Green protocol for synthesis of MgFe2O4 nanoparticles and study of their activity as an efficient catalyst for the synthesis of chromene and pyran derivatives under ultrasound irradiation
In this study, the MgFe 2 O 4 nanoparticles were synthesized via a green and simple approach. Then an effective procedure to synthesize 2-amino-7-hydroxy-4 H -chromene and tetrahydrobenzo[ b ]pyran derivatives was established through the chemical reaction between different aldehydes, malononitrile a...
Gespeichert in:
| Veröffentlicht in: | Journal of the Iranian Chemical Society 2020-02, Vol.17 (2), p.469-481 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 481 |
|---|---|
| container_issue | 2 |
| container_start_page | 469 |
| container_title | Journal of the Iranian Chemical Society |
| container_volume | 17 |
| creator | Eshtehardian, Bahar Rouhani, Morteza Mirjafary, Zohreh |
| description | In this study, the MgFe
2
O
4
nanoparticles were synthesized via a green and simple approach. Then an effective procedure to synthesize 2-amino-7-hydroxy-4
H
-chromene and tetrahydrobenzo[
b
]pyran derivatives was established through the chemical reaction between different aldehydes, malononitrile and resorcinol (or dimedone) in the presence of MgFe
2
O
4
nanoparticles as a beneficial catalyst in ethanol as solvent under ultrasound irradiation. Moreover, the synthesized MgFe
2
O
4
nanoparticles were easily recovered by an external magnet and reused for four times without significant loss of their catalytic activity. Simple, fast, effective and eco-friendly as well as quick purification method along with high product yields are some of the advantages of the present chemical reaction. |
| doi_str_mv | 10.1007/s13738-019-01783-3 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2343270182</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2343270182</sourcerecordid><originalsourceid>FETCH-LOGICAL-c356t-28d9a9219558aeddd1b11fd2cc890dc82208684489dfeab4be6e589e1fe25813</originalsourceid><addsrcrecordid>eNp9kctKBDEQRRtR8PkDrgKuW_Ponk4vRRwVFDcu3IVMUtFIm4yV9EB_mz9nZkYRNy5Cpah7T0Hdqjpl9JxR2l0kJjoha8r68joparFTHbBOtDVvuNz9-dPueb86TOmN0rajbXNQfd4gQCBLjDmaOBAXkaQp5FdIPpHoyMPLHPhjQ4IOcakxezNAIjpYkvJop7WkiD0SbbJf-TwRvR4TcM4bDyETo7MeppQ37KL9yzevGN8hwAa5nLBYLaBf6UIri8ZQOjIOGXWKpSEeUVtfpjEcV3tODwlOvutR9TS_frq6re8fb-6uLu9rI9pZrrm0ve4569tWarDWsgVjznJjZE-tkZxTOZNNI3vrQC-aBcyglT0wB7yVTBxVZ1tsOdLHCCmrtzhiKBsVF43gHWWSFxXfqgzGlBCcWqJ_1zgpRtU6I7XNSJWM1CYjJYpJbE2piMML4C_6H9cXyi-Z8w</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2343270182</pqid></control><display><type>article</type><title>Green protocol for synthesis of MgFe2O4 nanoparticles and study of their activity as an efficient catalyst for the synthesis of chromene and pyran derivatives under ultrasound irradiation</title><source>SpringerLink Journals - AutoHoldings</source><creator>Eshtehardian, Bahar ; Rouhani, Morteza ; Mirjafary, Zohreh</creator><creatorcontrib>Eshtehardian, Bahar ; Rouhani, Morteza ; Mirjafary, Zohreh</creatorcontrib><description>In this study, the MgFe
2
O
4
nanoparticles were synthesized via a green and simple approach. Then an effective procedure to synthesize 2-amino-7-hydroxy-4
H
-chromene and tetrahydrobenzo[
b
]pyran derivatives was established through the chemical reaction between different aldehydes, malononitrile and resorcinol (or dimedone) in the presence of MgFe
2
O
4
nanoparticles as a beneficial catalyst in ethanol as solvent under ultrasound irradiation. Moreover, the synthesized MgFe
2
O
4
nanoparticles were easily recovered by an external magnet and reused for four times without significant loss of their catalytic activity. Simple, fast, effective and eco-friendly as well as quick purification method along with high product yields are some of the advantages of the present chemical reaction.</description><identifier>ISSN: 1735-207X</identifier><identifier>EISSN: 1735-2428</identifier><identifier>DOI: 10.1007/s13738-019-01783-3</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Aldehydes ; Analytical Chemistry ; Biochemistry ; Catalysts ; Catalytic activity ; Chemical reactions ; Chemical synthesis ; Chemistry ; Chemistry and Materials Science ; Derivatives ; Ethanol ; Inorganic Chemistry ; Irradiation ; Malononitrile ; Nanoparticles ; Organic Chemistry ; Original Paper ; Physical Chemistry ; Ultrasonic imaging ; Ultrasound</subject><ispartof>Journal of the Iranian Chemical Society, 2020-02, Vol.17 (2), p.469-481</ispartof><rights>Iranian Chemical Society 2019</rights><rights>2019© Iranian Chemical Society 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c356t-28d9a9219558aeddd1b11fd2cc890dc82208684489dfeab4be6e589e1fe25813</citedby><cites>FETCH-LOGICAL-c356t-28d9a9219558aeddd1b11fd2cc890dc82208684489dfeab4be6e589e1fe25813</cites><orcidid>0000-0002-6708-6131</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s13738-019-01783-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s13738-019-01783-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Eshtehardian, Bahar</creatorcontrib><creatorcontrib>Rouhani, Morteza</creatorcontrib><creatorcontrib>Mirjafary, Zohreh</creatorcontrib><title>Green protocol for synthesis of MgFe2O4 nanoparticles and study of their activity as an efficient catalyst for the synthesis of chromene and pyran derivatives under ultrasound irradiation</title><title>Journal of the Iranian Chemical Society</title><addtitle>J IRAN CHEM SOC</addtitle><description>In this study, the MgFe
2
O
4
nanoparticles were synthesized via a green and simple approach. Then an effective procedure to synthesize 2-amino-7-hydroxy-4
H
-chromene and tetrahydrobenzo[
b
]pyran derivatives was established through the chemical reaction between different aldehydes, malononitrile and resorcinol (or dimedone) in the presence of MgFe
2
O
4
nanoparticles as a beneficial catalyst in ethanol as solvent under ultrasound irradiation. Moreover, the synthesized MgFe
2
O
4
nanoparticles were easily recovered by an external magnet and reused for four times without significant loss of their catalytic activity. Simple, fast, effective and eco-friendly as well as quick purification method along with high product yields are some of the advantages of the present chemical reaction.</description><subject>Aldehydes</subject><subject>Analytical Chemistry</subject><subject>Biochemistry</subject><subject>Catalysts</subject><subject>Catalytic activity</subject><subject>Chemical reactions</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Derivatives</subject><subject>Ethanol</subject><subject>Inorganic Chemistry</subject><subject>Irradiation</subject><subject>Malononitrile</subject><subject>Nanoparticles</subject><subject>Organic Chemistry</subject><subject>Original Paper</subject><subject>Physical Chemistry</subject><subject>Ultrasonic imaging</subject><subject>Ultrasound</subject><issn>1735-207X</issn><issn>1735-2428</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kctKBDEQRRtR8PkDrgKuW_Ponk4vRRwVFDcu3IVMUtFIm4yV9EB_mz9nZkYRNy5Cpah7T0Hdqjpl9JxR2l0kJjoha8r68joparFTHbBOtDVvuNz9-dPueb86TOmN0rajbXNQfd4gQCBLjDmaOBAXkaQp5FdIPpHoyMPLHPhjQ4IOcakxezNAIjpYkvJop7WkiD0SbbJf-TwRvR4TcM4bDyETo7MeppQ37KL9yzevGN8hwAa5nLBYLaBf6UIri8ZQOjIOGXWKpSEeUVtfpjEcV3tODwlOvutR9TS_frq6re8fb-6uLu9rI9pZrrm0ve4569tWarDWsgVjznJjZE-tkZxTOZNNI3vrQC-aBcyglT0wB7yVTBxVZ1tsOdLHCCmrtzhiKBsVF43gHWWSFxXfqgzGlBCcWqJ_1zgpRtU6I7XNSJWM1CYjJYpJbE2piMML4C_6H9cXyi-Z8w</recordid><startdate>20200201</startdate><enddate>20200201</enddate><creator>Eshtehardian, Bahar</creator><creator>Rouhani, Morteza</creator><creator>Mirjafary, Zohreh</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0002-6708-6131</orcidid></search><sort><creationdate>20200201</creationdate><title>Green protocol for synthesis of MgFe2O4 nanoparticles and study of their activity as an efficient catalyst for the synthesis of chromene and pyran derivatives under ultrasound irradiation</title><author>Eshtehardian, Bahar ; Rouhani, Morteza ; Mirjafary, Zohreh</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c356t-28d9a9219558aeddd1b11fd2cc890dc82208684489dfeab4be6e589e1fe25813</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Aldehydes</topic><topic>Analytical Chemistry</topic><topic>Biochemistry</topic><topic>Catalysts</topic><topic>Catalytic activity</topic><topic>Chemical reactions</topic><topic>Chemical synthesis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Derivatives</topic><topic>Ethanol</topic><topic>Inorganic Chemistry</topic><topic>Irradiation</topic><topic>Malononitrile</topic><topic>Nanoparticles</topic><topic>Organic Chemistry</topic><topic>Original Paper</topic><topic>Physical Chemistry</topic><topic>Ultrasonic imaging</topic><topic>Ultrasound</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Eshtehardian, Bahar</creatorcontrib><creatorcontrib>Rouhani, Morteza</creatorcontrib><creatorcontrib>Mirjafary, Zohreh</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of the Iranian Chemical Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Eshtehardian, Bahar</au><au>Rouhani, Morteza</au><au>Mirjafary, Zohreh</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Green protocol for synthesis of MgFe2O4 nanoparticles and study of their activity as an efficient catalyst for the synthesis of chromene and pyran derivatives under ultrasound irradiation</atitle><jtitle>Journal of the Iranian Chemical Society</jtitle><stitle>J IRAN CHEM SOC</stitle><date>2020-02-01</date><risdate>2020</risdate><volume>17</volume><issue>2</issue><spage>469</spage><epage>481</epage><pages>469-481</pages><issn>1735-207X</issn><eissn>1735-2428</eissn><abstract>In this study, the MgFe
2
O
4
nanoparticles were synthesized via a green and simple approach. Then an effective procedure to synthesize 2-amino-7-hydroxy-4
H
-chromene and tetrahydrobenzo[
b
]pyran derivatives was established through the chemical reaction between different aldehydes, malononitrile and resorcinol (or dimedone) in the presence of MgFe
2
O
4
nanoparticles as a beneficial catalyst in ethanol as solvent under ultrasound irradiation. Moreover, the synthesized MgFe
2
O
4
nanoparticles were easily recovered by an external magnet and reused for four times without significant loss of their catalytic activity. Simple, fast, effective and eco-friendly as well as quick purification method along with high product yields are some of the advantages of the present chemical reaction.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s13738-019-01783-3</doi><tpages>13</tpages><orcidid>https://orcid.org/0000-0002-6708-6131</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1735-207X |
| ispartof | Journal of the Iranian Chemical Society, 2020-02, Vol.17 (2), p.469-481 |
| issn | 1735-207X 1735-2428 |
| language | eng |
| recordid | cdi_proquest_journals_2343270182 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Aldehydes Analytical Chemistry Biochemistry Catalysts Catalytic activity Chemical reactions Chemical synthesis Chemistry Chemistry and Materials Science Derivatives Ethanol Inorganic Chemistry Irradiation Malononitrile Nanoparticles Organic Chemistry Original Paper Physical Chemistry Ultrasonic imaging Ultrasound |
| title | Green protocol for synthesis of MgFe2O4 nanoparticles and study of their activity as an efficient catalyst for the synthesis of chromene and pyran derivatives under ultrasound irradiation |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-07T09%3A32%3A10IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Green%20protocol%20for%20synthesis%20of%20MgFe2O4%20nanoparticles%20and%20study%20of%20their%20activity%20as%20an%20efficient%20catalyst%20for%20the%20synthesis%20of%20chromene%20and%20pyran%20derivatives%20under%20ultrasound%20irradiation&rft.jtitle=Journal%20of%20the%20Iranian%20Chemical%20Society&rft.au=Eshtehardian,%20Bahar&rft.date=2020-02-01&rft.volume=17&rft.issue=2&rft.spage=469&rft.epage=481&rft.pages=469-481&rft.issn=1735-207X&rft.eissn=1735-2428&rft_id=info:doi/10.1007/s13738-019-01783-3&rft_dat=%3Cproquest_cross%3E2343270182%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2343270182&rft_id=info:pmid/&rfr_iscdi=true |