The Assessment of Bone Deterioration with Nuclear Magnetic Resonance Spectroscopy in a Multidisciplinary Context: The Case of the UNESCO World Heritage Site of Sedlec, Czechia
Human remains from the skeletal collection of the UNESCO world heritage site of Sedlec (Czechia) have been investigated with 1H, 31P and 13C magic‐angle‐spinning nuclear magnetic resonance spectroscopy. The quantitative description of the component of the phosphorus signal attributed to the external...
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| Veröffentlicht in: | Archaeometry 2019-10, Vol.61 (5), p.1144-1159 |
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| container_title | Archaeometry |
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| creator | Viani, A. Mácová, P. Machová, D. Čendak, T. |
| description | Human remains from the skeletal collection of the UNESCO world heritage site of Sedlec (Czechia) have been investigated with 1H, 31P and 13C magic‐angle‐spinning nuclear magnetic resonance spectroscopy. The quantitative description of the component of the phosphorus signal attributed to the external amorphous hydrated layer of the mineral apatite particles is considered a sensitive index of the bone integrity, in general agreement with indicators of decay derived from other analytical techniques. Differences in proton and phosphorus resonances were related to deterioration effects, allowing for the identification of local conditions posing a threat to bone preservation. |
| doi_str_mv | 10.1111/arcm.12475 |
| format | Article |
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The quantitative description of the component of the phosphorus signal attributed to the external amorphous hydrated layer of the mineral apatite particles is considered a sensitive index of the bone integrity, in general agreement with indicators of decay derived from other analytical techniques. Differences in proton and phosphorus resonances were related to deterioration effects, allowing for the identification of local conditions posing a threat to bone preservation.</description><identifier>ISSN: 0003-813X</identifier><identifier>EISSN: 1475-4754</identifier><identifier>DOI: 10.1111/arcm.12475</identifier><language>eng</language><publisher>Oxford: Wiley Subscription Services, Inc</publisher><subject>archaeological bones ; bone diagenesis ; Deterioration ; NMR ; Nuclear magnetic resonance ; Phosphorus ; Resonance ; Spectroscopy ; Spectrum analysis ; taphonomy ; World Heritage Areas</subject><ispartof>Archaeometry, 2019-10, Vol.61 (5), p.1144-1159</ispartof><rights>2019 University of Oxford</rights><rights>University of Oxford</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a3245-18a9eec08c42e189b9bebdaf7fa1a2d7c38f7ef0c9ca0411e5423f9b450ad7683</citedby><cites>FETCH-LOGICAL-a3245-18a9eec08c42e189b9bebdaf7fa1a2d7c38f7ef0c9ca0411e5423f9b450ad7683</cites><orcidid>0000-0002-6019-1094 ; 0000-0002-0528-3930</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Farcm.12475$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Farcm.12475$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27923,27924,45573,45574</link.rule.ids></links><search><creatorcontrib>Viani, A.</creatorcontrib><creatorcontrib>Mácová, P.</creatorcontrib><creatorcontrib>Machová, D.</creatorcontrib><creatorcontrib>Čendak, T.</creatorcontrib><title>The Assessment of Bone Deterioration with Nuclear Magnetic Resonance Spectroscopy in a Multidisciplinary Context: The Case of the UNESCO World Heritage Site of Sedlec, Czechia</title><title>Archaeometry</title><description>Human remains from the skeletal collection of the UNESCO world heritage site of Sedlec (Czechia) have been investigated with 1H, 31P and 13C magic‐angle‐spinning nuclear magnetic resonance spectroscopy. The quantitative description of the component of the phosphorus signal attributed to the external amorphous hydrated layer of the mineral apatite particles is considered a sensitive index of the bone integrity, in general agreement with indicators of decay derived from other analytical techniques. Differences in proton and phosphorus resonances were related to deterioration effects, allowing for the identification of local conditions posing a threat to bone preservation.</description><subject>archaeological bones</subject><subject>bone diagenesis</subject><subject>Deterioration</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Phosphorus</subject><subject>Resonance</subject><subject>Spectroscopy</subject><subject>Spectrum analysis</subject><subject>taphonomy</subject><subject>World Heritage Areas</subject><issn>0003-813X</issn><issn>1475-4754</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp9kcFO4zAQhi20SHSBC08wEjdEWDtxm4RbCeyCREGiILhFU2dCjVI72K6gvBSvuC7lzEijmZG-mV-jn7EDwU9EjD_o1OJEpDIfbrGBiCWJKX-xAec8SwqRPe2w396_xHEkJR-wz_s5wdh78n5BJoBt4cwagnMK5LR1GLQ18KbDHG6WqiN0MMFnQ0EruCNvDRpFMO1JBWe9sv0KtAGEybILutFe6b7TBt0KKmsCvYdTWCtW6GmtFWL_cHMxrW7h0bqugcuoGvA5ntThi5hS05E6huqD1FzjHttusfO0_1132cPfi_vqMrm-_XdVja8TzFI5TESBJZHihZIpiaKclTOaNdjmLQpMm1xlRZtTy1WpkEshaCjTrC1ncsixyUdFtssON3d7Z1-X5EP9YpfORMk6zbjIR6Ms5ZE62lAqPu8dtXXv9CJ-Wwterw2p14bUX4ZEWGzgN93R6geyHt9Vk83Of-97kC8</recordid><startdate>201910</startdate><enddate>201910</enddate><creator>Viani, A.</creator><creator>Mácová, P.</creator><creator>Machová, D.</creator><creator>Čendak, T.</creator><general>Wiley Subscription Services, Inc</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0002-6019-1094</orcidid><orcidid>https://orcid.org/0000-0002-0528-3930</orcidid></search><sort><creationdate>201910</creationdate><title>The Assessment of Bone Deterioration with Nuclear Magnetic Resonance Spectroscopy in a Multidisciplinary Context: The Case of the UNESCO World Heritage Site of Sedlec, Czechia</title><author>Viani, A. ; Mácová, P. ; Machová, D. ; Čendak, T.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a3245-18a9eec08c42e189b9bebdaf7fa1a2d7c38f7ef0c9ca0411e5423f9b450ad7683</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>archaeological bones</topic><topic>bone diagenesis</topic><topic>Deterioration</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Phosphorus</topic><topic>Resonance</topic><topic>Spectroscopy</topic><topic>Spectrum analysis</topic><topic>taphonomy</topic><topic>World Heritage Areas</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Viani, A.</creatorcontrib><creatorcontrib>Mácová, P.</creatorcontrib><creatorcontrib>Machová, D.</creatorcontrib><creatorcontrib>Čendak, T.</creatorcontrib><collection>CrossRef</collection><jtitle>Archaeometry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Viani, A.</au><au>Mácová, P.</au><au>Machová, D.</au><au>Čendak, T.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The Assessment of Bone Deterioration with Nuclear Magnetic Resonance Spectroscopy in a Multidisciplinary Context: The Case of the UNESCO World Heritage Site of Sedlec, Czechia</atitle><jtitle>Archaeometry</jtitle><date>2019-10</date><risdate>2019</risdate><volume>61</volume><issue>5</issue><spage>1144</spage><epage>1159</epage><pages>1144-1159</pages><issn>0003-813X</issn><eissn>1475-4754</eissn><abstract>Human remains from the skeletal collection of the UNESCO world heritage site of Sedlec (Czechia) have been investigated with 1H, 31P and 13C magic‐angle‐spinning nuclear magnetic resonance spectroscopy. 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| language | eng |
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| subjects | archaeological bones bone diagenesis Deterioration NMR Nuclear magnetic resonance Phosphorus Resonance Spectroscopy Spectrum analysis taphonomy World Heritage Areas |
| title | The Assessment of Bone Deterioration with Nuclear Magnetic Resonance Spectroscopy in a Multidisciplinary Context: The Case of the UNESCO World Heritage Site of Sedlec, Czechia |
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