High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination

Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three ort...

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Veröffentlicht in:Geostandards and geoanalytical research 2019-12, Vol.43 (4), p.585-593
Hauptverfasser: Tang, Guo‐Qiang, Su, Ben‐Xun, Li, Qiu‐Li, Xia, Xiao‐Ping, Jing, Jie‐Jun, Feng, Lian‐Jun, Martin, Laure, Yang, Qing, Li, Xian‐Hua
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container_issue 4
container_start_page 585
container_title Geostandards and geoanalytical research
container_volume 43
creator Tang, Guo‐Qiang
Su, Ben‐Xun
Li, Qiu‐Li
Xia, Xiao‐Ping
Jing, Jie‐Jun
Feng, Lian‐Jun
Martin, Laure
Yang, Qing
Li, Xian‐Hua
description Secondary ion mass spectrometry (SIMS) requires matrix‐matched reference materials to calibrate mass fractionation during oxygen isotope measurement. Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three orthopyroxenes) in nineteen sessions using CAMECA IMS 1280 SIMS instruments to evaluate their potential as SIMS reference materials. The obtained results reveal oxygen isotope homogeneity of these samples. No matrix effect was measured for the same variety of mineral samples with limited Mg‐number variations (89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively). The recommended oxygen isotope compositions of these samples were determined using laser fluorination. These samples are therefore suitable to be used as reference materials for in situ oxygen isotope microanalysis. Key Points We suggest five olivine, three clinopyroxene and three orthopyroxene SIMS reference materials for oxygen isotope analysis. Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively. The recommended oxygen isotope compositions were determined using the laser fluorination method.
doi_str_mv 10.1111/ggr.12288
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Over one thousand SIMS oxygen isotope measurements were conducted on eleven natural mineral samples (five olivines, three clinopyroxenes and three orthopyroxenes) in nineteen sessions using CAMECA IMS 1280 SIMS instruments to evaluate their potential as SIMS reference materials. The obtained results reveal oxygen isotope homogeneity of these samples. No matrix effect was measured for the same variety of mineral samples with limited Mg‐number variations (89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively). The recommended oxygen isotope compositions of these samples were determined using laser fluorination. These samples are therefore suitable to be used as reference materials for in situ oxygen isotope microanalysis. Key Points We suggest five olivine, three clinopyroxene and three orthopyroxene SIMS reference materials for oxygen isotope analysis. Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively. The recommended oxygen isotope compositions were determined using the laser fluorination method.</description><identifier>ISSN: 1639-4488</identifier><identifier>EISSN: 1751-908X</identifier><identifier>DOI: 10.1111/ggr.12288</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc</publisher><subject>Fractionation ; Homogeneity ; IMF ; Instruments ; Isotopes ; Lasers ; Magma ; mantle minerals ; Mass spectrometry ; Mass spectroscopy ; Mineral samples ; Olivine ; Oxygen isotopes ; reference material ; Reference materials ; SIMS</subject><ispartof>Geostandards and geoanalytical research, 2019-12, Vol.43 (4), p.585-593</ispartof><rights>2019 The Authors. 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Mg‐number variations are 89.6–94.2, 90–91.9 and 90.1–92.1 for olivine, clinopyroxene and orthopyroxene, respectively. 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subjects Fractionation
Homogeneity
IMF
Instruments
Isotopes
Lasers
Magma
mantle minerals
Mass spectrometry
Mass spectroscopy
Mineral samples
Olivine
Oxygen isotopes
reference material
Reference materials
SIMS
title High‐Mg# Olivine, Clinopyroxene and Orthopyroxene Reference Materials for In Situ Oxygen Isotope Determination
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