High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination
Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three ort...
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Veröffentlicht in: | Geostandards and geoanalytical research 2019-12, Vol.43 (4), p.585-593 |
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creator | Tang, Guo‐Qiang Su, Ben‐Xun Li, Qiu‐Li Xia, Xiao‐Ping Jing, Jie‐Jun Feng, Lian‐Jun Martin, Laure Yang, Qing Li, Xian‐Hua |
description | Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three orthopyroxenes) in nineteen sessions using CAMECA IMS 1280 SIMS instruments to evaluate their potential as SIMS reference materials. The obtained results reveal oxygen isotope homogeneity of these samples. No matrix effect was measured for the same variety of mineral samples with limited Mg‐number variations (89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively). The recommended oxygen isotope compositions of these samples were determined using laser fluorination. These samples are therefore suitable to be used as reference materials for in situ oxygen isotope microanalysis.
Key Points
We suggest five olivine, three clinopyroxene and three orthopyroxene SIMS reference materials for oxygen isotope analysis.
Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively.
The recommended oxygen isotope compositions were determined using the laser fluorination method. |
doi_str_mv | 10.1111/ggr.12288 |
format | Article |
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Key Points
We suggest five olivine, three clinopyroxene and three orthopyroxene SIMS reference materials for oxygen isotope analysis.
Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively.
The recommended oxygen isotope compositions were determined using the laser fluorination method.</description><identifier>ISSN: 1639-4488</identifier><identifier>EISSN: 1751-908X</identifier><identifier>DOI: 10.1111/ggr.12288</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc</publisher><subject>Fractionation ; Homogeneity ; IMF ; Instruments ; Isotopes ; Lasers ; Magma ; mantle minerals ; Mass spectrometry ; Mass spectroscopy ; Mineral samples ; Olivine ; Oxygen isotopes ; reference material ; Reference materials ; SIMS</subject><ispartof>Geostandards and geoanalytical research, 2019-12, Vol.43 (4), p.585-593</ispartof><rights>2019 The Authors. Geostandards and Geoanalytical Research © 2019 International Association of Geoanalysts</rights><rights>Geostandards and Geoanalytical Research © 2019 International Association of Geoanalysts</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a3868-f28d0a1772383307b82b2a44b72dfea744980298cec5fe1102bbf2cdb7ee61693</citedby><cites>FETCH-LOGICAL-a3868-f28d0a1772383307b82b2a44b72dfea744980298cec5fe1102bbf2cdb7ee61693</cites><orcidid>0000-0001-7754-9390 ; 0000-0002-7280-5508 ; 0000-0002-0714-4651 ; 0000-0002-3203-039X ; 0000-0002-0325-3789 ; 0000-0001-5512-7736</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Fggr.12288$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Fggr.12288$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids></links><search><creatorcontrib>Tang, Guo‐Qiang</creatorcontrib><creatorcontrib>Su, Ben‐Xun</creatorcontrib><creatorcontrib>Li, Qiu‐Li</creatorcontrib><creatorcontrib>Xia, Xiao‐Ping</creatorcontrib><creatorcontrib>Jing, Jie‐Jun</creatorcontrib><creatorcontrib>Feng, Lian‐Jun</creatorcontrib><creatorcontrib>Martin, Laure</creatorcontrib><creatorcontrib>Yang, Qing</creatorcontrib><creatorcontrib>Li, Xian‐Hua</creatorcontrib><title>High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination</title><title>Geostandards and geoanalytical research</title><description>Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three orthopyroxenes) in nineteen sessions using CAMECA IMS 1280 SIMS instruments to evaluate their potential as SIMS reference materials. The obtained results reveal oxygen isotope homogeneity of these samples. No matrix effect was measured for the same variety of mineral samples with limited Mg‐number variations (89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively). The recommended oxygen isotope compositions of these samples were determined using laser fluorination. These samples are therefore suitable to be used as reference materials for in situ oxygen isotope microanalysis.
Key Points
We suggest five olivine, three clinopyroxene and three orthopyroxene SIMS reference materials for oxygen isotope analysis.
Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively.
The recommended oxygen isotope compositions were determined using the laser fluorination method.</description><subject>Fractionation</subject><subject>Homogeneity</subject><subject>IMF</subject><subject>Instruments</subject><subject>Isotopes</subject><subject>Lasers</subject><subject>Magma</subject><subject>mantle minerals</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Mineral samples</subject><subject>Olivine</subject><subject>Oxygen isotopes</subject><subject>reference material</subject><subject>Reference materials</subject><subject>SIMS</subject><issn>1639-4488</issn><issn>1751-908X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp10N1KwzAUB_AgCs7phW8Q2JVgtyT9SHopU7fBRmEqeFfS9rTL6JKadrre-Qg-o09itYJX5uaEw--cA3-ELikZ0-5NisKOKWNCHKEB5T51QiKej7t_4IaO5wlxis7qekuI74U-HaBqrorN5_vHqhjhqFSvSsM1npZKm6q15gAasNQZjmyz-eusIQcLOgW8kg1YJcsa58bihcYPqtnj6NAWoPGiNo2pAN9Ch3ZKy0YZfY5O8s7DxW8doqf7u8fp3FlGs8X0ZulIVwTCyZnIiKScM1e4LuGJYAmTnpdwluUgueeFgrBQpJD6OVBKWJLkLM0SDhDQIHSHaNTvrax52UPdxFuzt7o7GTOX-gEPKaeduupVak1dW8jjyqqdtG1MSfwdaNwFGv8E2tlJb99UCe3_MJ7N1v3EF0A6eTE</recordid><startdate>201912</startdate><enddate>201912</enddate><creator>Tang, Guo‐Qiang</creator><creator>Su, Ben‐Xun</creator><creator>Li, Qiu‐Li</creator><creator>Xia, Xiao‐Ping</creator><creator>Jing, Jie‐Jun</creator><creator>Feng, Lian‐Jun</creator><creator>Martin, Laure</creator><creator>Yang, Qing</creator><creator>Li, Xian‐Hua</creator><general>Wiley Subscription Services, Inc</general><scope>AAYXX</scope><scope>CITATION</scope><scope>F1W</scope><scope>H96</scope><scope>L.G</scope><orcidid>https://orcid.org/0000-0001-7754-9390</orcidid><orcidid>https://orcid.org/0000-0002-7280-5508</orcidid><orcidid>https://orcid.org/0000-0002-0714-4651</orcidid><orcidid>https://orcid.org/0000-0002-3203-039X</orcidid><orcidid>https://orcid.org/0000-0002-0325-3789</orcidid><orcidid>https://orcid.org/0000-0001-5512-7736</orcidid></search><sort><creationdate>201912</creationdate><title>High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination</title><author>Tang, Guo‐Qiang ; Su, Ben‐Xun ; Li, Qiu‐Li ; Xia, Xiao‐Ping ; Jing, Jie‐Jun ; Feng, Lian‐Jun ; Martin, Laure ; Yang, Qing ; Li, Xian‐Hua</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a3868-f28d0a1772383307b82b2a44b72dfea744980298cec5fe1102bbf2cdb7ee61693</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Fractionation</topic><topic>Homogeneity</topic><topic>IMF</topic><topic>Instruments</topic><topic>Isotopes</topic><topic>Lasers</topic><topic>Magma</topic><topic>mantle minerals</topic><topic>Mass spectrometry</topic><topic>Mass spectroscopy</topic><topic>Mineral samples</topic><topic>Olivine</topic><topic>Oxygen isotopes</topic><topic>reference material</topic><topic>Reference materials</topic><topic>SIMS</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tang, Guo‐Qiang</creatorcontrib><creatorcontrib>Su, Ben‐Xun</creatorcontrib><creatorcontrib>Li, Qiu‐Li</creatorcontrib><creatorcontrib>Xia, Xiao‐Ping</creatorcontrib><creatorcontrib>Jing, Jie‐Jun</creatorcontrib><creatorcontrib>Feng, Lian‐Jun</creatorcontrib><creatorcontrib>Martin, Laure</creatorcontrib><creatorcontrib>Yang, Qing</creatorcontrib><creatorcontrib>Li, Xian‐Hua</creatorcontrib><collection>CrossRef</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 2: Ocean Technology, Policy & Non-Living Resources</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><jtitle>Geostandards and geoanalytical research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tang, Guo‐Qiang</au><au>Su, Ben‐Xun</au><au>Li, Qiu‐Li</au><au>Xia, Xiao‐Ping</au><au>Jing, Jie‐Jun</au><au>Feng, Lian‐Jun</au><au>Martin, Laure</au><au>Yang, Qing</au><au>Li, Xian‐Hua</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination</atitle><jtitle>Geostandards and geoanalytical research</jtitle><date>2019-12</date><risdate>2019</risdate><volume>43</volume><issue>4</issue><spage>585</spage><epage>593</epage><pages>585-593</pages><issn>1639-4488</issn><eissn>1751-908X</eissn><abstract>Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three orthopyroxenes) in nineteen sessions using CAMECA IMS 1280 SIMS instruments to evaluate their potential as SIMS reference materials. The obtained results reveal oxygen isotope homogeneity of these samples. No matrix effect was measured for the same variety of mineral samples with limited Mg‐number variations (89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively). The recommended oxygen isotope compositions of these samples were determined using laser fluorination. These samples are therefore suitable to be used as reference materials for in situ oxygen isotope microanalysis.
Key Points
We suggest five olivine, three clinopyroxene and three orthopyroxene SIMS reference materials for oxygen isotope analysis.
Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively.
The recommended oxygen isotope compositions were determined using the laser fluorination method.</abstract><cop>Hoboken</cop><pub>Wiley Subscription Services, Inc</pub><doi>10.1111/ggr.12288</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0001-7754-9390</orcidid><orcidid>https://orcid.org/0000-0002-7280-5508</orcidid><orcidid>https://orcid.org/0000-0002-0714-4651</orcidid><orcidid>https://orcid.org/0000-0002-3203-039X</orcidid><orcidid>https://orcid.org/0000-0002-0325-3789</orcidid><orcidid>https://orcid.org/0000-0001-5512-7736</orcidid></addata></record> |
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subjects | Fractionation Homogeneity IMF Instruments Isotopes Lasers Magma mantle minerals Mass spectrometry Mass spectroscopy Mineral samples Olivine Oxygen isotopes reference material Reference materials SIMS |
title | High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination |
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