Preparation and characterization of nano‐Co‐[4‐chlorophenyl‐salicylaldimine‐methyl pyranopyrazole]Cl2 as a new Schiff base complex and catalyst for the solvent‐free synthesis of 1‐amidoalkyl‐2‐naphthols
By the reaction of 4‐chlorobenzaldehyde with ethyl acetoacetate, malononitrile, and hydrazine hydrate, 6‐amino‐4‐(4‐chlorophenyl)‐3‐methyl‐2,4‐dihydropyrano[2,3‐c]pyrazole‐5‐carbonitrile was prepared and then reacted with salicylaldehyde and CoCl2·6H2O to produce nano‐Co‐[4‐cholorophenyl‐salicylaldi...
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| Veröffentlicht in: | Applied organometallic chemistry 2020-01, Vol.34 (1), p.n/a |
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| creator | Moosavi‐Zare, Ahmad Reza Goudarziafshar, Hamid Nooraei, Fatemeh |
| description | By the reaction of 4‐chlorobenzaldehyde with ethyl acetoacetate, malononitrile, and hydrazine hydrate, 6‐amino‐4‐(4‐chlorophenyl)‐3‐methyl‐2,4‐dihydropyrano[2,3‐c]pyrazole‐5‐carbonitrile was prepared and then reacted with salicylaldehyde and CoCl2·6H2O to produce nano‐Co‐[4‐cholorophenyl‐salicylaldimine‐methylpyranopyrazole]Cl2 (nano‐[Co‐4CSMP]Cl2). The prepared nano‐Schiff base complex was reported for the first time and fully characterized by Fourier transform‐infrared spectroscopy, thermal gravimetric analysis, differential thermal gravimetric analysis, scanning electron microscopy, energy‐dispersive X‐ray spectroscopy, transmission electron microscopy, and Brunner–Emmett–Teller analyses and applied as an efficient catalyst for the synthesis of some 1‐amidoalkyl‐2‐naphthol derivatives.
Nano‐Co‐[4‐cholorophenyl‐salicylaldiminemethylpyranopyrazole] Cl2(nano‐[Co‐4CSMP]Cl2) was prepared and identified as a nano‐Schiffbase complex and applied as an efficient catalyst for the synthesis of some 1‐amido alkyl 2‐ naphthol derivatives. |
| doi_str_mv | 10.1002/aoc.5252 |
| format | Article |
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Nano‐Co‐[4‐cholorophenyl‐salicylaldiminemethylpyranopyrazole] Cl2(nano‐[Co‐4CSMP]Cl2) was prepared and identified as a nano‐Schiffbase complex and applied as an efficient catalyst for the synthesis of some 1‐amido alkyl 2‐ naphthol derivatives.</description><identifier>ISSN: 0268-2605</identifier><identifier>EISSN: 1099-0739</identifier><identifier>DOI: 10.1002/aoc.5252</identifier><language>eng</language><publisher>Chichester: Wiley Subscription Services, Inc</publisher><subject>1‐amidoalkyl‐2‐naphthol ; Catalysts ; Chemical synthesis ; Chemistry ; Differential thermal analysis ; Electron microscopy ; Fourier transforms ; Gravimetric analysis ; Hydrazines ; Imines ; Infrared analysis ; Malononitrile ; Microscopy ; nano‐[co‐4CSMP]Cl2 ; Naphthol ; pyranopyrazole ; Pyrazole ; Schiff base ; Spectrum analysis</subject><ispartof>Applied organometallic chemistry, 2020-01, Vol.34 (1), p.n/a</ispartof><rights>2019 John Wiley & Sons, Ltd.</rights><rights>2020 John Wiley & Sons, Ltd.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><orcidid>0000-0002-5930-6253 ; 0000-0003-0321-9326</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Faoc.5252$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Faoc.5252$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,777,781,1412,27905,27906,45555,45556</link.rule.ids></links><search><creatorcontrib>Moosavi‐Zare, Ahmad Reza</creatorcontrib><creatorcontrib>Goudarziafshar, Hamid</creatorcontrib><creatorcontrib>Nooraei, Fatemeh</creatorcontrib><title>Preparation and characterization of nano‐Co‐[4‐chlorophenyl‐salicylaldimine‐methyl pyranopyrazole]Cl2 as a new Schiff base complex and catalyst for the solvent‐free synthesis of 1‐amidoalkyl‐2‐naphthols</title><title>Applied organometallic chemistry</title><description>By the reaction of 4‐chlorobenzaldehyde with ethyl acetoacetate, malononitrile, and hydrazine hydrate, 6‐amino‐4‐(4‐chlorophenyl)‐3‐methyl‐2,4‐dihydropyrano[2,3‐c]pyrazole‐5‐carbonitrile was prepared and then reacted with salicylaldehyde and CoCl2·6H2O to produce nano‐Co‐[4‐cholorophenyl‐salicylaldimine‐methylpyranopyrazole]Cl2 (nano‐[Co‐4CSMP]Cl2). The prepared nano‐Schiff base complex was reported for the first time and fully characterized by Fourier transform‐infrared spectroscopy, thermal gravimetric analysis, differential thermal gravimetric analysis, scanning electron microscopy, energy‐dispersive X‐ray spectroscopy, transmission electron microscopy, and Brunner–Emmett–Teller analyses and applied as an efficient catalyst for the synthesis of some 1‐amidoalkyl‐2‐naphthol derivatives.
Nano‐Co‐[4‐cholorophenyl‐salicylaldiminemethylpyranopyrazole] Cl2(nano‐[Co‐4CSMP]Cl2) was prepared and identified as a nano‐Schiffbase complex and applied as an efficient catalyst for the synthesis of some 1‐amido alkyl 2‐ naphthol derivatives.</description><subject>1‐amidoalkyl‐2‐naphthol</subject><subject>Catalysts</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Differential thermal analysis</subject><subject>Electron microscopy</subject><subject>Fourier transforms</subject><subject>Gravimetric analysis</subject><subject>Hydrazines</subject><subject>Imines</subject><subject>Infrared analysis</subject><subject>Malononitrile</subject><subject>Microscopy</subject><subject>nano‐[co‐4CSMP]Cl2</subject><subject>Naphthol</subject><subject>pyranopyrazole</subject><subject>Pyrazole</subject><subject>Schiff base</subject><subject>Spectrum analysis</subject><issn>0268-2605</issn><issn>1099-0739</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNotUc1O3jAQtKoi9StU6iNY4hxw7DiJjyiiPxISlaAnhKKNYzemjh1sAw0nHqEP2FOfpA5fDzurGe2uRx6EPpbkpCSEnoKXJ5xy-gbtSiJEQRom3qIdoXVb0Jrwd-h9jHeEEFGX1Q79-RbUAgGS8Q6DG7GcMpNJBfO8F73GDpz_-_K72-CmyiAn64NfJuVWm2kEa-RqwY5mNk5lZVZpWi1e1pBXN3z2Vt12lmKIGLBTT_hKTkZrPEBUWPp5serX3gAksGtMWPuA06Rw9PZRuZSv6qAyXV1Wo4mbszKrMJvRg_35aoXmcrBMafI2HqEDDTaqD__7Ifr-6fy6-1JcXH7-2p1dFD8ob2kh26oZJNP5ixjVom40pe04VK2UnDAxNLSqAaoRgA-CE8XHUQoJrG7IALJp2CE63t9dgr9_UDH1d_4huPxkTxnjnAvG6zxV7KeejFVrvwQzQ1j7kvRbcH0Ort-C688uu62zf7cEnGA</recordid><startdate>202001</startdate><enddate>202001</enddate><creator>Moosavi‐Zare, Ahmad Reza</creator><creator>Goudarziafshar, Hamid</creator><creator>Nooraei, Fatemeh</creator><general>Wiley Subscription Services, Inc</general><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0002-5930-6253</orcidid><orcidid>https://orcid.org/0000-0003-0321-9326</orcidid></search><sort><creationdate>202001</creationdate><title>Preparation and characterization of nano‐Co‐[4‐chlorophenyl‐salicylaldimine‐methyl pyranopyrazole]Cl2 as a new Schiff base complex and catalyst for the solvent‐free synthesis of 1‐amidoalkyl‐2‐naphthols</title><author>Moosavi‐Zare, Ahmad Reza ; Goudarziafshar, Hamid ; Nooraei, Fatemeh</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g2582-c847bc3f26832f967f228db48cc5039b7246aa4daa5b950e5ddc9ca3670bac773</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>1‐amidoalkyl‐2‐naphthol</topic><topic>Catalysts</topic><topic>Chemical synthesis</topic><topic>Chemistry</topic><topic>Differential thermal analysis</topic><topic>Electron microscopy</topic><topic>Fourier transforms</topic><topic>Gravimetric analysis</topic><topic>Hydrazines</topic><topic>Imines</topic><topic>Infrared analysis</topic><topic>Malononitrile</topic><topic>Microscopy</topic><topic>nano‐[co‐4CSMP]Cl2</topic><topic>Naphthol</topic><topic>pyranopyrazole</topic><topic>Pyrazole</topic><topic>Schiff base</topic><topic>Spectrum analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Moosavi‐Zare, Ahmad Reza</creatorcontrib><creatorcontrib>Goudarziafshar, Hamid</creatorcontrib><creatorcontrib>Nooraei, Fatemeh</creatorcontrib><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Applied organometallic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Moosavi‐Zare, Ahmad Reza</au><au>Goudarziafshar, Hamid</au><au>Nooraei, Fatemeh</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and characterization of nano‐Co‐[4‐chlorophenyl‐salicylaldimine‐methyl pyranopyrazole]Cl2 as a new Schiff base complex and catalyst for the solvent‐free synthesis of 1‐amidoalkyl‐2‐naphthols</atitle><jtitle>Applied organometallic chemistry</jtitle><date>2020-01</date><risdate>2020</risdate><volume>34</volume><issue>1</issue><epage>n/a</epage><issn>0268-2605</issn><eissn>1099-0739</eissn><abstract>By the reaction of 4‐chlorobenzaldehyde with ethyl acetoacetate, malononitrile, and hydrazine hydrate, 6‐amino‐4‐(4‐chlorophenyl)‐3‐methyl‐2,4‐dihydropyrano[2,3‐c]pyrazole‐5‐carbonitrile was prepared and then reacted with salicylaldehyde and CoCl2·6H2O to produce nano‐Co‐[4‐cholorophenyl‐salicylaldimine‐methylpyranopyrazole]Cl2 (nano‐[Co‐4CSMP]Cl2). The prepared nano‐Schiff base complex was reported for the first time and fully characterized by Fourier transform‐infrared spectroscopy, thermal gravimetric analysis, differential thermal gravimetric analysis, scanning electron microscopy, energy‐dispersive X‐ray spectroscopy, transmission electron microscopy, and Brunner–Emmett–Teller analyses and applied as an efficient catalyst for the synthesis of some 1‐amidoalkyl‐2‐naphthol derivatives.
Nano‐Co‐[4‐cholorophenyl‐salicylaldiminemethylpyranopyrazole] Cl2(nano‐[Co‐4CSMP]Cl2) was prepared and identified as a nano‐Schiffbase complex and applied as an efficient catalyst for the synthesis of some 1‐amido alkyl 2‐ naphthol derivatives.</abstract><cop>Chichester</cop><pub>Wiley Subscription Services, Inc</pub><doi>10.1002/aoc.5252</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-5930-6253</orcidid><orcidid>https://orcid.org/0000-0003-0321-9326</orcidid></addata></record> |
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| subjects | 1‐amidoalkyl‐2‐naphthol Catalysts Chemical synthesis Chemistry Differential thermal analysis Electron microscopy Fourier transforms Gravimetric analysis Hydrazines Imines Infrared analysis Malononitrile Microscopy nano‐[co‐4CSMP]Cl2 Naphthol pyranopyrazole Pyrazole Schiff base Spectrum analysis |
| title | Preparation and characterization of nano‐Co‐[4‐chlorophenyl‐salicylaldimine‐methyl pyranopyrazole]Cl2 as a new Schiff base complex and catalyst for the solvent‐free synthesis of 1‐amidoalkyl‐2‐naphthols |
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