In Situ Monitoring of Nanoparticle Formation during Iridium‐Catalysed Oxygen Evolution by Real‐Time Small Angle X‐Ray Scattering

Real‐time Small Angle X‐Ray Scattering (SAXS) has been used to investigate the homogeneity of a series of molecular iridium complexes during water oxidation catalysis in aqueous NaIO4 solution through a continuous flow cell. The results obtained for the unstable [Cp*Ir(OH2)3]2+ precursor forming amo...

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Veröffentlicht in:	ChemCatChem 2019-11, Vol.11 (21), p.5313-5321
Hauptverfasser:	Singer Hobbs, Maya, Sackville, Emma V., Smith, Andrew J., Edler, Karen J., Hintermair, Ulrich
Format:	Artikel
Sprache:	eng
Schlagworte:	Catalysis Chemical evolution Continuous flow homogeneous vs. heterogeneous catalysis iridium Iridium compounds Nanoparticles Oxidation Photon correlation spectroscopy SAXS Sensitivity enhancement Small angle X ray scattering Temporal resolution water oxidation
Online-Zugang:	Volltext
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