, ultimate tensile strength (UTS), and tensile ductility have a direct relation with reinforcement (WS2) contents and has optimal value for 0.6 wt% WS2/AZ91 composites then slightly decrease afterward. The UTS and hardness of 0.6 wt%WS2/AZ91 were increased by 23.23% and 10.65% respectively with respect to monolithic AZ91. The ultimate compressive strength(UCS) is directly related with WS2 concentration and 10.07% enhancement in UCS for 1 wt%WS2/AZ91 composites have been noted. The trend is interlinked with density and hardness of composites. SEM images depict, WS2 micro-particles suppress β-Mg17Al12 precipitates, refine the microstructure and enhance the grain size resulting in an increase in mechanical properties. The improvement in microstructure and mechanical properties is attributed to the dispersion of WS2 particles which hinder the grain growth. The increase in porosity has causes the decrease in mechanical behavior of 1 wt%WS2/AZ91. Twin boundary fracture has been found major fracture phenomenon in fractured WS2/AZ91 surfaces. •WS2/AZ91 metal matrix composites have been manufacture by stir casting method.•Density and porosity of WS2/AZ91 composites has been assessed.•Mechanical behavior under compression and tension has been analyzed.•Effect of WS2 on microstructure has been investigated.•Fracture behavior of composites has been studied.
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Effects of WS2 microparticles on mechanical properties, microstructure, and their correlation have been analyzed. The microstructure of composites has been investigated by scanning electron microscope (SEM) equipped with energy dispersive spectroscopy (EDS) and X-ray diffractometer. Results indicate that density, hardness, ultimate tensile strength (UTS), and tensile ductility have a direct relation with reinforcement (WS2) contents and has optimal value for 0.6 wt% WS2/AZ91 composites then slightly decrease afterward. The UTS and hardness of 0.6 wt%WS2/AZ91 were increased by 23.23% and 10.65% respectively with respect to monolithic AZ91. The ultimate compressive strength(UCS) is directly related with WS2 concentration and 10.07% enhancement in UCS for 1 wt%WS2/AZ91 composites have been noted. The trend is interlinked with density and hardness of composites. SEM images depict, WS2 micro-particles suppress β-Mg17Al12 precipitates, refine the microstructure and enhance the grain size resulting in an increase in mechanical properties. The improvement in microstructure and mechanical properties is attributed to the dispersion of WS2 particles which hinder the grain growth. The increase in porosity has causes the decrease in mechanical behavior of 1 wt%WS2/AZ91. Twin boundary fracture has been found major fracture phenomenon in fractured WS2/AZ91 surfaces. •WS2/AZ91 metal matrix composites have been manufacture by stir casting method.•Density and porosity of WS2/AZ91 composites has been assessed.•Mechanical behavior under compression and tension has been analyzed.•Effect of WS2 on microstructure has been investigated.•Fracture behavior of composites has been studied.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2019.153321</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Casting alloys ; Compressive strength ; Correlation analysis ; Density ; Density and porosity ; Fracture behavior ; Grain growth ; Grain size ; Hardness ; Image enhancement ; Magnesium alloys ; Magnesium base alloys ; Mechanical behavior ; Mechanical properties ; Metal matrix composites ; Microparticles ; Microstructure ; Particulate composites ; Porosity ; Precipitates ; Scanning electron microscopy ; Tungsten disulfide ; Twin boundaries ; Ultimate tensile strength ; WS2/AZ91</subject><ispartof>Journal of alloys and compounds, 2020-03, Vol.817, p.153321, Article 153321</ispartof><rights>2019 Elsevier B.V.</rights><rights>Copyright Elsevier BV Mar 15, 2020</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c337t-5331be958d8634b571bb2ff1241d5f2e62058ffe5041f280735ec7435d80d4a13</citedby><cites>FETCH-LOGICAL-c337t-5331be958d8634b571bb2ff1241d5f2e62058ffe5041f280735ec7435d80d4a13</cites><orcidid>0000-0002-6582-0339 ; 0000-0001-7724-9080</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jallcom.2019.153321$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Huang, Song-Jeng</creatorcontrib><creatorcontrib>Abbas, Aqeel</creatorcontrib><title>Effects of tungsten disulfide on microstructure and mechanical properties of AZ91 magnesium alloy manufactured by stir casting</title><title>Journal of alloys and compounds</title><description>In this work, AZ91 magnesium alloy reinforced with a low fraction (0–1) wt.% tungsten disulfide(WS2) microparticles have been fabricated using stir casting method. Effects of WS2 microparticles on mechanical properties, microstructure, and their correlation have been analyzed. The microstructure of composites has been investigated by scanning electron microscope (SEM) equipped with energy dispersive spectroscopy (EDS) and X-ray diffractometer. Results indicate that density, hardness, ultimate tensile strength (UTS), and tensile ductility have a direct relation with reinforcement (WS2) contents and has optimal value for 0.6 wt% WS2/AZ91 composites then slightly decrease afterward. The UTS and hardness of 0.6 wt%WS2/AZ91 were increased by 23.23% and 10.65% respectively with respect to monolithic AZ91. The ultimate compressive strength(UCS) is directly related with WS2 concentration and 10.07% enhancement in UCS for 1 wt%WS2/AZ91 composites have been noted. The trend is interlinked with density and hardness of composites. SEM images depict, WS2 micro-particles suppress β-Mg17Al12 precipitates, refine the microstructure and enhance the grain size resulting in an increase in mechanical properties. The improvement in microstructure and mechanical properties is attributed to the dispersion of WS2 particles which hinder the grain growth. The increase in porosity has causes the decrease in mechanical behavior of 1 wt%WS2/AZ91. Twin boundary fracture has been found major fracture phenomenon in fractured WS2/AZ91 surfaces. •WS2/AZ91 metal matrix composites have been manufacture by stir casting method.•Density and porosity of WS2/AZ91 composites has been assessed.•Mechanical behavior under compression and tension has been analyzed.•Effect of WS2 on microstructure has been investigated.•Fracture behavior of composites has been studied.</description><subject>Casting alloys</subject><subject>Compressive strength</subject><subject>Correlation analysis</subject><subject>Density</subject><subject>Density and porosity</subject><subject>Fracture behavior</subject><subject>Grain growth</subject><subject>Grain size</subject><subject>Hardness</subject><subject>Image enhancement</subject><subject>Magnesium alloys</subject><subject>Magnesium base alloys</subject><subject>Mechanical behavior</subject><subject>Mechanical properties</subject><subject>Metal matrix composites</subject><subject>Microparticles</subject><subject>Microstructure</subject><subject>Particulate composites</subject><subject>Porosity</subject><subject>Precipitates</subject><subject>Scanning electron microscopy</subject><subject>Tungsten disulfide</subject><subject>Twin boundaries</subject><subject>Ultimate tensile strength</subject><subject>WS2/AZ91</subject><issn>0925-8388</issn><issn>1873-4669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNqFkEtr3DAUhUVpINNJf0JA0LWneli2vCrDkKaBgWzSTTdClq6mMrY8leTCbPrbq3nss7pcOOfcez6EHinZUEKbr8Nm0ONo5mnDCO02VHDO6Ae0orLlVd003Ue0Ih0TleRS3qNPKQ2EFCWnK_TvyTkwOeHZ4byEQ8oQsPVpGZ23gOeAJ2_inHJcTF4iYB0snsD81sEbPeJjnI8Qs4dLwvZXR_GkDwGSXyZcvppPZQ-L0xe3xf0Jp-wjNrqMcHhAd06PCT7f5hr9_P70tvtR7V-fX3bbfWU4b3NVGtEeOiGtbHjdi5b2PXOOsppa4Rg0jAhZighSU8ckabkA09ZcWElsrSlfoy_X3PLvnwVSVsO8xFBOKsYFJ5wJ3haVuKrOjVMEp47RTzqeFCXqjFoN6oZanVGrK-ri-3b1Qanw10NUyXgIBqyPBa6ys38n4T8tQ4t9</recordid><startdate>20200315</startdate><enddate>20200315</enddate><creator>Huang, Song-Jeng</creator><creator>Abbas, Aqeel</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0002-6582-0339</orcidid><orcidid>https://orcid.org/0000-0001-7724-9080</orcidid></search><sort><creationdate>20200315</creationdate><title>Effects of tungsten disulfide on microstructure and mechanical properties of AZ91 magnesium alloy manufactured by stir casting</title><author>Huang, Song-Jeng ; Abbas, Aqeel</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c337t-5331be958d8634b571bb2ff1241d5f2e62058ffe5041f280735ec7435d80d4a13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Casting alloys</topic><topic>Compressive strength</topic><topic>Correlation analysis</topic><topic>Density</topic><topic>Density and porosity</topic><topic>Fracture behavior</topic><topic>Grain growth</topic><topic>Grain size</topic><topic>Hardness</topic><topic>Image enhancement</topic><topic>Magnesium alloys</topic><topic>Magnesium base alloys</topic><topic>Mechanical behavior</topic><topic>Mechanical properties</topic><topic>Metal matrix composites</topic><topic>Microparticles</topic><topic>Microstructure</topic><topic>Particulate composites</topic><topic>Porosity</topic><topic>Precipitates</topic><topic>Scanning electron microscopy</topic><topic>Tungsten disulfide</topic><topic>Twin boundaries</topic><topic>Ultimate tensile strength</topic><topic>WS2/AZ91</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Huang, Song-Jeng</creatorcontrib><creatorcontrib>Abbas, Aqeel</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of alloys and compounds</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Huang, Song-Jeng</au><au>Abbas, Aqeel</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effects of tungsten disulfide on microstructure and mechanical properties of AZ91 magnesium alloy manufactured by stir casting</atitle><jtitle>Journal of alloys and compounds</jtitle><date>2020-03-15</date><risdate>2020</risdate><volume>817</volume><spage>153321</spage><pages>153321-</pages><artnum>153321</artnum><issn>0925-8388</issn><eissn>1873-4669</eissn><abstract>In this work, AZ91 magnesium alloy reinforced with a low fraction (0–1) wt.% tungsten disulfide(WS2) microparticles have been fabricated using stir casting method. Effects of WS2 microparticles on mechanical properties, microstructure, and their correlation have been analyzed. The microstructure of composites has been investigated by scanning electron microscope (SEM) equipped with energy dispersive spectroscopy (EDS) and X-ray diffractometer. Results indicate that density, hardness, ultimate tensile strength (UTS), and tensile ductility have a direct relation with reinforcement (WS2) contents and has optimal value for 0.6 wt% WS2/AZ91 composites then slightly decrease afterward. The UTS and hardness of 0.6 wt%WS2/AZ91 were increased by 23.23% and 10.65% respectively with respect to monolithic AZ91. The ultimate compressive strength(UCS) is directly related with WS2 concentration and 10.07% enhancement in UCS for 1 wt%WS2/AZ91 composites have been noted. The trend is interlinked with density and hardness of composites. SEM images depict, WS2 micro-particles suppress β-Mg17Al12 precipitates, refine the microstructure and enhance the grain size resulting in an increase in mechanical properties. The improvement in microstructure and mechanical properties is attributed to the dispersion of WS2 particles which hinder the grain growth. The increase in porosity has causes the decrease in mechanical behavior of 1 wt%WS2/AZ91. Twin boundary fracture has been found major fracture phenomenon in fractured WS2/AZ91 surfaces. •WS2/AZ91 metal matrix composites have been manufacture by stir casting method.•Density and porosity of WS2/AZ91 composites has been assessed.•Mechanical behavior under compression and tension has been analyzed.•Effect of WS2 on microstructure has been investigated.•Fracture behavior of composites has been studied.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2019.153321</doi><orcidid>https://orcid.org/0000-0002-6582-0339</orcidid><orcidid>https://orcid.org/0000-0001-7724-9080</orcidid></addata></record>
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subjects Casting alloys
Compressive strength
Correlation analysis
Density
Density and porosity
Fracture behavior
Grain growth
Grain size
Hardness
Image enhancement
Magnesium alloys
Magnesium base alloys
Mechanical behavior
Mechanical properties
Metal matrix composites
Microparticles
Microstructure
Particulate composites
Porosity
Precipitates
Scanning electron microscopy
Tungsten disulfide
Twin boundaries
Ultimate tensile strength
WS2/AZ91
title Effects of tungsten disulfide on microstructure and mechanical properties of AZ91 magnesium alloy manufactured by stir casting
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