Flash sintering of 3YSZ/Al2O3‐platelet composites

Preparation of 3YSZ/Al2O3‐platelet composites always requires high temperature, long duration, and/or high pressure. Herein, 3YSZ/Al2O3‐platelet composites are prepared at low temperature of 492°C‐645°C in 30 seconds by flash sintering under the electric field of 300‐800 V/cm. The influence of elect...

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Veröffentlicht in:Journal of the American Ceramic Society 2020-04, Vol.103 (4), p.2351-2361
Hauptverfasser: Jia, Yongjie, Su, Xinghua, Wu, Yajuan, Wang, Zhenjun, Meng, Leichao, Xu, Xiqing, Zhang, Anni
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container_issue 4
container_start_page 2351
container_title Journal of the American Ceramic Society
container_volume 103
creator Jia, Yongjie
Su, Xinghua
Wu, Yajuan
Wang, Zhenjun
Meng, Leichao
Xu, Xiqing
Zhang, Anni
description Preparation of 3YSZ/Al2O3‐platelet composites always requires high temperature, long duration, and/or high pressure. Herein, 3YSZ/Al2O3‐platelet composites are prepared at low temperature of 492°C‐645°C in 30 seconds by flash sintering under the electric field of 300‐800 V/cm. The influence of electric field and current limit on the densification and grain growth of composites is investigated. The onset temperature for flash sintering is determined by electric field, which is decreased with increasing the electric field. Under the constant electric field, the current limit has a great effect on the density and grain size of composite. The flash‐sintered 3YSZ/Al2O3‐platelet composites exhibit relatively high hardness and elastic modulus. Both Joule heating and defects generation are proposed to be responsible for the rapid densification in flash sintering. This work demonstrates the feasibility of employing the flash sintering to prepare ceramic composites with fine grain size.
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subjects Aluminum oxide
ceramic matrix composites
Composite materials
Crystal defects
defects
Densification
Electric fields
flash sintering
Grain growth
Grain size
High temperature
Low temperature
Modulus of elasticity
Ohmic dissipation
Resistance heating
Resistance sintering
Sintering
title Flash sintering of 3YSZ/Al2O3‐platelet composites
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