Study on morphology of LaFeO3 nanofibers under different voltage connections

Continuous LaFeO3 nanowires and nanobelts were successfully synthesized using a sol–gel assisted electrospinning method followed by calcination at 500°C in air. The thermal decomposition processes of LaFeO3 are carefully investigated and the best calcining temperature was found to be 500°C. The two...

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Veröffentlicht in:Journal of the Chinese Chemical Society (Taipei) 2019-11, Vol.66 (11), p.1469-1473
Hauptverfasser: Guo, Meiling, Li, Shudan, Wang, Xiuhua, Gao, Kun
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container_issue 11
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creator Guo, Meiling
Li, Shudan
Wang, Xiuhua
Gao, Kun
description Continuous LaFeO3 nanowires and nanobelts were successfully synthesized using a sol–gel assisted electrospinning method followed by calcination at 500°C in air. The thermal decomposition processes of LaFeO3 are carefully investigated and the best calcining temperature was found to be 500°C. The two nanofibers obtained were characterized using X‐ray diffraction analysis, which shows single phase and the structure of nanobelts has higher crystallinity than that of the nanowires. The scanning electron microscopy reveals that the diameter of the obtained LaFeO3 nanowires is 139.3 nm. And the thickness and width of the nanobelts are 80 and 459 nm. Moreover, the electrospun LaFeO3 nanobelts are endowed with a higher specific surface area compared with the nanowires, which results from the regular one dimensional morphology without any detectable agglomeration and a rough surface. Continuous LaFeO3 nanowires and porous nanobelts were successfully synthesized using a sol–gel assisted electrospinning method. The structure and morphology of the prepared nanofibers were characterized using thermal gravity analysis‐differential thermal gravity (TG‐DTG), X‐ray diffraction (XRD), and scanning electron microscope (SEM). Possible mechanisms leading to the formation of different morphologies were also discussed.
doi_str_mv 10.1002/jccs.201900012
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The thermal decomposition processes of LaFeO3 are carefully investigated and the best calcining temperature was found to be 500°C. The two nanofibers obtained were characterized using X‐ray diffraction analysis, which shows single phase and the structure of nanobelts has higher crystallinity than that of the nanowires. The scanning electron microscopy reveals that the diameter of the obtained LaFeO3 nanowires is 139.3 nm. And the thickness and width of the nanobelts are 80 and 459 nm. Moreover, the electrospun LaFeO3 nanobelts are endowed with a higher specific surface area compared with the nanowires, which results from the regular one dimensional morphology without any detectable agglomeration and a rough surface. Continuous LaFeO3 nanowires and porous nanobelts were successfully synthesized using a sol–gel assisted electrospinning method. 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source Wiley Online Library Journals Frontfile Complete
subjects Diameters
Ferrites
LaFeO3
Lanthanum compounds
Morphology
nanobelts
Nanofibers
Nanowires
one‐dimensional
Roasting
Sol-gel processes
Thermal decomposition
title Study on morphology of LaFeO3 nanofibers under different voltage connections
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