Evaluation of Dispersive Solid-Phase Extraction (d-SPE) as a Clean-up Step for Phenolic Compound Determination of Myrciaria cauliflora Peel
In this study, dispersive solid-phase extraction (d-SPE) was evaluated as a clean-up step for the determination of phenolic compounds in Myrciaria cauliflora peel using an ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method. For the d-SPE clean-up step, the sor...
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| Veröffentlicht in: | Food analytical methods 2020, Vol.13 (1), p.155-165 |
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| creator | Senes, Carlos Eduardo Rubio Nicácio, Antonio Eduardo Rodrigues, Carina Alexandra Manin, Luciana Pelissari Maldaner, Liane Visentainer, Jesuí Vergílio |
| description | In this study, dispersive solid-phase extraction (d-SPE) was evaluated as a clean-up step for the determination of phenolic compounds in
Myrciaria cauliflora
peel using an ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method. For the d-SPE clean-up step, the sorbents, diatomaceous earth (DE), chitosan (CT), and graphitized carbon black (GCB), were evaluated in different proportions. The d-SPE clean-up step efficiency was evaluated through total anthocyanin content (ACC) and spectrophotometric scanning of the extracts. The use of DE with GCB in a ratio of 100:10 (
m
/
m
) was the best clean-up step condition. The ACC showed an 83% reduction of the amount of anthocyanins, and the scanning spectra confirmed that all extracts submitted to the clean-up step presented pigment reduction. A total of eight compounds were found in
M. cauliflora
peel, with the highest abundance of ellagic acid (1643 ± 353 mg kg
−1
), gallic acid (252 ± 10 mg kg
−1
), and 4-hydroxybenzoic acid (154 ± 133 mg kg
−1
), indicating the antioxidant potential of the peel, which is frequently considered a by-product of
Myrciaria cauliflora
fruits. |
| doi_str_mv | 10.1007/s12161-019-01566-9 |
| format | Article |
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Myrciaria cauliflora
peel using an ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method. For the d-SPE clean-up step, the sorbents, diatomaceous earth (DE), chitosan (CT), and graphitized carbon black (GCB), were evaluated in different proportions. The d-SPE clean-up step efficiency was evaluated through total anthocyanin content (ACC) and spectrophotometric scanning of the extracts. The use of DE with GCB in a ratio of 100:10 (
m
/
m
) was the best clean-up step condition. The ACC showed an 83% reduction of the amount of anthocyanins, and the scanning spectra confirmed that all extracts submitted to the clean-up step presented pigment reduction. A total of eight compounds were found in
M. cauliflora
peel, with the highest abundance of ellagic acid (1643 ± 353 mg kg
−1
), gallic acid (252 ± 10 mg kg
−1
), and 4-hydroxybenzoic acid (154 ± 133 mg kg
−1
), indicating the antioxidant potential of the peel, which is frequently considered a by-product of
Myrciaria cauliflora
fruits.</description><identifier>ISSN: 1936-9751</identifier><identifier>EISSN: 1936-976X</identifier><identifier>DOI: 10.1007/s12161-019-01566-9</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Analytical Chemistry ; Anthocyanins ; Antioxidants ; Black carbon ; Carbon black ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Chitosan ; Diatomaceous earth ; Dispersion ; Ellagic acid ; Environmental cleanup ; Food Science ; Gallic acid ; Graphitization ; High performance liquid chromatography ; Liquid chromatography ; Mass spectrometry ; Mass spectroscopy ; Microbiology ; Myrciaria cauliflora ; p-Hydroxybenzoic acid ; Phenolic compounds ; Phenols ; Reduction ; Scanning ; Solid phases ; Sorbents ; Spectrophotometry</subject><ispartof>Food analytical methods, 2020, Vol.13 (1), p.155-165</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2019</rights><rights>2019© Springer Science+Business Media, LLC, part of Springer Nature 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-dc9048598129598f25b8fdb02a4a4a2068591e11ead1788415651f48bd03e2d23</citedby><cites>FETCH-LOGICAL-c319t-dc9048598129598f25b8fdb02a4a4a2068591e11ead1788415651f48bd03e2d23</cites><orcidid>0000-0003-3860-4646</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s12161-019-01566-9$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s12161-019-01566-9$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Senes, Carlos Eduardo Rubio</creatorcontrib><creatorcontrib>Nicácio, Antonio Eduardo</creatorcontrib><creatorcontrib>Rodrigues, Carina Alexandra</creatorcontrib><creatorcontrib>Manin, Luciana Pelissari</creatorcontrib><creatorcontrib>Maldaner, Liane</creatorcontrib><creatorcontrib>Visentainer, Jesuí Vergílio</creatorcontrib><title>Evaluation of Dispersive Solid-Phase Extraction (d-SPE) as a Clean-up Step for Phenolic Compound Determination of Myrciaria cauliflora Peel</title><title>Food analytical methods</title><addtitle>Food Anal. Methods</addtitle><description>In this study, dispersive solid-phase extraction (d-SPE) was evaluated as a clean-up step for the determination of phenolic compounds in
Myrciaria cauliflora
peel using an ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method. For the d-SPE clean-up step, the sorbents, diatomaceous earth (DE), chitosan (CT), and graphitized carbon black (GCB), were evaluated in different proportions. The d-SPE clean-up step efficiency was evaluated through total anthocyanin content (ACC) and spectrophotometric scanning of the extracts. The use of DE with GCB in a ratio of 100:10 (
m
/
m
) was the best clean-up step condition. The ACC showed an 83% reduction of the amount of anthocyanins, and the scanning spectra confirmed that all extracts submitted to the clean-up step presented pigment reduction. A total of eight compounds were found in
M. cauliflora
peel, with the highest abundance of ellagic acid (1643 ± 353 mg kg
−1
), gallic acid (252 ± 10 mg kg
−1
), and 4-hydroxybenzoic acid (154 ± 133 mg kg
−1
), indicating the antioxidant potential of the peel, which is frequently considered a by-product of
Myrciaria cauliflora
fruits.</description><subject>Analytical Chemistry</subject><subject>Anthocyanins</subject><subject>Antioxidants</subject><subject>Black carbon</subject><subject>Carbon black</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Chitosan</subject><subject>Diatomaceous earth</subject><subject>Dispersion</subject><subject>Ellagic acid</subject><subject>Environmental cleanup</subject><subject>Food Science</subject><subject>Gallic acid</subject><subject>Graphitization</subject><subject>High performance liquid chromatography</subject><subject>Liquid chromatography</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Microbiology</subject><subject>Myrciaria cauliflora</subject><subject>p-Hydroxybenzoic acid</subject><subject>Phenolic compounds</subject><subject>Phenols</subject><subject>Reduction</subject><subject>Scanning</subject><subject>Solid phases</subject><subject>Sorbents</subject><subject>Spectrophotometry</subject><issn>1936-9751</issn><issn>1936-976X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kNtKw0AQhoMoWKsv4NWCN3oR3dmcL6WNB6gYqIJ3yzaZtVvSbNxNin0GX9q1kXonwxxg_n8GPs87B3oNlCY3FhjE4FPIXEZx7GcH3giywA1J_Ha4nyM49k6sXVEa0xDYyPvKN6LuRad0Q7QkU2VbNFZtkMx1rSq_WAqLJP_sjCh3osvKnxf5FRGWCDKpUTR-35J5hy2R2pBiiY0zlmSi163um4pMsUOzVs3-x9PWlEoYJUgp-lrJWhtBCsT61DuSorZ49tvH3utd_jJ58GfP94-T25lfBpB1flVmNEyjLAWWuSpZtEhltaBMhC4Yjd0OEABFBUmaho5HBDJMFxUNkFUsGHsXw93W6I8ebcdXujeNe8lZEAYsDZMYnIoNqtJoaw1K3hq1FmbLgfIf6HyAzh10voPOM2cKBpN14uYdzd_pf1zfaS2Enw</recordid><startdate>2020</startdate><enddate>2020</enddate><creator>Senes, Carlos Eduardo Rubio</creator><creator>Nicácio, Antonio Eduardo</creator><creator>Rodrigues, Carina Alexandra</creator><creator>Manin, Luciana Pelissari</creator><creator>Maldaner, Liane</creator><creator>Visentainer, Jesuí Vergílio</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-3860-4646</orcidid></search><sort><creationdate>2020</creationdate><title>Evaluation of Dispersive Solid-Phase Extraction (d-SPE) as a Clean-up Step for Phenolic Compound Determination of Myrciaria cauliflora Peel</title><author>Senes, Carlos Eduardo Rubio ; Nicácio, Antonio Eduardo ; Rodrigues, Carina Alexandra ; Manin, Luciana Pelissari ; Maldaner, Liane ; Visentainer, Jesuí Vergílio</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-dc9048598129598f25b8fdb02a4a4a2068591e11ead1788415651f48bd03e2d23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Analytical Chemistry</topic><topic>Anthocyanins</topic><topic>Antioxidants</topic><topic>Black carbon</topic><topic>Carbon black</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Chitosan</topic><topic>Diatomaceous earth</topic><topic>Dispersion</topic><topic>Ellagic acid</topic><topic>Environmental cleanup</topic><topic>Food Science</topic><topic>Gallic acid</topic><topic>Graphitization</topic><topic>High performance liquid chromatography</topic><topic>Liquid chromatography</topic><topic>Mass spectrometry</topic><topic>Mass spectroscopy</topic><topic>Microbiology</topic><topic>Myrciaria cauliflora</topic><topic>p-Hydroxybenzoic acid</topic><topic>Phenolic compounds</topic><topic>Phenols</topic><topic>Reduction</topic><topic>Scanning</topic><topic>Solid phases</topic><topic>Sorbents</topic><topic>Spectrophotometry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Senes, Carlos Eduardo Rubio</creatorcontrib><creatorcontrib>Nicácio, Antonio Eduardo</creatorcontrib><creatorcontrib>Rodrigues, Carina Alexandra</creatorcontrib><creatorcontrib>Manin, Luciana Pelissari</creatorcontrib><creatorcontrib>Maldaner, Liane</creatorcontrib><creatorcontrib>Visentainer, Jesuí Vergílio</creatorcontrib><collection>CrossRef</collection><jtitle>Food analytical methods</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Senes, Carlos Eduardo Rubio</au><au>Nicácio, Antonio Eduardo</au><au>Rodrigues, Carina Alexandra</au><au>Manin, Luciana Pelissari</au><au>Maldaner, Liane</au><au>Visentainer, Jesuí Vergílio</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Evaluation of Dispersive Solid-Phase Extraction (d-SPE) as a Clean-up Step for Phenolic Compound Determination of Myrciaria cauliflora Peel</atitle><jtitle>Food analytical methods</jtitle><stitle>Food Anal. Methods</stitle><date>2020</date><risdate>2020</risdate><volume>13</volume><issue>1</issue><spage>155</spage><epage>165</epage><pages>155-165</pages><issn>1936-9751</issn><eissn>1936-976X</eissn><abstract>In this study, dispersive solid-phase extraction (d-SPE) was evaluated as a clean-up step for the determination of phenolic compounds in
Myrciaria cauliflora
peel using an ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method. For the d-SPE clean-up step, the sorbents, diatomaceous earth (DE), chitosan (CT), and graphitized carbon black (GCB), were evaluated in different proportions. The d-SPE clean-up step efficiency was evaluated through total anthocyanin content (ACC) and spectrophotometric scanning of the extracts. The use of DE with GCB in a ratio of 100:10 (
m
/
m
) was the best clean-up step condition. The ACC showed an 83% reduction of the amount of anthocyanins, and the scanning spectra confirmed that all extracts submitted to the clean-up step presented pigment reduction. A total of eight compounds were found in
M. cauliflora
peel, with the highest abundance of ellagic acid (1643 ± 353 mg kg
−1
), gallic acid (252 ± 10 mg kg
−1
), and 4-hydroxybenzoic acid (154 ± 133 mg kg
−1
), indicating the antioxidant potential of the peel, which is frequently considered a by-product of
Myrciaria cauliflora
fruits.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s12161-019-01566-9</doi><tpages>11</tpages><orcidid>https://orcid.org/0000-0003-3860-4646</orcidid></addata></record> |
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| subjects | Analytical Chemistry Anthocyanins Antioxidants Black carbon Carbon black Chemistry Chemistry and Materials Science Chemistry/Food Science Chitosan Diatomaceous earth Dispersion Ellagic acid Environmental cleanup Food Science Gallic acid Graphitization High performance liquid chromatography Liquid chromatography Mass spectrometry Mass spectroscopy Microbiology Myrciaria cauliflora p-Hydroxybenzoic acid Phenolic compounds Phenols Reduction Scanning Solid phases Sorbents Spectrophotometry |
| title | Evaluation of Dispersive Solid-Phase Extraction (d-SPE) as a Clean-up Step for Phenolic Compound Determination of Myrciaria cauliflora Peel |
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