Synthesis, characterization and hydration analysis of Ba2+-, Cu2+- or Bi3+-doped CaO–Al2O3–ZrO2-based cements
This paper deals with the design, synthesis, hydration mechanism and hydration products of novel Ba 2+ -, Cu 2+ - or Bi 3+ -doped CaO–Al 2 O 3 –ZrO 2 -based cementitious materials used for heavyweight concrete mixes. The results of the heating microscopy thermal analysis indicated that both Cu and B...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2019, Vol.138 (6), p.4331-4340 |
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| container_title | Journal of thermal analysis and calorimetry |
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| creator | Madej, Dominika Boris, Renata |
| description | This paper deals with the design, synthesis, hydration mechanism and hydration products of novel Ba
2+
-, Cu
2+
- or Bi
3+
-doped CaO–Al
2
O
3
–ZrO
2
-based cementitious materials used for heavyweight concrete mixes. The results of the heating microscopy thermal analysis indicated that both Cu and Bi in a Ca
7
ZrAl
6
O
18
-based cement clinker can effectively reduce the sintering temperature by 150–200 °C. Incorporation of barium for the synthesis of calcium zirconium aluminate-based hydraulic binder increased its thermal resistance since Ba
2+
-doped Ca
7
ZrAl
6
O
18
along with accessory (Ca,Ba)ZrO
3
with a perovskite‐type structure and BaAl
2
O
4
phases having high melting points were formed. The presence of metal ions, i.e., Cu
2+
or Bi
3+
, created conditions which were favorable for the formation of hexagonal calcium aluminate hydrates rather than the cubic one, as confirmed by coupled DSC–TG/EGA–MS thermal analysis techniques and X-ray diffraction. For the Ba
2+
doping ions, this effect was the least noticeable. The effect of metal ions including Ba
2+
, Cu
2+
and Bi
3+
on microstructural features of cement pastes was investigated by SEM–EDS. These doping ions strongly affected the morphologies of Ca–Al hydrates. |
| doi_str_mv | 10.1007/s10973-019-08142-7 |
| format | Article |
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2+
-, Cu
2+
- or Bi
3+
-doped CaO–Al
2
O
3
–ZrO
2
-based cementitious materials used for heavyweight concrete mixes. The results of the heating microscopy thermal analysis indicated that both Cu and Bi in a Ca
7
ZrAl
6
O
18
-based cement clinker can effectively reduce the sintering temperature by 150–200 °C. Incorporation of barium for the synthesis of calcium zirconium aluminate-based hydraulic binder increased its thermal resistance since Ba
2+
-doped Ca
7
ZrAl
6
O
18
along with accessory (Ca,Ba)ZrO
3
with a perovskite‐type structure and BaAl
2
O
4
phases having high melting points were formed. The presence of metal ions, i.e., Cu
2+
or Bi
3+
, created conditions which were favorable for the formation of hexagonal calcium aluminate hydrates rather than the cubic one, as confirmed by coupled DSC–TG/EGA–MS thermal analysis techniques and X-ray diffraction. For the Ba
2+
doping ions, this effect was the least noticeable. The effect of metal ions including Ba
2+
, Cu
2+
and Bi
3+
on microstructural features of cement pastes was investigated by SEM–EDS. These doping ions strongly affected the morphologies of Ca–Al hydrates.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>DOI: 10.1007/s10973-019-08142-7</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Aluminum oxide ; Analytical Chemistry ; Barium ; Bismuth ; Calcium aluminate ; Calcium oxide ; Calcium zirconate ; Cement paste ; Cements ; Chemistry ; Chemistry and Materials Science ; Clinker ; Copper ; Doping ; Hydrates ; Hydration ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Melting points ; Metal ions ; Morphology ; Perovskites ; Physical Chemistry ; Polymer Sciences ; Synthesis ; Thermal analysis ; Thermal resistance ; Zirconium dioxide</subject><ispartof>Journal of thermal analysis and calorimetry, 2019, Vol.138 (6), p.4331-4340</ispartof><rights>The Author(s) 2019</rights><rights>Copyright Springer Nature B.V. 2019</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c330t-b6dc8fefdf3eb76344602d365c91344ef7c5ab8a9ef3aebad20194ed1966b1d03</citedby><cites>FETCH-LOGICAL-c330t-b6dc8fefdf3eb76344602d365c91344ef7c5ab8a9ef3aebad20194ed1966b1d03</cites><orcidid>0000-0002-5418-1973</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10973-019-08142-7$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10973-019-08142-7$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Madej, Dominika</creatorcontrib><creatorcontrib>Boris, Renata</creatorcontrib><title>Synthesis, characterization and hydration analysis of Ba2+-, Cu2+- or Bi3+-doped CaO–Al2O3–ZrO2-based cements</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>This paper deals with the design, synthesis, hydration mechanism and hydration products of novel Ba
2+
-, Cu
2+
- or Bi
3+
-doped CaO–Al
2
O
3
–ZrO
2
-based cementitious materials used for heavyweight concrete mixes. The results of the heating microscopy thermal analysis indicated that both Cu and Bi in a Ca
7
ZrAl
6
O
18
-based cement clinker can effectively reduce the sintering temperature by 150–200 °C. Incorporation of barium for the synthesis of calcium zirconium aluminate-based hydraulic binder increased its thermal resistance since Ba
2+
-doped Ca
7
ZrAl
6
O
18
along with accessory (Ca,Ba)ZrO
3
with a perovskite‐type structure and BaAl
2
O
4
phases having high melting points were formed. The presence of metal ions, i.e., Cu
2+
or Bi
3+
, created conditions which were favorable for the formation of hexagonal calcium aluminate hydrates rather than the cubic one, as confirmed by coupled DSC–TG/EGA–MS thermal analysis techniques and X-ray diffraction. For the Ba
2+
doping ions, this effect was the least noticeable. The effect of metal ions including Ba
2+
, Cu
2+
and Bi
3+
on microstructural features of cement pastes was investigated by SEM–EDS. These doping ions strongly affected the morphologies of Ca–Al hydrates.</description><subject>Aluminum oxide</subject><subject>Analytical Chemistry</subject><subject>Barium</subject><subject>Bismuth</subject><subject>Calcium aluminate</subject><subject>Calcium oxide</subject><subject>Calcium zirconate</subject><subject>Cement paste</subject><subject>Cements</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Clinker</subject><subject>Copper</subject><subject>Doping</subject><subject>Hydrates</subject><subject>Hydration</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Melting points</subject><subject>Metal ions</subject><subject>Morphology</subject><subject>Perovskites</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Synthesis</subject><subject>Thermal analysis</subject><subject>Thermal resistance</subject><subject>Zirconium dioxide</subject><issn>1388-6150</issn><issn>1588-2926</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><recordid>eNp9UL1OwzAYtBBIlMILMFlibA3-SZx4bCP-pEoZgIXFcvxDU7VJa6dDmHgH3pAnwRAQG9Pdp-_upDsAzgm-JBhnV4FgkTGEiUA4JwlF2QEYkTTPERWUH0bOIuckxcfgJIQVxlgITEZg99A33dKGOkyhXiqvdGd9_aq6um2gagxc9sb_XmrdRyFsHZwrOkFTWOwjwNbDec0myLRba2Chyo-399malizisy8pqlSID203tunCKThyah3s2Q-OwdPN9WNxhxbl7X0xWyDNGO5QxY3OnXXGMVtlnCUJx9QwnmpB4mFdplNV5UpYx5StlKGxfGINEZxXxGA2BhdD7ta3u70NnVy1ex87BEkZEVmaC06jig4q7dsQvHVy6-uN8r0kWH5NK4dpZUyX39PKLJrYYApR3LxY_xf9j-sTXzR8xg</recordid><startdate>2019</startdate><enddate>2019</enddate><creator>Madej, Dominika</creator><creator>Boris, Renata</creator><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>C6C</scope><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0002-5418-1973</orcidid></search><sort><creationdate>2019</creationdate><title>Synthesis, characterization and hydration analysis of Ba2+-, Cu2+- or Bi3+-doped CaO–Al2O3–ZrO2-based cements</title><author>Madej, Dominika ; Boris, Renata</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c330t-b6dc8fefdf3eb76344602d365c91344ef7c5ab8a9ef3aebad20194ed1966b1d03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Aluminum oxide</topic><topic>Analytical Chemistry</topic><topic>Barium</topic><topic>Bismuth</topic><topic>Calcium aluminate</topic><topic>Calcium oxide</topic><topic>Calcium zirconate</topic><topic>Cement paste</topic><topic>Cements</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Clinker</topic><topic>Copper</topic><topic>Doping</topic><topic>Hydrates</topic><topic>Hydration</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Melting points</topic><topic>Metal ions</topic><topic>Morphology</topic><topic>Perovskites</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Synthesis</topic><topic>Thermal analysis</topic><topic>Thermal resistance</topic><topic>Zirconium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Madej, Dominika</creatorcontrib><creatorcontrib>Boris, Renata</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>CrossRef</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Madej, Dominika</au><au>Boris, Renata</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis, characterization and hydration analysis of Ba2+-, Cu2+- or Bi3+-doped CaO–Al2O3–ZrO2-based cements</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2019</date><risdate>2019</risdate><volume>138</volume><issue>6</issue><spage>4331</spage><epage>4340</epage><pages>4331-4340</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><abstract>This paper deals with the design, synthesis, hydration mechanism and hydration products of novel Ba
2+
-, Cu
2+
- or Bi
3+
-doped CaO–Al
2
O
3
–ZrO
2
-based cementitious materials used for heavyweight concrete mixes. The results of the heating microscopy thermal analysis indicated that both Cu and Bi in a Ca
7
ZrAl
6
O
18
-based cement clinker can effectively reduce the sintering temperature by 150–200 °C. Incorporation of barium for the synthesis of calcium zirconium aluminate-based hydraulic binder increased its thermal resistance since Ba
2+
-doped Ca
7
ZrAl
6
O
18
along with accessory (Ca,Ba)ZrO
3
with a perovskite‐type structure and BaAl
2
O
4
phases having high melting points were formed. The presence of metal ions, i.e., Cu
2+
or Bi
3+
, created conditions which were favorable for the formation of hexagonal calcium aluminate hydrates rather than the cubic one, as confirmed by coupled DSC–TG/EGA–MS thermal analysis techniques and X-ray diffraction. For the Ba
2+
doping ions, this effect was the least noticeable. The effect of metal ions including Ba
2+
, Cu
2+
and Bi
3+
on microstructural features of cement pastes was investigated by SEM–EDS. These doping ions strongly affected the morphologies of Ca–Al hydrates.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s10973-019-08142-7</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-5418-1973</orcidid><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1388-6150 |
| ispartof | Journal of thermal analysis and calorimetry, 2019, Vol.138 (6), p.4331-4340 |
| issn | 1388-6150 1588-2926 |
| language | eng |
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| source | SpringerLink Journals - AutoHoldings |
| subjects | Aluminum oxide Analytical Chemistry Barium Bismuth Calcium aluminate Calcium oxide Calcium zirconate Cement paste Cements Chemistry Chemistry and Materials Science Clinker Copper Doping Hydrates Hydration Inorganic Chemistry Measurement Science and Instrumentation Melting points Metal ions Morphology Perovskites Physical Chemistry Polymer Sciences Synthesis Thermal analysis Thermal resistance Zirconium dioxide |
| title | Synthesis, characterization and hydration analysis of Ba2+-, Cu2+- or Bi3+-doped CaO–Al2O3–ZrO2-based cements |
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